Changes of volatile flavor components during brewing of pomegranate wine based on GC-IMS

  • ZHANG Busheng ,
  • GAO Xing ,
  • YAN Xin ,
  • CUI Danyao ,
  • LYU Xiaotong ,
  • LIN Liangcai ,
  • ZHANG Cuiying
Expand
  • 1(Key Laboratory of Industrial Fermentation Microbiology,Ministry of Education,Tianjin University of Science and Technology,Tianjin 300457,China)
    2(College of Bioengineering,Tianjin University of Science and Technology,Tianjin 300457,China)

Received date: 2021-06-23

  Revised date: 2021-07-23

  Online published: 2022-04-27

Abstract

The migration and change law of volatile flavor components of Daqingpi pomegranate wine were analyzed by GC-IMS technology, principal component anaglysis (PCA) and fingerprint similarity analysis. The results showed that 36 kinds of compounds were identified. The aldehyde components such as heptanaldehyde, nonanal and hexanal disappeared, and the content of ethyl acetate, ethanol, 3-methyl-1-butanol and 2-methyl-1-propanol were significantly increased after fermentation. The volatile substances of pomegranate wine fermented for 20 days or one year were basically same, in which isobutyl acetate, isoamyl acetate and butyl acetate decreased, and the content of ethyl butyrate and ethyl caproate were significantly increased with aging. It indicated that the flavor components of pomegranate wine were mainly produced during alcoholic fermentation. The results provide a scientific basis for the improvement of the brewing process of pomegranate fruit wine.

Cite this article

ZHANG Busheng , GAO Xing , YAN Xin , CUI Danyao , LYU Xiaotong , LIN Liangcai , ZHANG Cuiying . Changes of volatile flavor components during brewing of pomegranate wine based on GC-IMS[J]. Food and Fermentation Industries, 2022 , 48(7) : 252 -257 . DOI: 10.13995/j.cnki.11-1802/ts.028433

