This paper investigated the effects of the most two commonly used microcapsule drying technology,spray drying and vacuum freeze drying,on the quality of peony seed oil microcapsules. The embedding rates of peony seed oil microcapsules prepared by spray drying and freeze drying methods were 88.12% and 76.55%,respectively. The moisture content,solubility and color were significantly different(P<0.05). Spray-dried microcapsules were spherical,smooth without wrinkles. And the particle size distributions followed a normal distribution and the average particle size was 2 563 nm. While,cold-dried microcapsules were irregular flakes with depressions and holes on the surface,and the particle size distribution didn't follow a normal distribution and the average particle size was 765.5 nm. From the FTIR curve,in the microcapsule products prepared by the two drying methods,the core material was covered by the wall material. Moreover,no significant difference in fatty acid composition of peony seed oil microcapsules prepared by two drying methods(P<0.05). The microencapsulation of peony seed oil was beneficial to maintain the thermal stability and oxidation stability of peony seeds oil,and high temperature above 200 ℃ could decompose the wall material. Furthermore,the oxidation stability of microcapsules prepared by spray drying method was better than that of cold drying method. In summary,spray drying is a better process condition for preparing peony seed oil microcapsules than freeze drying.
[1] 袁琴琴,刘文营. 牡丹籽中营养和功能性成分研究进展[J]. 食品工业科技,2019,40(17):333-339.
[2] 王顺利,任秀霞,薛璟祺,等. 牡丹籽油成分、功效及加工工艺的研究进展[J]. 中国粮油学报,2016,31(3):139-146.
[3] 毛善巧,李西俊. 牡丹籽油的研究进展及油用牡丹综合利用价值分析[J]. 中国油脂,2017,42(5):123-126.
[4] 周宇,晏敏,梅明鑫,等. 微胶囊技术在油脂工业中的研究进展[J]. 食品与发酵工业,2018,44(4):293-300.
[5] 王慧梅,范艳敏,王连艳. 基于微胶囊技术对油脂包埋的研究进展[J]. 现代食品科技,2018,34(10):271-280;195.
[6] 石燕,李如一,王辉,等. 月见草油微胶囊的制备及微观结构分析[J]. 食品科学,2014,35(21):5-9.
[7] 叶繁,彭茜,李思敏,等. 喷雾干燥与冷冻干燥对鱼油微胶囊品质的影响[J]. 渔业现代化,2019,46(3):73-82.
[8] 刘成祥. 牡丹籽油微胶囊的制备及其性质研究[D]. 无锡:江南大学,2016.
[9] 江连洲,王朝云,古力那孜·买买提努,等. 干燥工艺对鱼油微胶囊结构和品质特性的影响[J]. 食品科学,2020,41(3):86-92.
[10] 葛双双,李坤,涂行浩,等. 余甘子核仁油微胶囊的制备及其稳定性分析[J]. 食品科学,2018,39(20):253-259.
[11] 杨小斌,周爱梅,王爽,等. 蓝圆鲹鱼油微胶囊的结构表征与体外消化特性[J]. 食品科学,2019,40(1):117-122.
[12] TONON R V,GROSSO C R F,HUBINGER M D. Influence of emulsion composition and inlet air temperature on the microencapsulation of flaxseed oil by spray drying[J]. Food Research International,2011,44(1):282-289.
[13] 刘成祥,王力,苏建辉,等. 牡丹籽油微胶囊的制备及特性研究[J]. 中国油脂,2016,41(11):12-16.
[14] TATAR F,TUNÇ M T,DERVISOGLU M,et al.Evaluation of hemicellulose as a coating material with gum arabic for food microencapsulation[J]. Food Research International,2014,57:168-175.
[15] JAYASUNDERA M,ADHIKARI B,HOWES T,et al.Surface protein coverage and its implications on spray-drying of model sugar-rich foods: Solubility,powder production and characterisation[J]. Food Chemistry,2011,128(4):1 003-1 016.
[16] 王寒,罗庆华,魏梦雅,等. 大鲵油微胶囊的贮藏稳定性研究[J]. 中国油脂,2018,43(11):24-27;48.
[17] 陈琳,李荣,张禄捷,等. 复凝聚法紫苏油微胶囊的制备及其性能研究[J]. 食品工业科技,2015,36(3):232-238.
[18] 刘双双,那治国,徐飞,等. 壁材对香草兰精油微胶囊物性与释放特性的影响[J]. 食品科学,2019,40(3):129-134.
[19] 杨鹏,沈汪洋,刘零怡,等. 油茶籽油微胶囊的制备及其品质分析[J]. 粮食与油脂,2019,32(5):34-39.
[20] 彭莹芸,付复华,朱平平,等. 超声辅助制备葡萄柚精油纳米微胶囊及其表征[J]. 食品与机械,2019,35(5):208-212.
[21] 刘全亮,马传国,王化林,等. 微胶囊化棕榈油的品质分析[J]. 粮油食品科技,2015,23(1):38-42.
[22] 谢岩黎,朱晓路,王芬. 常用微胶囊壁材的分子结构及流变学特性研究[J]. 现代食品科技,2015,31(5):59-64;168.
[23] 夏慧亭. 复凝聚法制备橄榄油微胶囊及其性质研究[D]. 哈尔滨:东北农业大学,2016.
[24] 葛双双,李坤,涂行浩,等. 余甘子核仁油微胶囊的制备及其稳定性分析[J]. 食品科学,2018,39(20):253-259.
[25] 叶繁,彭茜,李思敏,等. 喷雾干燥与冷冻干燥对鱼油微胶囊品质的影响[J]. 渔业现代化,2019,46(3):73-82.
[26] 艾文婷,张敏,黄汝国,等. 热分析技术在食品热物性研究中的应用[J]. 食品工业科技,2016,37(19):377-380;386.
[27] 范方宇,常艳琼,董选刚,等. 茶油微胶囊的性质[J]. 食品与发酵工业,2014,40(7):106-110.
[28] 伍亚华,石亚中,钱时权. 怀远石榴籽油微胶囊的制备及稳定性研究[J]. 中国油脂,2017,42(5):23-27.
[29] DRUSCH S,SCHWARZ K.Microencapsulation properties of two different types of n-octenylsuccinate-derivatised starch[J]. European Food Research and Technology,2006,222(1-2):155-164.