Food and Fermentation Industries >

2024 , Vol. 50 >Issue 20: 273 - 278

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.037888

Comparing contents of phenylethanol glycosides in two different host Cistanches Herba after different drying treatments

  • GAO Peiwen ,
  • GUO Yehong ,
  • ZHAO Fafa ,
  • ZHANG Dan ,
  • ZHANG Fangming
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  • 1(Agronomy College, Gansu Agricultural University, Lanzhou 730070, China)
    2(State Key Laboratory of Aridland Crop Science, Lanzhou 730070, China)

Received date: 2023-11-07

  Revised date: 2023-12-07

  Online published: 2024-11-01

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Abstract

This study aimed to compare the content of 10 phenylethanoid glycosides in different processed Cistanches Herba from different hosts using ultra-high performance liquid chromatography-triple quadrupole mass spectrometry (UPLC-QQQ-MS).The dried Cistanches Herba was crushed, sieved through a 60-mesh sieve, and extracted by ultrasound with 50% methanol.Separation was performed on an Agilent Eclipse Plus C18 column (2.1 mm×150 mm, 1.8 μm) using gradient elution with mobile phase A (0.1% formic acid aqueous solution) and B (acetonitrile).Detection was carried out in dynamic multiple reaction monitoring mode using an electrospray ionization source in UPLC-QQQ-MS.Results showed that significant variations were observed in the composition of 10 phenylethanoid glycosides among Cistanches Herba cultivated on different hosts and subjected to various drying treatments.Freeze-dried Cistanches Herba showed the highest content of these compounds for both host plants, followed by drying at 80 ℃.Although freeze-drying preserved the maximum content of 10 phenylethanoid glycosides in Cistanches Herba, drying at 80 ℃ was more cost-effective for large-scale production.

Key words： ultra-high performance liquid chromatography-triple quadrupole mass spectrometry; Cistanches Herba; Haloxylon ammodendron (C.A.Mey.) Bunge; Atriplex canescens (Pursh) Nutt; phenylethanoid glycosides; drying method

Cite this article

GAO Peiwen , GUO Yehong , ZHAO Fafa , ZHANG Dan , ZHANG Fangming . Comparing contents of phenylethanol glycosides in two different host Cistanches Herba after different drying treatments[J]. Food and Fermentation Industries, 2024 , 50(20) : 273 -278 . DOI: 10.13995/j.cnki.11-1802/ts.037888

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