Food and Fermentation Industries >

2022 , Vol. 48 >Issue 7: 231 - 237

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.027811

Effect of different preparation conditions on green synthesis of silver nanoparticles

  • XING Yage ,
  • LIAO Xingmei ,
  • LI Wenxiu ,
  • TANG Jing ,
  • XU Qinglian ,
  • LI Xuanlin ,
  • HUANG Ruihan ,
  • YU Jinze
Expand
  • 1(School of Food and Bioengineering,Xihua University,Chengdu 611743,China)
    2(Key Laboratory of Food Non Thermal Technology,Research Institute of Xihua University,Yibin 644000,China)
    3(Department of Agricultural Technology,Neijiang Vocational & Technical College,Neijiang 641000,China)
    4(National Engineering Technology Research Center for Preservation of Agricultural Products,Key Laboratory of Storage of Agricultural Products,Ministry of Agriculture and Rural Affairs,Tianjin Key Laboratory of Postharvest Physiology and Storage of Agricultural Products,Tianjin 300384,China)

Received date: 2021-04-20

  Revised date: 2021-05-13

  Online published: 2022-04-27

Fold

Abstract

With the development of fresh-keeping technology for fruits and vegetables, the use of nano-silver for single or compound coating fresh-keeping technology has become increasingly obvious in the application of fresh-keeping technology for fruits and vegetables. Silver nanoparticles were prepared by biological reduction method with silver nitrate as the source of silver and mango peel extract as reducing agent. The effects of reaction time, reaction temperature, mango peel extract concentration, silver nitrate concentration and powdered sodium dodecyl sulfate (SDS) addition amount on the color, UV visible absorption and particle size of nano-Ag sol were analyzed by Malvern laser particle size analyzer and enzyme-labeled instrument. And then the physical and chemical properties of silver nanoparticles were also analyzed with transmission electron microscopy and Fourier transform infrared spectroscopy. The results showed that the color, yield and size of the synthesized silver nanoparticles could be controlled by changing the reaction temperature, time and amount of addition in a certain range. The size of the silver nanoparticles was between 25 nm and 70 nm, and the distribution was uniform. According to the influence of various factors on the preparation of silver nanoparticles, the optimum conditions were determined as: reaction was performed at 75 ℃ for 1 h with the concentration of the mango peel extract 0.20 g/mL, silver nitrate concentration 2.0 mmol/L and the addition of 0.15 g SDS. This study provides a theoretical and practical basis for green preparation of high-performance silver nanoparticles and the development of more nanoparticles composite preservation technology.

Key words： mango peel; bioreduction; green synthesis; silver nanoparticles; nanometer materials

Cite this article

XING Yage , LIAO Xingmei , LI Wenxiu , TANG Jing , XU Qinglian , LI Xuanlin , HUANG Ruihan , YU Jinze . Effect of different preparation conditions on green synthesis of silver nanoparticles[J]. Food and Fermentation Industries, 2022 , 48(7) : 231 -237 . DOI: 10.13995/j.cnki.11-1802/ts.027811

