Effect of different cleaning methods combined with grinding oil treatment on removing pesticide residues in whole navel orange

  • SHU Nan ,
  • FU Fuhua ,
  • LI Gaoyang ,
  • SHAN Yang ,
  • LI Tao ,
  • LUO Binbin ,
  • ZHU Xiangrong ,
  • LI Qili ,
  • ZHANG Qun
Expand
  • 1(Longping Branch,Graduate School of Hunan University,Changsha 410125,China)
    2(Hunan Agricultural Product Processing Institute,Hunan Academy of Agricultural Sciences,Changsha 410125,China)
    3(Hunan Key Laboratory of Fruits & Vegetables Storage,Processing,Quality and Safety,Changsha 410125,China)
    4(Hunan Province International Joint Lab on Fruits & Vegetables Processing,Quality and Safety,Changsha 410125,China)
    5(Changde Agriculture and Forestry Sciences Academy of Hunan Province,Changde 415000,China)

Received date: 2020-10-29

  Revised date: 2020-12-18

  Online published: 2021-08-02

Abstract

The effects of different cleaning methods combined with grinding oil treatment on the removal of pesticide residues from whole navel orange were investigated. Changes of five pesticide residues (bifenthrin, 2,4-Dichlorophenoxyacetic acid, prochloraz, spiromethrin, and amiphos) from whole navel orange by five different cleaning methods (immersing with clean water, rinsing with running water, cleaning with ultrasonic, immersing with hot water and cleaning with ozone water) were studied under laboratory conditions. The results showed that these cleaning methods all could remove pesticide residues with varying degrees in whole navel orange samples. The processing factors of each pesticide varied in the range of (0.298 9±0.032 0)-(0.899 6±0.034 5). Ozone water cleaning had a better removal effect on pesticides among them. After five cleaning methods combined with grinding oil treatment, pesticide residues on whole navel orange samples were significantly removed. The processing factors were (0.000 8±0.001 5)-(0.232 8±0.010 7), only 0.10%-27.19% of the whole navel orange with no grinding oil. Ozone water combined with grinding oil was proved to be the most effective pesticide removal method. The research results provide a reference for the quality and safety control of the subsequent processing of whole navel orange products.

Cite this article

SHU Nan , FU Fuhua , LI Gaoyang , SHAN Yang , LI Tao , LUO Binbin , ZHU Xiangrong , LI Qili , ZHANG Qun . Effect of different cleaning methods combined with grinding oil treatment on removing pesticide residues in whole navel orange[J]. Food and Fermentation Industries, 2021 , 47(13) : 232 -239 . DOI: 10.13995/j.cnki.11-1802/ts.026033

