Appellation identification of wines from different small production areas in Ningxia based on mineral elements

  • CUI Zefang ,
  • KAI Jianrong ,
  • ZHANG Yuanke ,
  • LIU Na ,
  • JIANG Wenguang ,
  • GE Qian ,
  • MA Tingting ,
  • FANG Yulin ,
  • SUN Xiangyu
Expand
  • 1(College of Enology, Northwest A&F University, Yangling 712100, China)
    2(Ningxia Research Institute of Quality Standards and Testing Technology of Agricultural Products, Yinchuan 750002, China)
    3(Ningxia Changyu Longyu Estate Co.Ltd., Yinchuan 750002, China)
    4(Shaanxi Provincial Key Laboratory of Viti-Viniculture, Yangling 712100, China)
    5(Shaanxi Engineering Research Center of Characteristic Fruit Directional Design and Machining, Yangling 712100, China)

Received date: 2024-07-29

  Revised date: 2024-09-07

  Online published: 2025-08-04

Abstract

By detecting and analyzing the mineral element content of wines in different core small producing areas of Ningxia, combined with multivariate statistical analysis method, a regional scale wine producing area identification model based on mineral elements in the province (autonomous region) was established.In this study, Cabernet Sauvignon grapes were collected from five small production areas of Yinchuan, Helan, Yongning, Qingtongxia and Hongsipu in Ningxia, and 78 cabernet sauvignon wine samples were obtained by using the same method.The contents of 57 mineral elements such as B, Bi and Be were determined by ICP-MS, and the 57 mineral elements were analyzed by principal component analysis.The extracted principal components were used as input variables for LDA statistical analysis, and the origin discrimination model was constructed.The results showed that among the 57 mineral elements detected in wines, the contents of 46 elements were significantly different between different production areas in Ningxia (P<0.05).Through principal component analysis(PCA), 13 principal components were successfully extracted from the 57 mineral elements, and the total variance contribution reached 86.931%.Based on Fisher discriminant analysis method, a wine region identification model was established.The correct discriminant rates of back generation test and cross-verification were 100% and 98.7%, which realized the discrimination of wines from different small production areas in the geographical scale within Ningxia, and proved that the traceability technology of mineral elements could be used for the identification of wine production areas in the geographical scale within the province (autonomous region).

Cite this article

CUI Zefang , KAI Jianrong , ZHANG Yuanke , LIU Na , JIANG Wenguang , GE Qian , MA Tingting , FANG Yulin , SUN Xiangyu . Appellation identification of wines from different small production areas in Ningxia based on mineral elements[J]. Food and Fermentation Industries, 2025 , 51(13) : 311 -319 . DOI: 10.13995/j.cnki.11-1802/ts.040597

