Orthogonal test design for optimization of extraction process of Elsholtzia bodinieri Vaniot oil and formula of herbal tea beverage

  • ZHAN Yong ,
  • FAN Baomin ,
  • LIAO Xia ,
  • YANG Yong
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  • 1 (Chongqing Academy of Chinese Materia Medica, Chongqing 400065, China)
    2 (Yunnan Minzu University, Kunming 650031, China)

Received date: 2019-05-21

  Online published: 2020-02-10

Abstract

Herbal tea beverage was developed with Elsholtzia bodinieri Vaniot as raw material, with the most favorable extraction conditions and the optimal formula of herbal tea beverage explored and determined in this study. By L9(34) orthogonal test design method, the most favorable technical parameters for essence oil extraction were determined with extraction rate as the index and the optimal formula of the herbal tea beverage was determined with sensory score as the index. The results showed that the most favorable extraction conditions of E. bodinieri essence oil were: solid-liquid ratio of 1∶16 g/mL, soaking time for 2 h, distillation for 8 h, and aromatic water flow rate of 0.7 mL/min for an extraction rate of 0.60%; while the optimal formula of the herbal tea beverage was: sugar 55 g/L, E. bodinieri juice 15 g/L, citric acid 3 g/L, essence oil 5 g/L. The best stability was achieved with 0.4 g/L xanthan gum and 0.8 g/L CMC-Na used as stabilizers, when the precipitation rate was 6.3%. Such herbal tea beverage featured soluble solids content above 5.6%, total acid (in citric acid) of 0.28 g/kg and compliance in microbial indicators. These results would provide a theoretical basis for research on E. bodinieri oil, as well as a reference for product development based on E. bodinieri.

Cite this article

ZHAN Yong , FAN Baomin , LIAO Xia , YANG Yong . Orthogonal test design for optimization of extraction process of Elsholtzia bodinieri Vaniot oil and formula of herbal tea beverage[J]. Food and Fermentation Industries, 2019 , 45(24) : 196 -201 . DOI: 10.13995/j.cnki.11-1802/ts.021160

References

[1] 毛媛.东紫苏中木犀草苷的分离及其生物活性研究[D].上海:上海海洋大学,2016.
[2] 罗燕,王文静,张红霞,等.东紫苏昆明居群叶特征与挥发油的相关性研究[J].时珍国医国药,2017,28(5): 198-201.
[3] 周林宗,马永杰,蒋金,等.大理产凤尾茶挥发油成分的研究[J].安徽农业科学,2009,37(18):8 461-8 462.
[4] ZHONG J D,ZHAO X W,LI H M,et al.Five new oleanane triterpenoid saponins from the aerial parts of elsholtzia bodinieri[J].Helvetica Chimica Acta,2016,99(3):204-209.
[5] HU H B,JIAN Y F,CAO H,et al.Phenolic compounds from Elsholtzia bodinieri Van't [J].Journal of the Chinese Chemical Society, 2013,54(5):1 189-1 194.
[6] 毛媛,刘克武,刘克海,等.东紫苏化学成分研究概述[J].中国中医药信息杂志,2016,23(3):134-136.
[7] 胡浩斌,曹宏,刘建新,等.微波溶样ICP-AES法测定甘肃东紫苏中的无机元素[J].光谱学与光谱分析,2006, 26(11):2 130-2 133.
[8] ZHONG J D,FENG Y,LI H M,et al.A new flavonoid glycoside from Elsholtzia bodinieri [J].Natural Product Research,2016,30(20):1-5.
[9] 毛媛,吕留庄,刘克武,等.东紫苏(Elsholtiza bodinieri Vaniot)总黄酮的提取及其抗氧化、免疫活性的研究[J].食品工业科技, 2016,37(9):85-88.
[10] XIANG L,ZHANG L,CHEN X,et al.Ursane-type triterpenoid saponins from Elsholtzia bodinieri[J].Natural Product Research,2018,33(9):1-8.
[11] 方舒婷,曾荣,李海贤,等.苗族特色凉茶饮料的开发[J].农产品加工,2018(10):1-5.
[12] 何薇.核桃分心木总黄酮提取工艺及复合凉茶饮料研制[D].绵阳:西南科技大学,2018.
[13] 邓开野,缪晓平.凉茶抗微生物作用的研究进展[J].广东农业科学,2010,37(6):158-159.
[14] JESZKA S M,ZGOLA G A,FRANKOWSKI R.Cistus incanus a promising herbal tea rich in bioactive compounds: LC-MS/MS determination of catechins, flavonols, phenolic acids and alkaloids—A comparison with Camellia sinensis, Rooibos and Hoan Ngoc herbal tea [J].Journal of Food Composition and Analysis,2018, 74:71-81.
[15] 张科明,许杨彪,刘向红,等. QuEChERS-液质联用法快速测定凉茶中非法添加的10种止咳平喘类化学药物[J].食品工业科技,2018,39(24):294-297.
[16] 陈康,李洪军,贺稚非.金银花乳杆菌发酵凉茶的研制[J].食品科学,2016,37(3):131-136.
[17] 王霞,许菊香,于晓明,等.尾叶香茶菜挥发油的提取工艺及其抗菌和抗氧化作用[J].福建农业学报,2016,31(7):747-751.
[18] 支梓鉴,张萌,褚冠勇,等.三根汤凉茶的工艺研究[J].食品工业科技,2012,33(22):299-302.
[19] 韩翠萍,秦培正,汤慧娟.姜香奶茶的加工工艺研究[J].中国乳品工业,2013,41(10):52-54.
[20] 胡小军,江敏,蔡春菊,等.胡萝卜木瓜南瓜复合保健饮料的研制[J].食品研究与开发,2009,30(9):113-115.
[21] 杨柳,邵婷,钟金锋,等.三种稳定剂对猕猴桃椰汁复合乳饮料稳定性的影响[J].食品与发酵工业, 2019, 45(10): 116-121;128.
[22] GB/T 12143—2008 饮料通用分析方法[S].北京:中国标准出版社,2008.
[23] GB/T 12456—2008 食品中总酸的测定[S].北京:中国标准出版社,2008.
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