References

[1] 王馨,胡文忠,陈晨,等.纳米材料在果蔬保鲜中的应用[J].食品与发酵工业,2017,43(1):281-286.
WANG X,HU W Z,CHEN C,et al.Application of nanomaterials in storage of fruits and vegetables[J].Food and Fermentation Industries,2017,43(1):281-286.
[2] 刘小莉,图尔荪阿依,图尔贡,等.纳米银对革兰氏阴性水产品腐败菌的抑制作用[J].中国食品学报,2019,19(11):186-190.
LIU X L,TURS A Y,TUR G,et al.Inhibitory activity of silver nanoparticles against gram-negative bacteria in spoiled fishes[J].Journal of Chinese Institute of Food Science and Technology,2019,19(11):186-190.
[3] 高雪.纳米银的制备及其对羊毛织物的整理[D].天津:天津工业大学,2020.
GAO X.Preparation of nano silver and its finishing of wool fabric[D].Tianjin:Tianjin Polytechnic University,2020.
[4] ALKHULAIFI M M,ALSHEHRI J H,ALWEHAIBI M A,et al.Green synthesis of silver nanoparticles using Citrus limon peels and evaluation of their antibacterial and cytotoxic properties[J].Saudi Journal of Biological Sciences,2020,27(12):3 434-3 441.
[5] 杨斌,曹银娟,余群力,等.纳米银酯化淀粉膜对牛肉保鲜的影响[J].食品科学,2019,40(23):199-205.
YANG B,CAO Y J,YU Q L,et al.Application of nanosilver esterified starch film in beef preservation[J].Food Science,2019,40(23):199-205.
[6] 龙娅,胡文忠,萨仁高娃,等.鲜切果蔬精准保鲜包装技术的研究进展[J].食品与发酵工业,2019,45(12):249-256.
LONG Y,HU W Z,SAREN G W,et al.Precise fresh-keeping packaging for fresh-cut fruits and vegetables[J].Food and Fermentation Industries,2019,45(12):249-256.
[7] 吴宗山,李莉.天然产物绿色合成小尺寸纳米银及抗菌性[J].精细化工,2014,31(8):964-968;973.
WU Z S,LI L.Green synthesis of small size silver nanoparticles by nature product and their antimicrobial properties[J].Fine Chemicals,2014,31(8):964-968;973.
[8] 陶晶,付争伟,董春法,等.芦荟叶提取物绿色制备单分散纳米金及其性能(英文)[J].稀有金属材料与工程,2019,48(11):3 470-3 475.
TAO J,FU Z W,DONG C F,et al.Green synthesis and characterization of monodisperse gold nanoparticles using aloe vera leaf extract[J].Rare Metal Materials and Engineering,2019,48(11):3 470-3 475.
[9] NILUXSSHUN M C D,MASILAMANI K,MATHIVENTHAN U,et al.Green synthesis of silver nanoparticles from the extracts of fruit peel of Citrus tangerina,Citrus sinensis,and Citrus limon for antibacterial activities[J].Bioinorganic Chemistry and Applications,2021.DOI:10.1155/2021/6695734.
[10] 彭红,刘洋,袁林,等.银纳米粒子材料制备研究进展[J].现代化工,2017,37(7):23-28.
PENG H,LIU Y,YUAN L,et al.Progress in preparation of silver nanoparticle materials[J].Modern Chemical Industry,2017,37(7):23-28.
[11] 朱雨婕,代安然,李佳铭,等.金针菇无细胞滤液合成纳米银颗粒[J].食品与发酵工业,2021,47(5):71-78.
ZHU Y J,DAI A R,LI J M,et al.Synthesis of silver nanoparticles using cell-free filtrate of Flammulina velutipes[J].Food and Fermentation Industries,2021,47(5):71-78.
[12] 杨宁,郝林,杨鹏.芒果皮提取物合成纳米银及抑菌性研究[J].山西农业大学学报(自然科学版),2013,33(1):59-65.
YANG N,HAO L,YANG P.Mango peel extract mediated novel route for synthesis of silver nanoparticles and antibacterial application of silver nanoparticles[J].Journal of Shanxi Agricultural University(Natural Science Edition),2013,33(1):59-65.
[13] 付锐平,董春法,郭小燕,等.桔子皮提取液绿色可控制备单分散纳米银的研究[J].电子元件与材料,2021,40(1):30-35.
FU R P,DONG C F,GUO X Y,et al.Green and controllable synthesis of monodisperse silver nanoparticles by using orange peel extract[J].Electronic Components and Materials,2021,40(1):30-35.
[14] 张青山,岳秀萍.纳米银粒子的生物制备及应用研究进展[J].材料导报,2014,28(1):53-58.
ZHANG Q S,YUE X P.Research progress of biological preparation and application of silver nanoparticles[J].Materials Review,2014,28(1):53-58.
[15] 曹雪玲,陆书来,张东杰,等.纳米银作为抗菌剂的抗菌性能研究[J].吉林化工学院学报,2017,34(11):30-34.
CAO X L,LU S L,ZHANG D J,et al.Study on antimicrobial activity of nano silver as antimicrobial agents[J].Journal of Jilin Institute of Chemical Technology,2017,34(11):30-34.
[16] 姚平,邢铁玲,陈国强.杜仲纳米银的制备及其对直接橙26的催化还原降解[J].纺织学报,2018,39(1):104-110.
YAO P,XING T L,CHEN G Q.Biosynthesis of Eucommia ulmoides silver nanoparticles and application thereof in reductive catalytic degradation of Direct Orange 26[J].Journal of Textile Research,2018,39(1):104-110.
[17] 刘冲冲,王磊,徐慧,等.姜提取物生物合成纳米银抑菌活性的研究[J].食品与生物技术学报,2017,36(6):590-597.
LIU C C,WANG L,XU H,et al.Antibacterial study of silver nanoparticles biosynthesized with ginger extract[J].Journal of Food Science and Biotechnology,2017,36(6):590-597.
[18] 薛海燕,张颖,张宝艳,等.安石榴苷还原壳聚糖/纳米银溶胶制备表征及其抑菌性能[J].农业工程学报,2018,34(4):306-314.
XUE H Y,ZHANG Y,ZHANG B Y,et al.Preparation characterization and bacteriostatic properties of punicalagin reducing chitosan/nano silver Sol[J].Transactions of the Chinese Society of Agricultural Engineering,2018,34(4):306-314.
[19] 吴宗山.纳米银的可控制备及其抗菌性研究[D].北京:北京林业大学,2015.
WU Z S.Controllable preparation of silver nanoparticles and its antibacterial property[D].Beijing:Beijing Forestry University,2015.
[20] SONG J Y,KIM B S.Rapid biological synthesis of silver nanoparticles using plant leaf extracts[J].Bioprocess and Biosystems Engineering,2009,32(1):79-84.
[21] 司友琳,张胜义,闵宏林.Ag/TiO2纳米复合物的模板法制备及其性质研究[J].硅酸盐通报,2010,29(1):72-76.
SI Y L,ZHANG S Y,MIN H L.Preparation and characterization of silver deposited nano-TiO2 through the chitosan template method[J].Bulletin of the Chinese Ceramic Society,2010,29(1):72-76.
[22] 秦聪丽,傅吉全.桑叶提取物还原制备钯纳米颗粒[J].贵金属,2016,37(3):29-32.
QIN C L,FU J Q.Preparation of palladium nanoparticles using mulberry leaf extract[J].Precious Metals,2016,37(3):29-32.
Options
Outlines

/

〈 〉

Powered by Beijing Magtech Co. Ltd,.