The effects of extrusion temperature on the physicochemical properties and in vitro digestibility of yam flour were studied by using the same direction twin-screw extruder. The flour was extruded under the conditions of different temperatures (90, 100, 110, and 130 ℃) with a screw speed of 180 r/min and the feed moisture of 30%. The results showed that the crystallinity of yam flour decreased with the increase of extrusion temperature, and the crystal structure changed. After extrusion, the solubility of the flour was increased, while the expansion degree and the gelatinization enthalpy decreased. With the increase of extrusion temperature, the highest solubility and the lowest expansion degree and gelatinization enthalpy were obtained at 130 ℃. The dynamic rheology of yam flour showed weak gel properties. In the range of frequency scanning, the energy storage modulus (G') and loss modulus (G″) of yam flour decreased with the increasing of temperature. The results of in vitro starch digestion showed that the content of starch with slow digestion properties increased and the content of resistant starch decreased. Meanwhile, the overall digestibility increased after extrusion, and the content of slowly digested starch increased with the increase of temperature. Therefore, when the extrusion temperature was 130 ℃, the flour was stable and not easy to gelatinization. It had a good water-soluble and the content of slowly digested starch was higher than that of untreated flour. The extrusion process could improve the functional properties and quality of the food by affecting the structure and in vitro digestibility of the flour.
[1] 王盼, 汪丽萍, 田晓红, 等.挤压加工与淀粉理化性质关系的研究进展[J].粮油食品科技, 2016, 24(6):13-17.
WANG P, WANG L P, TIAN X H, et al. Research progress on the influence of extrusion processing on the physicochemical properties of starch[J]. Science and Technology of Cereals, Oils and Foods, 2016, 24(6):13-17.
[2] ALI S, SINGH B, SHARMA S.Impact of feed moisture on microstructure, crystallinity, pasting, physico-functional properties and in vitro digestibility of twin-screw extruded corn and potato starches [J].Plant Foods for Human Nutrition(Dordrecht,Netherlands), 2019, 74(4):474-480.
[3] QI M M, ZHANG G Y, REN Z S, et al.Impact of extrusion temperature on in vitro digestibility and pasting properties of pea flour [J].Plant Foods for Human Nutrition(Dordrecht,Netherlands), 2021,76(1):26-30.
[4] ZHANG H, MENG Y J, LIU X L, et al.Effect of extruded mung bean flour on dough rheology and quality of Chinese noodles[J].Cereal Chemistry, 2019, 96(5):836-846.
[5] 王超. 挤压条件对豌豆粉及其主要组分加工特性的影响研究[D].天津:天津商业大学, 2019.
WANG C.Effect of extrusion conditions on processing properties of pea flour and its main components [D].Tianjin:Tianjin University of Commerce, 2019.
[6] JIANG Q Q, GAO W Y, SHI Y P.et al.Physicochemical properties and in vitro digestion of starches from different Dioscorea plants [J].Food Hydrocolloids, 2013,32(2):432-439.
[7] 戚明明, 任志尚, 张光耀, 等.挤压处理对豌豆淀粉的流变特性和体外淀粉消化率的影响(英文)[J].食品科学, 2021,42(9):55-63.
QI M M, REN Z S, ZHANG G Y, et al.Effect of extrusion treatment on rheological properties and in vitro starch digestibility of pea starch[J].Food Science, 2021,42(9):55-63.
[8] ENGLYST H N, KINGMAN S M, CUMMINGS J H.Classification and measurement of nutritionally important starch fractions[J].European Journal of Clinical Nutrition, 1992, 46(Suppl2):S33-S50.
[9] ALI S, SINGH B, SHARMA S.Effect of processing temperature on morphology, crystallinity, functional properties, and in vitro digestibility of extruded corn and potato starches [J].Journal of Food Processing and Preservation, 2020,44(7):e14531.
[10] 贾祥泽, 陈秉彦, 赵蓓蓓, 等.直链淀粉-脂质复合物的形成及其结构性质研究进展[J].食品与发酵工业, 2017, 43(3):276-284.
JIA X Z, CHEN B Y, ZHAO B B, et al.Research advance in the formation and structural properties of amylose-lipid complex [J].Food and Fermentation Industries, 2017, 43(3):276-284.
[11] BIDZIN'SKA E, MICHALEC M, PAWCENIS D.Effect of thermal treatment on potato starch evidenced by EPR, XRD and molecular weight distribution [J].Magnetic Resonance in Chemistry, 2015, 53(12):1 051-1 056.
[12] YANG Q Y, YANG Y, LUO Z G, et al.Effects of lecithin addition on the properties of extruded maize starch [J].Journal of Food Processing and Preservation, 2016, 40(1):20-28.
[13] 杨晓惠. 木薯淀粉的理化性质及其抗性淀粉制备工艺研究[D].广州:暨南大学, 2011.
YANG X H.Physicochemical properties of cassava starch and preparation of cassava resistant starch [D].Guangzhou:Jinan University, 2011.
[14] JAYAKODY L, LAN H, HOOVER R, et al.Composition, molecular structure, and physicochemical properties of starches from two grass pea (Lathyrus sativus L.) cultivars grown in Canada [J].Food Chemistry, 2007, 105(1):116-125.
[15] GANDHI N, SINGH B, SINGH P, et al.Functional, rheological, morphological, and micro-Structural properties of extrusion-processed corn and potato starches [J].Starch-Stärke, 2021, 73(1-2):2000140.
[16] ALI S, SINGH B, SHARMA S.Development of high-quality weaning food based on maize and chickpea by twin-screw extrusion process for low-income populations [J].Journal of Food Process Engineering, 2017, 40(3):e12500.
[17] JOSHI S M R, BERA M B, PANESAR P S.Extrusion cooking of maize/Spirulina mixture:Factors affecting expanded product characteristics and sensory quality[J].Journal of Food Processing and Preservation, 2014, 38(2), 655-664.
[18] SINGH B, RACHNA, HUSSAIN S Z, et al.Response surface analysis and process optimization of twin-screw extrusion cooking of potato-based snacks[J].Journal of Food Processing and Preservation, 2015, 39(3):270-281.
[19] 王宏伟, 肖乃勇, 马颖.超声处理时间对小麦淀粉聚集态结构及理化性能的影响[J].轻工学报, 2019, 34(5):10-19.
WANG H W, XIAO N Y, MA Y.Effect of ultrasonic treatment time on aggregation structure and physicochemical properties of wheat starch [J].Journal of Light Industry, 2019, 34(5):10-19.
[20] 王艳, 王宏伟, 王凯旭, 等.湿热处理对大米淀粉流变特性的影响[J].食品工业科技, 2021, 42(3):48-52.
WANG Y, WANG H W, WANG K X, et al.Effect of heat-moisture treatment on rheological properties of rice starch [J].Science and Technology of Food Industry, 2021, 42(3):48-52.
[21] RAFIQ A, SHARMA S, SINGH B.Regression analysis of gluten-free pasta from brown rice for characterization and in vitro digestibility [J].Journal of Food Processing and Preservation, 2017, 41(2):e12830.
[22] 李云龙, 董桂梅, 董吉林, 等.不同糊化度苦荞粉理化性质和体外消化性的研究[J].中国粮油学报, 2021, 36(3):21-27.
LI Y L, DONG G M, DONG J L, et al.Physicochemical properties and in vitro digestibility of Tartary buckwheat flour with different degrees of gelatinization[J]. Journal of the Chinese Cereals and Oils Association, 2021, 36(3):21-27.