[1] MUSCHIETTI L, REDKO F, ULLOA J. Adulterants in selected dietary supplements and their detection methods[J]. Drug Testing and Analysis, 2020, 12(7):861-886.
[2] 宁霄, 张伟清, 王钢力, 等. 保健食品中非法添加药物的检测现状及筛查策略研究[J]. 食品安全质量检测学报, 2015, 6(5):1876-1882.
NING X, ZHANG W Q, WANG G L, et al. Detection status and screening strategy of illegally added drugs in healthy food[J]. Journal of Food Safety & Quality, 2015, 6(5):1876-1882.
[3] 田甜, 覃艳淑, 赵德恩, 等. 食品和保健食品中非法添加药物的筛查探究[J]. 食品安全质量检测学报, 2021, 12(3):1200-1208.
TIAN T, QIN Y S, ZHAO D E, et al. Research of screening of illegal added drugs in food and health food[J]. Journal of Food Safety & Quality, 2021, 12(3):1200-1208.
[4] CORONA G, RASTRELLI G, BURRI A, et al. First-generation phosphodiesterase type 5 inhibitors dropout: A comprehensive review and meta-analysis[J]. Andrology, 2016, 4(6):1002-1009.
[5] NAGASAWA S, SAKA K J, YAMAGISHI Y, et al. Association between sexual activity-related death and non-prescription use of phosphodiesterase type 5 inhibitors[J]. Legal Medicine, 2021, 48:101815.
[6] EIDEN C, LAUREAU M, RICHEVAL C, et al. Acute cardiovascular disorders related to aphrodisiac honey (“Jaguar power”) consumption: Warning of unintentional exposure to Sildenafil[J]. La Revue de Medecine Interne, 2022, 43(1):68-69.
[7] 刘素丽. 食品中非法添加物质情况及其检测方法研究概述[J]. 中国食品药品监管, 2022(8):90-95.
LIU S L. Research on illegally added substances and the relevant detection methods in food[J]. China Food & Drug Administration Magazine, 2022(8):90-95.
[8] 陈燕, 严丽娟, 徐敦明, 等. 高效液相色谱-串联质谱法同时检测蒸馏酒及其配制酒中90种那非类物质[J]. 分析测试学报, 2023, 42(5):519-530.
CHEN Y, YAN L J, XU D M, et al. Simultaneous determination of 90 nafils in distilled liquor and its products by QuEChERS/high performance liquid chromatography-tandem mass spectrometry[J]. Journal of Instrumental Analysis, 2023, 42(5):519-530.
[9] LEE J H, PARK O R, YANG Y J, et al. Detection of 94 PDE-5is and their analogs including N-desmethylthiosildenafil in various formulations of dietary supplements and food samples using HPLC and LC-Q-TOF/MS[J]. Journal of Chromatographic Science, 2022, 60(10):953-962.
[10] KIM U, CHO H D, KANG M H, et al. Screening of phosphodiesterase-5 inhibitors and their analogs in dietary supplements by liquid chromatography-hybrid ion trap-time of flight mass spectrometry[J]. Molecules, 2020, 25(12):2734.
[11] NGUYEN T O, TRAN C S, DO T T H, et al. Rapid screening and quantitative determination of illegal phosphodiesterase type 5 inhibitors (PDE-5i) in herbal dietary supplements[J]. Journal of Analytical Methods in Chemistry, 2021, 2021(1):5579500.
[12] 孙婷婷, 徐彦红, 张雪梅, 等. HPLC法快速筛查保健酒中那非药物及质谱确证[J]. 食品研究与开发, 2018, 39(17):197-204.
SUN T T, XU Y H, ZHANG X M, et al. Rapid determination of nafil drug in health wine by high performance liquid chromatography and their verification by mass spectrometry[J]. Food Research and Development, 2018, 39(17):197-204.
[13] 郑娟梅, 余婉松, 覃文霞, 等. 表面增强拉曼光谱法快速测定保健酒中西地那非[J]. 食品安全质量检测学报, 2018, 9(21):5659-5665.
ZHENG J M, YU W S, QIN W X, et al. Rapid determination of Sildenafil in health wine by surface-enhanced Raman scattering[J]. Journal of Food Safety & Quality, 2018, 9(21):5659-5665.
[14] 吴国萍, 周亚红, 李静泉, 等. 表面增强拉曼光谱测定保健品中非法添加物西地那非[J]. 食品工业科技, 2019, 40(11):254-259; 264.
WU G P, ZHOU Y H, LI J Q, et al. Surface enhanced Raman spectroscopy(SERS) for the detection of Sildenafil in health care products[J]. Science and Technology of Food Industry, 2019, 40(11):254-259; 264.
[15] 司星宇, 陈致, 周千渝, 等. 保健品中西地那非和他达拉非的拉曼光谱同时检测方法研究[J]. 光散射学报, 2022, 34(1):30-35.
SI X Y, CHEN Z, ZHOU Q Y, et al. Simultaneous detection of Sildenafil and tadalafil in healthcare products by Raman spectroscopy[J]. The Journal of Light Scattering, 2022, 34(1):30-35.
[16] 胡家勇, 彭青枝, 张莉, 等. 表面增强拉曼光谱技术在快速检测保健食品中非法添加药物中的应用[J]. 食品安全质量检测学报, 2021, 12(1):7-15.