References

[1] 林雨晴,秦丹.石榴果酒营养成分及加工工艺进展[J].农产品加工,2018(13):44-46.
LIN Y Q,QIN D.Research progress in nutrient ingredients and processing technology of pomegranate wine[J].Farm Products Processing,2018(13):44-46.
[2] MENA P,GIRONÉS-VILAPLANA A,MARTÍ N,et al.Pomegranate varietal wines:Phytochemical composition and quality parameters[J].Food Chemistry,2012,133(1):108-115.
[3] 杨彬彬.我国石榴浓缩汁的产业现状及发展趋势[J].陕西农业科学,2009,55(1):94-96.
YANG B B.The current situation and development trend of our country's pomegranate juice concentrate[J].Shaanxi Journal of Agricultural Sciences,2009,55(1):94-96.
[4] FERRARA G,CAVOSKI I,PACIFICO A,et al.Morpho-pomological and chemical characterization of pomegranate(Punica granatum L.) genotypes in Apulia region,Southeastern Italy[J].Scientia Horticulturae,2011,130(3):599-606.
[5] MENA P,GIRONES-VILAPLANA A,MORENO D A,et al.Phenolic composition of pomegranate wines.Influence of variety and winemaking stage[C]//5th International Conference on Polyphenols and Health(ICPH).Sitges(Spain).2011.
[6] ANDREU-SEVILLA A J,MENA P,MARTI N,et al.Volatile composition and descriptive sensory analysis of pomegranate juice and wine[J].Food Research International,2013,54(1):246-254.
[7] 兰永丽.石榴酒及石榴乳酸饮料发酵工艺优化及其风味和抗氧化性研究[D].杨凌:西北农林科技大学,2017.
LAN Y L.Study on fermentation process and flavor and antioxidant quality of pomegranate wine and pomegranate lactic acid drink[D].Yangling,China:Northwest A & F University,2017.
[8] 姚文生,蔡莹暄,刘登勇,等.不同材料熏制鸡腿肉挥发性物质GC-IMS指纹图谱分析[J].北京工商大学学报(自然科学版),2019,37(6):37-45.
YAO W S,CAI Y X,LIU D Y,et al.GC-IMS fingerprint analysis of volatile substances in chicken thighs smoked from different materials[J].Journal of Food Science and Technology,2019,37(6):37-45.
[9] COHEN M J,KARASEK F W.Plasma chromatographyTM—A new dimension for gas chromatography and mass spectrometry[J].Journal of Chromatographic Science,1970,8(6):330-337.
[10] 周晨曦,郑福平,孙宝国.离子迁移谱技术在食品风味分析中的应用研究进展[J].食品工业科技,2019,40(18):309-318.
ZHOU C X,ZHENG F P,SUN B G.Research progress on the application of ion mobility spectrometry(IMS) in food flavor analysis[J].Science and Technology of Food Industry,2019,40(18):309-318.
[11] 陈东杰,张明岗,聂小宝,等.基于气相离子迁移谱检测静电场处理的大菱鲆品质[J].食品科学,2019,40(24):313-319.
CHEN D J,ZHANG M G,NIE X B,et al.Quality detection of turbot(Scophtalmus maximus) treated with electrostatic field using gas chromatography-ion mobility spectrometry[J].Food Science,2019,40(24):313-319.
[12] GARRIDO-DELGADO R,DOBAO-PRIETO M D M,ARCE L,et al.Determination of volatile compounds by GC-IMS to assign the quality of virgin olive oil[J].Food Chemistry,2015,187:572-579.
[13] 唐柯,王茜,周霞,等.石榴酒发酵过程中香气动态变化规律[J].食品与发酵工业,2019,45(6):197-202;214.
TANG K,WANG X,ZHOU X,et al.Dynamic changes in aroma during pomegranate wine fermentation[J].Food and Fermentation Industries,2019,45(6):197-202;214.
[14] 彭潇,邹文静,邵清清,等.石榴酒发酵过程中真菌种群演替及风味物质代谢规律解析[J].食品科学,2021,42(6):157-163.
PENG X,ZOU W J,SHAO Q Q,et al.Fungal community succession and flavor compounds metabolism during pomegranate wine fermentation[J].Food Science,2021,42(6):157-163.
[15] LI S Y,YANG H F,TIAN H H,et al.Correlation analysis of the age of brandy and volatiles in brandy by gas chromatography-mass spectrometry and gas chromatography-ion mobility spectrometry[J].Microchemical Journal,2020,157:104948.
[16] 李美萍,苗潇潇,张生万.HS-SPME-GC-MS分析石榴酒中易挥发性成分[J].食品科学,2014,35(8):263-268.
LI M P,MIAO X X,ZHANG S W.Analysis of volatile compounds in pomegranate wine by headspace solid phase micro-extraction and gas chromatography-mass spectrometry[J].Food Science,2014,35(8):263-268.
[17] JIN G Y,ZHU Y,XU Y.Mystery behind Chinese liquor fermentation[J].Trends in Food Science & Technology,2017,63:18-28.
[18] 王磊.GC-MS、GC-O和感官鉴定对六种白兰地挥发性成分和香气成分差异研究[D].烟台:烟台大学,2010.
WANG L.Difference of volatile compounds and aroma compounds in six brandies by GC-MS,GC-O and sensory evaluation[D].Yantai,China:Yantai University,2010.
[19] 张宝香,舒楠,金宇宁,等.不同果胶酶处理北冰红冰葡萄汁酿制北冰红冰酒香气成分分析[J].酿酒科技,2020(12):38-43.
ZHANG B X,SHU N,JIN Y N,et al.Analysis of aroma components of Beibing red ice wine brewed from Beibing red ice grape juice with different pectinase[J].Liquor-Making Science & Technology,2020(12):38-43.
[20] WANG N,CHEN S,ZHOU Z M.Characterization of volatile organic compounds as potential aging markers in Chinese rice wine using multivariable statistics[J].Journal of the Science of Food and Agriculture,2019,99(14):6 444-6 454.
[21] 杨颖迪,李闽,彭帮柱.苹果酒香气成分代谢研究进展[J].食品工业科技,2018,39(19):314-320.
YANG Y D,LI M,PENG B Z.Research on the metabolism of aroma components in apple cider[J].Science and Technology of Food Industry,2018,39(19):314-320.
Outlines

/