References

[1] 吴雪莹, 屈立武,周雅涵,等.壳聚糖和纳米SiOx处理对采后脐橙果实硬度的影响[J].食品科学,2015,36(2):204-209.
WU X Y,QU L W,ZHOU Y H,et al.Effects of chitosan and SiOx treatments on firmness of postharvest Navel Orange fruits[J].Food Science,2015,36(2):204-209.
[2] 李绮丽, 孙俊杰,单杨,等.不同柑橘品种全果制汁适宜性分析[J].食品科学,2019,40(13):36-44.
LI Q L,SUN J J,SHAN Y,et al.Suitability evaluation of different citrus varieties for whole fruit juice processing[J].Food Science,2019,40(13):36-44.
[3] 郑巧, 张桂伟,郑惠文,等.制粒对柑橘全果果粉酚类物质及抗氧化活性的影响[J].食品科学,2015,36(23):136-142.
ZHENG Q,ZHANG G W,ZHENG H W,et al.Effect of granulation on phenolic compounds and antioxidant activity of whole citrus fruit powder[J].Food Science,2015,36(23):136-142.
[4] 郑淑丹,陈钢,阙发秀,等.脐橙全果酒发酵工艺优化及其与脐橙果汁酒风味物质的对比分析[J].食品科学,2019,40(10):171-177.
ZHENG S D,CHEN G,QUE F X,et al.Optimization of fermentation process for whole navel orange wine and comparative analysis of flavor components with navel orange juice wine[J].Food Science,2019,40(10):171-177.
[5] 沈兆敏,张弩,秦光成.脐橙优质丰产技术[M].第2版.北京:金盾出版社,2011.
SHEN Z M,ZHANG N,QIN G C.High quality and yield technology of navel orange[M].2rd ed.Beijing:Jindun Publisher,2011.
[6] CALVARUSO E,CAMMILLERI G,PULVIRENTI A,et al.Residues of 165 pesticides in citrus fruits using LC-MS/MS:A study of the pesticides distribution from the peel to the pulp[J].Natural Product Research,2020,34(1):34-38.
[7] YI T,HU D J,YAN G,et al.Investigation and analysis of pesticide residues in citrus from parts of Hubei province[J].Agricultural Science & Technology,2017,18(4):680-682.
[8] POLAT B,TIRYAKI O.Assessing washing methods for reduction of pesticide residues in Capia pepper with LC-MS/MS[J].Journal of Environmental Science & Health,2020,55(1):1-10.
[9] SOWIK-BOROWIEC M,SZPYRKA E.Selected food processing techniques as a factor for pesticide residue removal in apple fruit[J].Environmental Science and Pollution Research,2020,27(2):2 361-2 373.
[10] 刘淑敏, 唐兰兰,陈智玲,等.湛江四种市售蔬菜农药残留的监测分析及洗涤方法对农残的影响[J].现代食品科技,2020,36(1):275-280;15.
LIU S M,TANG L L,CHEN Z L,et al.Monitoring analysis in four varieties of vegetables from Zhanjiang and their effects of washing methods on the content of pesticide residues[J].Modern Food Science and Technology,2020,36(1):275-280;15.
[11] WANG S,WANG J Y,LI C,et al.Ozone treatment pak choi for the removal of malathion and carbosulfan pesticide residues[J].Food Chemistry,2021,337:127 755.
[12] RODRIGUES A A Z,DE QUEIROZ M E L R,DE OLIVEIRA A F,et al.Pesticide residue removal in classic domestic processing of tomato and its effects on product quality[J].Journal of Environmental Science and Health,2017,52(12):850-857.
[13] WANWIMOLRUK C,PHOPIN K,WANWIMOLRUK S.Food safety in Thailand 6:How to eat guava fruits safely? Effects of washing and peeling on removing pesticide residues in guava fruits[J].Journal of Food Safety,2019,39(4):e12 654.
[14] HAN Y T,YANG J,SONG L,et al.Residue change of six pesticides in Chinese liquor produced from sorghum[J].International Journal of Food Properties,2017,20(Supl):S755-S765.
[15] YIGIT N,VELIOGLU Y S.Effects of processing and storage on pesticide residues in foods[J].Critical Reviews in Food Science and Nutrition,2020,60(21):3 622-3 641.
[16] NIAHIJIMA W,OKUDA T,NAKAI S,et al.A green procedure using ozone for Cleaning-in-Place in the beverage industry[J].Chemosphere,2014,105(4):106-111
[17] 中华人民共和国卫生部.GB/T 5009.218—2008 水果和蔬菜中多种农药残留量的测定[S].北京:中国标准出版社,2008.
Ministry of Health of the People’s Republic of China.GB/T 5009.218—2008 Determination of multiple pesticide residues in fruits and vegetables[S].Beijing:China Standard Press,2008.
[18] LARA-ORTEGA F J,ROBLES-MOLINA J,BRANDT S,et al.Use of dielectric barrier discharge ionization to minimize matrix effects and expand coverage in pesticide residue analysis by liquid chromatography-mass spectrometry[J].Analytica Chimica Acta,2018,1 020:76-85.