HU J Y, PENG Q Z, ZHANG L, et al. Application of surface-enhanced Raman spectroscopy in the rapid detection of illegal additives in health food[J]. Journal of Food Safety & Quality, 2021, 12(1):7-15.
[17] FRENS G. Controlled nucleation for the regulation of the particle size in monodisperse gold suspensions[J]. Nature Physical Science, 1973, 241(105):20-22.
[18] HAISS W, THANH N T K, AVEYARD J, et al. Determination of size and concentration of gold nanoparticles from UV-vis spectra[J]. Analytical Chemistry, 2007, 79(11):4215-4221.
[19] HU J Y, ZHOU T H, YAO X F, et al. Screening of PDE-5 inhibitors in health wine by surface-enhanced Raman spectroscopy[J]. Food and Machinery, 2022, 38(9):64-71.
[20] 李丹, 姬瑞瑞, 陈辉, 等. 手持式拉曼光谱快速检测功能饮料非法添加西地那非的研究[J]. 海军医学杂志, 2019, 40(5):436-439.
LI D, JI R R, CHEN H, et al. Rapid detection of illegal addition of Sildenafil citrate in functional beverage by nano-surface enhanced Raman spectroscopy[J]. Journal of Navy Medicine, 2019, 40(5):436-439.
[21] WANG H M, LI L L, CHEN H B, et al. Simultaneous detection of sildenafil and tadalafil in healthcare products by Raman spectroscopy[J]. Chemical Journal Of Chinese Universities, 2017, 38(6): 1040-1045.
[22] 李秀明, 李金阳, 刘新兰. 纳米银溶胶稳定性的考察及其对表面增强拉曼光谱检测的影响[J]. 药物分析杂志, 2013, 33(6):1048-1053.
LI X M, LI J Y, LIU X L. Stability of nano silver particles and the influence on surface-enhanced Raman spectroscopic detection[J]. Chinese Journal of Pharmaceutical Analysis, 2013, 33(6):1048-1053.
[23] YING Y, TANG Z Y, LIU Y L. Material design, development, and trend for surface-enhanced Raman scattering substrates[J]. Nanoscale, 2023, 15(26):10860-10881.
[24] 冯彦婷, 林沛纯, 谢慧风, 等. 基于纳米银颗粒团聚反应的表面增强拉曼光谱法测定牛奶中三聚氰胺的含量[J]. 食品与发酵工业, 2019, 45(15):256-261.
FENG Y T, LIN P C, XIE H F, et al. Determination of melamine in milk based on silver nanoparticles aggregation by surface enhanced Raman spectroscopy[J]. Food and Fermentation Industries, 2019, 45(15):256-261.
[25] DA SILVEIRA G D, BRESSAN L P, SCHMIDT M E P, et al. Electrochemical behavior of 5-type phosphodiesterase inhibitory drugs in solid state by voltammetry of immobilized microparticles[J]. Journal of Solid State Electrochemistry, 2020, 24(8):1999-2010.
[26] ROUHANI M, SOLEYMANPOUR A. Molecularly imprinted Sol-gel electrochemical sensor for Sildenafil based on a pencil graphite electrode modified by Preyssler heteropolyacid/gold nanoparticles/MWCNT nanocomposite[J]. Mikrochimica Acta, 2020, 187(9):512.
[27] HE F, YANG J Y, ZOU T T, et al. A gold nanoparticle-based immunochromatographic assay for simultaneous detection of multiplex Sildenafil adulterants in health food by only one antibody[J]. Analytica Chimica Acta, 2021, 1141:1-12.
[28] SONG M S, WU Q, LIU B B, et al. Using a quantum dot bead-based lateral flow immunoassay to broadly detect the adulteration of PDE-5 inhibitors in functional foods[J]. Analytical Methods, 2022, 14(26):2586-2595.
[29] WANG X Y, HUANG M, LI X G, et al. Rapid screening of illegal additives in functional food using atmospheric pressure solids analysis probe coupled to a portable mass spectrometer[J]. Journal of Pharmaceutical and Biomedical Analysis, 2022, 214:114722.
[30] QI R R, WANG X Y, HUANG M, et al. Rapid screening of illegal additives in functional food using desorption electrospray ionization mass spectrometry imaging[J]. Journal of Pharmaceutical and Biomedical Analysis, 2023, 229:115351.
[31] ICHIKAWA-KAJI Y, ISHIZAWA F, NISHIYAMA R, et al. Development of a detector tube for screening tadalafil and its analogues in adulterated sexual enhancement products[J]. Drug Testing and Analysis, 2023, 15(3):345-360.
[32] GHEORGHIU O R C, CIOBANU A M, GUTU C M, et al. Determination of phosphodiesterase type-5 inhibitors (PDE-5) in dietary supplements[J]. Molecules, 2023, 28(10):4116.
[33] PIORUNSKA-SEDLAK K, STYPULKOWSKA K. Selectivity of identification of compounds from the group of phosphodiesterase-5 inhibitors (PDE-5i) in falsified products from the Polish market using attenuated total reflectance Fourier transform infrared spectroscopy and X-ray powder diffraction[J]. Science & Justice, 2021, 61(6):714-722.