References

[1] 李媛媛, 李德美, 张亚东, 等.赤霞珠干红葡萄酒在不同子产区香气特征的差异[J].食品与发酵工业, 2020, 46(6):256-262;268.
LI Y Y, LI D M, ZHANG Y D, et al.Comparative study of aroma characteristics of Cabernet Sauvignon dry red wine in different sub-regions[J].Food and Fermentation Industries, 2020, 46(6):256-262;268.
[2] 刘紫凌, 靳赫, 任玮.戈壁荒滩上打造“紫色奇迹”:宁夏葡萄酒产业发展新观察[J].中国产经, 2023(11):46-51.
LIU Z L, JIN H, REN W.Creating “purple miracle” on Gobi Desert—a new observation on the development of wine industry in Ningxia[J].Chinese Industry & Economy, 2023(11):46-51.
[3] 高艾英, 韩德娟, 李凤玲, 等.ICP-MS法检测山东省境内蜂蜜矿质元素及产地溯源性研究[J].中国计量, 2023(12):68-73.
GAO A Y, HAN D J, LI F L, et al.Determination of honey mineral elements in Shandong Province by ICP-MS and traceability to its origin[J].China Metrology, 2023(12):68-73.
[4] 王静娴, 张昂.稳定同位素和矿质元素指纹在蜂蜜产地溯源中的发展与应用[J].食品安全导刊, 2023(13):165-167.
WANG J X, ZHANG A.Development and application of stable isotope and mineral element fingerprint in honey origin traceability[J].China Food Safety Magazine, 2023(13):165-167.
[5] 罗钦, 陈谢勇, 徐梦婷, 等.不同海拔区间白茶化学元素特征分析及产地判别[J].核农学报, 2024, 38(3):481-493.
LUO Q, CHEN X Y, XU M T, et al.Characteristic analysis of chemical elements and identification of production regions of white tea from different altitudes intervals[J].Journal of Nuclear Agricultural Sciences, 2024, 38(3):481-493.
[6] 徐芝亮, 章新泉.基于电感耦合等离子体串联质谱法分析矿物元素的江西茶叶产地溯源[J].食品安全质量检测学报, 2024, 15(4):186-193.
XU Z L, ZHANG X Q.Geographical origin traceability of tea in Jiangxi Province based on inductively coupled plasma tandem mass spectrometry analysis of trace mineral elements[J].Journal of Food Safety & Quality, 2024, 15(4):186-193.
[7] 李涛, 王斌, 王玉, 等.静宁苹果的矿质元素特征及产地溯源[J].甘肃农业大学学报, 2025,60(1):181-192.
LI T, WANG B, WANG Y, et al.Mineral element characteristics and origin tracing of Jingning apple[J].Journal of Gansu Agricultural University,2025,60(1):181-192.
[8] 谭椰子, 李涛, 王玉, 等.不同产地苹果的品质成分分析与产地判别[J].农产品质量与安全, 2023(6):75-80.
TAN Y Z, LI T, WANG Y, et al.Quality components analysis and geographical origin distinguishing for apples from different producing areas[J].Quality and Safety of Agro-Products, 2023(6):75-80.
[9] 宗万里. 西藏自治区牦牛肉产地溯源技术研究[D].北京:中国农业科学院, 2023.
ZONG W L.Research on the traceability technology of yak beef origin in the Tibet autonomous region[D].Beijing:Journal of Integrative Agriculture (JIA), 2023.
[10] GAO F F, HAO X Y, ZENG G H, et al.Identification of the geographical origin of Ecolly (Vitis vinifera L.) grapes and wines from different Chinese regions by ICP-MS coupled with chemometrics[J].Journal of Food Composition and Analysis, 2022, 105:104248.
[11] PŁOTKA-WASYLKA J, FRANKOWSKI M, SIMEONOV V, et al.Determination of metals content in wine samples by inductively coupled plasma-mass spectrometry[J].Molecules, 2018, 23(11):2886.
[12] 宋向飞. 基于矿质元素指纹图谱技术的碧螺春茶产地溯源研究[D].南京:南京农业大学, 2018.
SONG X F.Study on origin traceability of biluochun tea based on mineral element fingerprint technology[D].Nanjing:Nanjing Agricultural University, 2018.
[13] SHIMIZU H, AKAMATSU F, KAMADA A, et al.Effects of variety and vintage on the minerals of grape juice from a single vineyard[J].Journal of Food Composition and Analysis, 2022, 107:104377.
[14] 李彩虹. 不同品种、产地葡萄酒中酚类物质差异性分析研究[Z].宁夏回族自治区:宁夏农产品质量标准与检测技术研究所, 2021.
LI C H.Study on the differences of phenolic substances in wines of different varieties and origins[Z].Ningxia Autonomous Region:Ningxia Institute of Agricultural Products and Testing Technology, 2021.
[15] PASVANKA K, KOSTAKIS M, TARAPOULOUZI M, et al.ICP-MS analysis of multi-elemental profile of Greek wines and their classification according to variety, area and year of production[J].Separations, 2021, 8(8):119.
[16] 李彩虹, 开建荣, 闫玥, 等.基于矿质元素的我国不同产地葡萄酒的判别分析[J].食品与发酵工业, 2022, 48(20):265-272.
LI C H, KAI J R, YAN Y, et al.Discriminant analysis of wines from different regions of China based on mineral elements[J].Food and Fermentation Industries, 2022, 48(20):265-272.
[17] 吕真真, 谢辉, 庞荣丽, 等.基于矿质元素的赤霞珠葡萄酒产地溯源[J].食品研究与开发, 2023, 44(19):159-164.
LYU Z Z, XIE H, PANG R L, et al.Origin tracing of cabernet sauvignon wine based on mineral elements[J].Food Research and Development, 2023, 44(19):159-164.
[18] 程文娟, 苏颖玥, 李潇潇, 等.矿质元素指纹技术结合化学计量学分析对中国葡萄酒原产地的判别研究[J].中外葡萄与葡萄酒, 2022(3):31-37.
CHENG W J, SU Y Y, LI X X, et al.Discrimination of Chinese wine origin by multi-element fingerprint technology combined with chemometrics analysis[J].Sino-Overseas Grapevine & Wine, 2022(3):31-37.
[19] AZCARATE S M, MARTINEZ L D, SAVIO M, et al.Classification of monovarietal Argentinean white wines by their elemental profile[J].Food Control, 2015, 57:268-274.
[20] CHEN K X, XUE H T, SHI Q, et al.Geographical identification of Chinese wine based on chemometrics combined with mineral elements, volatile components and untargeted metabonomics[J].Food Chemistry:X, 2024, 22:101412.
[21] 李燕, 贺燕, 邹金浩, 等.基于主成分和聚类分析的不同品种淮山淀粉品质评价[J].中国粮油学报, 2023, 38(10):223-230.
LI Y, HE Y, ZOU J H, et al.Quality evaluation of different cultivars of yam starches based on principal component analysis and cluster analysis[J].Journal of the Chinese Cereals and Oils Association, 2023, 38(10):223-230.
[22] 罗红霞, 王丽, 句荣辉, 等.不同品种谷子淀粉的品质特性及主成分分析[J].食品工业科技, 2018, 39(24):11-17.
LUO H X, WANG L,JU R H, et al.Quality characteristics and principal component analysis of different varieties of millet starch[J].Science and Technology of Food Industry, 2018, 39(24):11-17.
[23] 开建荣, 石欣, 李彩虹, 等.基于矿物元素技术的中宁不同产区枸杞的判别分析[J].食品与发酵工业, 2022, 48(9):253-260.
KAI J R, SHI X, LI C H, et al.Discrimination of Lycium barbarum from different areas in Zhongning based on mineral element technique[J].Food and Fermentation Industries, 2022, 48(9):253-260.
[24] 钱丽丽, 邱彦超, 李殿威, 等.基于产地、品种和年份影响矿物元素含量的大米判别[J].食品科学, 2021, 42(16):322-327.
QIAN L L, QIU Y C, LI D W, et al.Influence of geographical origin, variety and crop year on mineral element contents of rice and geographical origin discrimination based on mineral elements[J].Food Science, 2021, 42(16):322-327.
[25] 赵子丹, 开建荣, 王彩艳, 等.基于矿物元素技术的宁夏不同产地红枣的判别分析[J].经济林研究, 2022, 40(4):133-142.
ZHAO Z D, KAI J R, WANG C Y, et al.Discriminant analysis of red jujube from different origin in Ningxia based on mineral element technology[J].Non-wood Forest Research, 2022, 40(4):133-142.
Outlines

/