In response to the problems of freeze-dried milk-chocolate, such as high fat content, high cost, and poor oral solubility.The formula of conventional freeze-dried (CFD) milk chocolate was optimized through the response surface experiment.And then, the drying characteristics and the quality of dried products were compared between CFD and microwave assisted conventional freeze-drying (MCFD).Results showed that the optimal formula for CFD milk chocolate was 15% milk powder (based on milk quality), 3∶1 milk to chocolate mass ratio, and 6% of modified starch (based on total milk and chocolate mass).The hardness of the produced products was (8.21±0.44) N, the brittleness was (6.70±1.20) N, and the rehydration time was (8.88±1.49) s.Compared with CFD, MCFD could reduce the freeze-drying time by 41.94%, reduce the unit energy consumption by 60.58%, and the drying uniformity was much higher than the industry standard.The microstructures of MCFD products was more porous and the rehydration time was shorter.This study provides a reference for the industrial and healthy development of freeze-dried milk chocolate.
[1] 屠用利. 影响牛奶巧克力风味的因素[J].食品工业, 2001, 22(6):14-16.
TU Y L.Factors affecting the flavor of milk chocolate[J].Food Industry, 2001,22 (6):14-16.
[2] 李阳, 李佳佳, 杨晨昱, 等.牛奶巧克力基础配方研究[J].中国果菜, 2020, 40(2):22-27.
LI Y, LI J J, YANG C Y, et al.Study on the basic formula of milk chocolate[J].China Fruit and Vegetable, 2020, 40(2):22-27.
[3] 胡泊潇. 大豆酸奶冻干块的研制及品质影响因素研究[D].无锡:江南大学, 2022.
HU B X.Research on the development and quality influencing factors of soy yogurt freeze-dried blocks[D].Wuxi:Jiangnan University, 2022.
[4] 姜佳慧. 草莓微波冻干过程及品质调控研究[D].无锡:江南大学, 2021.
JIANG J H.Research on microwave freeze drying process and quality control of strawberries[D].Wuxi:Jiangnan University, 2021.
[5] 郭政铭. 脉冲喷动床微波冻干山楂中试工艺与品质调控研究[D].无锡:江南大学, 2023.
GUO Z M.Study on the pilot process and quality control of microwave freeze-drying hawthorn using pulse fluidized bed[D].Wuxi:Jiangnan University, 2023.
[6] 郭政铭, 王博, 王玉川, 等.中试脉冲喷动床微波冻干山楂干燥特性与品质特性研究[J].食品与发酵工业, 2024, 50(7):227-235.
GUO Z M, WANG B, WANG Y C, et al.Drying and quality characteristics of hawthorn after pilot-scale pulse-spouted bed microwave freeze-drying[J].Food and Fermentation Industries, 2024, 50(7):227-235.
[7] 王玉川. 莴苣颗粒负压微波高效节能均匀干燥机理及工艺研究[D].无锡:江南大学, 2013.
WANG Y C.Research on the mechanism and process of high efficiency, energy saving and uniform drying of lettuce granules by negative pressure microwave[D].Wuxi:Jiangnan University, 2013.
[8] 金鑫, 段续, 任广跃, 等.不同干燥方式对无花果干燥特性及品质的影响[J].食品与发酵工业, 2024, 50(10):69-75.
JIN X, DUAN X, REN G Y, et al.Effects of different drying methods on the drying characteristics and quality of figs[J].Food and Fermentation Industries, 2024, 50 (10):69-75.
[9] 李荣华, 徐红华, 温其标.乳成分对酸奶凝胶微观结构和流变学性质的影响[J].中国乳品工业, 2007, 35(1):27-30.
LI R H, XU H H, WEN Q B.Effect of milk component on the microstructure and rheological properties of yogurt gel[J].China Dairy Industry, 2007, 35(1):27-30.
[10] 汪清美, 徐源, 张雨洁, 等.乳清蛋白粉与豆乳不同质量比对凝固型沙棘酸奶品质的影响[J].粮食与油脂, 2024, 37(8):90-93;99.
WANG Q M, XU Y, ZHANG Y J, et al.Effect of different mass ratios of whey protein powder and soybean milk on the quality of solidified sea buckthorn yogurt[J].Grain and Oil, 2024, 37 (8):90-93;99.
[11] WANG Y, ZHANG G Y.The preparation of modified nano-starch and its application in food industry[J].Food Research International, 2021, 140:110009.
[12] 李星仪, 路风银, 刘爱平, 等.热风干燥中相对湿度对不同厚度山药片的影响[J].河南农业科学, 2023, 52(10):162-171.
LI X Y, LU F Y, LIU A P, et al.Effect of relative humidity on different thicknesses of yam slices during hot air drying[J].Journal Henan Agricultural Sciences, 2023, 52(10):162-171.
[13] 劳艳艳. 基于羽衣甘蓝的蔬菜酸奶溶豆高效干燥制备及其特性研究[D].无锡:江南大学, 2020.
LAO Y Y.Efficient drying preparation and characteristics study of vegetable yogurt dissolved beans based on kale [D].Wuxi:Jiangnan University, 2020.
[14] LI M R, WANG B, WANG Y C, et al.Evaluation of the uniformity, quality and energy cost of four types of vegetables and fruits after pilot-scale pulse-spouted bed microwave (915 MHz) freeze-drying[J].Drying Technology, 2023, 41(2):290-307.
[15] BAO Y F, LIU W C, LI L L, et al.Improvement of 3D printing and subsequent microwave freeze-drying solidification accuracy of pineapple gel-based inks:Infill percentage control and internal models design[J].Journal of Food Engineering, 2025, 386:112286.
[16] 苗峻伟, 段续, 任广跃, 等.微波冻干预制面条干燥特性及品质特征研究[J].食品与发酵工业, 2024, 50(9):262-267.
MIAO J W, DUAN X, REN G Y, et al.Drying and quality characteristics of microwave freeze-dried pre-pared noodles[J].Food and Fermentation Industries, 2024, 50 (9):262-267.
[17] LONG Y Z, ZHANG M, MUJUMDAR A S, et al.Valorization of turmeric (Curcuma longa L.) rhizome:Effect of different drying methods on antioxidant capacity and physical properties[J].Drying Technology, 2022, 40(8):1609-1619.
[18] 陈红惠, 张鲁梅.不同干燥方式对山药品质的影响[J].食品工业, 2022, 41 (11):195-199.
CHEN H H, ZHANG L M.Effects of different drying methods on quality of Chinese yam[J].Food Industry, 2022, 41 (11):195-199.
[19] JIANG J H, ZHANG M, DEVAHASTIN S, et al.Effect of ultrasound-assisted osmotic dehydration pretreatments on drying and quality characteristics of pulsed fluidized bed microwave freeze-dried strawberries[J].LWT, 2021, 145:111300.
[20] THONGCHAROENPIPAT C, YAMSAENGSUNG R.Microwave-assisted vacuum frying of durian chips:Impact of ripening level on the drying rate, physio-chemical characteristics, and acceptability[J].Food and Bioproducts Processing, 2023, 138:40-52.
[21] LI C Y, REN G Y, ZHANG L D, et al.Effects of different drying methods on the drying characteristics and drying quality of Cistanche deserticola[J].LWT, 2023, 184:115000.