Food and Fermentation Industries >

2024 , Vol. 50 >Issue 18: 317 - 325

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.039453

Rapid determination of 106 kinds of pesticide residues in peach gum by μ-QuEChERS and gas chromatography-triple quadrupole tandem masss pectrometry

  • PENG Rulin ,
  • YIN Zhuojun ,
  • LIU Yuanyuan ,
  • LONG Meichen ,
  • TANG Su ,
  • ZENG Ting ,
  • ZHANG Wenglong ,
  • ZHU Yutian
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  • (Shenzhen Academy of Metrology and Quality Inspection, Shenzhen 518131, China)

Received date: 2024-04-04

  Revised date: 2024-05-08

  Online published: 2024-10-14

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Abstract

To establish a method for the rapid determination of 106 kinds of pesticide residues simuletaneously in Peach gum by gas chromatography- triple quadrupole tandem mass spectrometry(GC-MS/MS) with μ-QuEChERS in 10 minutes.The samples were extracted and purified by μ-QuEChERS method, and then the pesticide residues separated by highly inert gas chromatographic column and analyzed by GC-MS/MS.Within the range of 0.002-0.400 mg/kg, the correlation coefficient of all pesticides is higher than 0.995.The detection limit and quantitation were (5.84×10-6)-(2.81×10-4) mg/kg and (1.95×10-5)-(9.36×10-3) mg/kg, respectively.Overall recoveries and relative standard deviations (RSDs) were ranged from 72% to 109% and from 0.73% to 10%, respectively.The method has the advantages of fast, less pollution and better reliability, which is suitable for rapid qualitative and quantitative detection of multiple pesticide residues in peach gum.

Key words： μ-QuEChERS; highly inert gas chromatographic column; gas chromatography-triple quadrupole tandem mass spectrometry; peach gum; pesticide residues

Cite this article

PENG Rulin , YIN Zhuojun , LIU Yuanyuan , LONG Meichen , TANG Su , ZENG Ting , ZHANG Wenglong , ZHU Yutian . Rapid determination of 106 kinds of pesticide residues in peach gum by μ-QuEChERS and gas chromatography-triple quadrupole tandem masss pectrometry[J]. Food and Fermentation Industries, 2024 , 50(18) : 317 -325 . DOI: 10.13995/j.cnki.11-1802/ts.039453

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