[19] 杨绿竹, 王馨雨,王蓉蓉,等.柑橘果皮角质层及其对采后贮藏保鲜影响的研究进展[J].食品科学,2020,41(7):234-244.
YANG L Z,WANG X Y,WNAG R R,et al.Progress in the knowledge of the cuticle of citrus fruit and its effect on the postharvest fruit quality during storage[J].Food Science,2020,41(7):234-244.
[20] HOU J X,LIANG L,WANG Y X.Volatile composition changes in navel orange at different growth stages by HS-SPME-GC-MS[J].Food Research International,2020,136:109 333.
[21] 高兴. 金柑果皮油胞特性和相关调控基因表达量的研究[D].南宁:广西大学,2016.
GAO X.Study on the characteristics of kumquat peel oil cells and the expression of related regulatory genes[D].Nanning:Guangxi University,2016.
[22] 李云成, 张耀海,陈卫军,等.橙汁加工过程对农药炔螨特残留的影响[J].农业工程学报,2012,28(9):270-275.
LI Y C,ZHANG Y H,CHEN W J,et al.Effects of processing techniques on propargite residues in orange juice and its by-products[J].Transactions of the Chinese Society of Agricultural Engineering,2012,28(9):270-275.
[23] 魏梅. 七种高检出农药在柑橘中的稳定性研究[D].重庆:西南大学,2016.
WEI M.Study on the stability of seven highly detected pesticides in Citrus[D].Chongqing:Southwest University,2016
[24] LOZOWICKA B,JANKOWSKA M,HRYNKO I,et al.Removal of 16 pesticide residues from strawberries by washing with tap and ozone water,ultrasonic cleaning and boiling[J].Environmental Monitoring & Assessment,2016,188(1):51-69.
[25] ZHU Y C,ZHANG T,XU D X,et al.The removal of pesticide residues from pakchoi (Brassica rape L.ssp.chinensis) by ultrasonic treatment[J].Food Control,2019,95:176-180.
[26] 马静, 付颖,叶非.超声波诱导降解消除农药残留的研究进展[J].东北农业大学学报,2009,40(5):140-144.
MA J,FU Y,YE F.Research advance in induced degradation of pesticide residues by ultrasonic irradiation[J].Journal of Northeast Agricultural University,2009,40(5):140-144.
[27] 刘伟森, 朱珍,张兴茂,等.清洗方法对蔬菜中有机磷农药残留去除效果的研究[J].现代食品科技,2010,26(12):1 395-1 398.
LIU W S,ZHU Z,ZHANG X M,et al.Study on removing organophosphorus pesticide residues from vegetable with four rinsing method[J].Modern Food Science and Technology,2010,26(12):1 395-1 398.
[28] FARHA W,EL-ATY A A,RAHMAN M M,et al.Analytical approach,dissipation pattern and risk assessment of pesticide residue in green leafy vegetables:A comprehensive review[J].Biomedical Chromatography,2018,32(1):e4 134.
[29] RANI M,SAINI S,KUMARI B.Persistence and effect of processing on chlorpyriphos residues in tomato (Lycopersicon esculantum Mill.)[J].Ecotoxicology & Environmental Safety,2013,95:247-252.
[30] 王明明, 龚艳,陈浩,等.吡虫啉在番茄中的残留动态及残留去除方法[J].食品科学,2010,31(19):133-136.
WANG M M,GONG Y,CHEN H,et al.Residual dynamics of imidacloprid in tomatoes and comparative analysis of commonly used methods for the removal of residual imidacloprid[J].Food Science,2010,31(19):133-136.
[31] 范珺.黄瓜中霜脲氰和喹啉铜动态残留的研究[D].泰安:山东农业大学,2014.
FAN J.Study on dynamic residues of cymoxanil and copper quinoline in cucumber[D].Tai’an:Shandong Agricultural University,2014.
[32] PANDISELVAM R,KAAVYA R,JAYANATH Y,et al.Ozone as a novel emerging technology for the dissipation of pesticide residues in foods-a review[J].Trends in Food Science & Technology,2020,97:38-54.
[33] De ÁVilA M B R,FARONI L R A,HELENO F F,et al.Ozone as degradation agent of pesticide residues in stored rice grains[J].Journal of Food Science & Technology,2017,54(12):1-8.
[34] 蒋红英. 娃娃菜农残消降组合方法及对品质的影响[J].食品与发酵工业,2011,37(4):92-96.
JIANG H Y.Study on combination degradation of pesticides residual and evaluation of the quality variation in baby cabbage[J].Food and Fermentation Industries,2011,37(4):92-96.
[35] 管文辰. 烹调对小白菜中两种杀菌剂残留变化的影响及其膳食暴露评估[D].南京:南京农业大学,2014.
GUAN W C.Effects of cooking on the changes of two fungicide residues in Chinese cabbage and its dietary exposure assessment[D].Nanjing:Nanjing Agricultural College,2014.
[36] 刘英, 王新全,汤涛,等.不同清洗方法对芹菜中吡虫啉残留的去除效果[J].农药学学报,2019,21(4):492-499.
LIU Y,WANG X Q,TANG T et al.Removal effect of imidacloprid residue in celery by different washing method[J].Chinese Journal of Pesticide Science,2019,21(4):492-499.
Outlines

/