This study aimed to establish a method that uses inductively coupled plasma mass spectrometry (ICP-MS) to simultaneously determine lead, arsenic, aluminum, chromium, iron, and copper in dried aquatic products. Samples were digested in automatic graphite digestion, followed by quantitative tests using internal standard method by ICP-MS. The results showed that the concentrations of lead, arsenic, aluminum, chromium, iron, and copper showed good linear relationships in the range of 0.25-25 μg/L, with correlation coefficients (R2) higher than 0.990. The detection limits for lead,arsenic,aluminum,chromium,iron,and copper were 0.02 μg/L, 0.08 μg/L, 0.12 μg/L, 0.10 μg/L, 0.03 μg/L, and 0.05 μg/L, respectively. The recovery rate was 84.0%-108.4%. The relative standard deviation of reproducibility was less than 10% (n=6). This method was proved to be simple, accurate, with low detection limits and good reproducibility, which can be used to detect metals in dried aquatic products.
ZHANG Hongyan
,
DING Wu
,
WU Fuxiang
,
WANG Xiaoqiao
,
LIU Xiaoxiao
,
MIAO Qian
,
ZHANG Jie
. Automatic graphite digestion and inductively coupled plasma massspectrometry for monitoring lead, arsenic, aluminum, chromium, iron, andcopper in dried aquatic products[J]. Food and Fermentation Industries, 2019
, 45(3)
: 266
-269
.
DOI: 10.13995/j.cnki.11-1802/ts.017281
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