The detection of additives in pickles in Sichuan province will provide a reference for government regulation and consumption of residents. There were 576 lot samples of pickles collected from 42 districts or counties of 21 prefectural-level cities and autonomous prefectures in Sichuan in 2019 used as raw materials. The additive contents in samples were detected according to Chinese national standards, and the residual status of additives in pickles was analyzed. The results showed that 12 kinds of additives were detected from pickles and the detection rates were from 1.91% to 65.10%. Moreover, the detection rates of benzoic acid, sorbic acid, acesulfame-k, dehydroacetic acid, sulfur dioxide, tartrazine, and nitrite of those additives exceeded 40%. Eight additives were added excessively and one additive was added illegally, their exceeding-standard rates were 0.17%-13.89%, and benzoic acid (8.33%), sulfur dioxide (13.89%), and tartrazine (1.91%) had higher exceeding-standard rates. Furthermore, at least five additives were detected from every district or country and some additives in pickles from 31 districts or counties (73.81%) exceeded Chinese national standards. 1-9 additives were simultaneously detected from 98.78% of pickle samples, and most of the samples (49.31%) simultaneously contained 3-4 additives. One to three additives in 22.57% of pickle samples simultaneously exceeded national standards, and one additive in most of the samples (18.23%) exceeded standards. Addition and the exceeding standard of additives in pickles were associated with the types of raw materials. Nine, nine, and six additives in bulk pickles and pickles produced by the self-employed and from farmer’s market exceeded standards, respectively, and exceeding-standard rates of benzoic acid and sulfur dioxide reached up to 13.64%-16.36% and 24.52%-36.35%. The results demonstrated that the additive is widely used in pickles in Sichuan and some additives were added excessively and illegally. Pickles produced by the self-employed and from farmer’s markets and bulk pickles should be attentively supervised and inspected for consumption safety.
[1] 章善生. 中国酱腌菜[M].北京:中国商业出版社, 1994.
ZHANG S S.Chinese Pickles[M].Beijing:China Business Press,1994.
[2] 陈伟萍, 倪铭炯.酱腌菜存在的质量安全问题及质量控制建议[J].现代食品, 2021(14):122-123;126.
CHEN W P, NI M J.Quality and safety problems of pickled vegetables and quality control suggestions[J].Modern Food, 2021(14):122-123;126.
[3] 罗钰珊, 乐丽华, 宋美英, 等.酱腌菜常用添加剂的调查分析[J].食品与发酵科技, 2019, 55(5):51-54.
LUO Y S, LE L H, SONG M Y, et al.Investigation and analysis of common additives for pickles[J].Food and Fermentation Sciences & Technology, 2019, 55(5):51-54.
[4] 崔文甲, 王月明, 弓志青, 等.酱腌菜国内外产业现状、研究进展及展望[J].食品工业, 2017, 38(11):238-241.
CUI W J, WANG Y M, GONG Z Q, et al.The industry situation, research progress at home and abroad and the development of pickles[J].The Food Industry, 2017, 38(11):238-241.
[5] QURRAT-UL-AIN, KHAN S A.Artificial sweeteners:Safe or unsafe?[J].JPMA.the Journal of the Pakistan Medical Association, 2015, 65(2):225-227.
[6] LIN D Y, TSAI C H, HUANG Y, et al.Novel strategy for food safety risk management and communication:Risk identification for benzoic acid residues in pickled vegetables[J].Food Science & Nutrition, 2020, 8(10):5 419-5 425.
[7] AMCHOVA P, KOTOLOVA H, RUDA-KUCEROVA J.Health safety issues of synthetic food colorants[J].Regulatory Toxicology and Pharmacology, 2015, 73(3):914-922.
[8] 吴逸华, 叶洁, 王碧波, 等.12家生产企业的酱腌菜防腐剂、甜味剂、亚硝酸盐检测结果分析[J].现代食品, 2019(19):186-188.
WU Y H, YE J, WANG B B, et al.Analysis of detection results of preservatives, sweeteners and nitrites of pickles in 12 production enterprises[J].Modern Food, 2019(19):186-188.
[9] 谭静, 周莉, 平洋, 等.郑州市售散装酱腌菜卫生状况和防腐剂含量检测分析[J].食品安全质量检测学报, 2021, 12(3):1 171-1 174.
TAN J, ZHOU L, PING Y, et al.Hygienic status and preservative content detection of bulk pickles sold in Zhengzhou city[J].Journal of Food Safety & Quality, 2021, 12(3):1 171-1 174.
[10] 尤妍. 市售酱腌菜中常用添加剂检测与分析[J].中国食物与营养, 2018, 24(4):26-28.
YOU Y.Detection and analysis of common additives in pickles[J].Food and Nutrition in China, 2018, 24(4):26-28.
[11] 中华人民共和国国家市场监督管理总局. 食品安全抽样检验管理办法(令第15号)[R].国家市场监督管理总局, 2019.
State Administration for Market Regulation, PRC.Measures for the administration of food safety spot inspections (Order No.15)[R].State Administration for Market Regulation, 2019.
[12] 中华人民共和国食品药品监督管理总局. 食品安全监督抽检和风险监测工作规范(食药监办食监三〔2015〕35号)[R].卫生部, 食品药品监管局, 2015.
China Food and Drug Administration.Code for supervision, sampling inspection and risk monitoring of food safety (No.35, 2015)[R].The Minister of Health of the People’s Republic of China, Food and drug administration,2015.
[13] 杨保刚. 我国酱腌菜行业质量调研报告[J].质量与标准化, 2014(11):31-33.
YANG B G.Quality investigation report port of Chinese pickle industry[J].Quality and Standardization, 2014(11):31-33.
[14] 张茜. 我国酱腌菜行业质量安全和管理探讨[J].现代农业科技, 2017(21):258-259.
ZHANG Q.Discussion on quality safety and management of Chinese pickle industry[J].Modern Agricultural Science and Technology, 2017(21):258-259.
[15] 董梅, 李金壕, 郭莉君, 等.酱腌菜中苯甲酸、山梨酸和糖精钠含量调查[J].中国卫生检验杂志, 2020, 30(20):2 552-2 553;2 558.
DONG M, LI J H, GUO L J, et al.Investigation of benzoic acid, sorbic acid and saccharin sodium contents in pickles[J].Chinese Journal of Health Laboratory Technology, 2020, 30(20):2 552-2 553;2 558.
[16] 赵磊, 李成康, 张其圣, 等.东坡泡菜质量安全调查报告[J].中国调味品, 2018, 43(3):114-118;121.
ZHAO L, LI C K, ZHANG Q S, et al.The quality safety investigation report of Dongpo pickles[J].China Condiment, 2018, 43(3):114-118;121.
[17] 陈国征, 林怡, 吴佳敏, 等.2018年桐乡市酱腌菜中4种食品添加剂含量的调查分析[J].中国卫生检验杂志, 2020, 30(7):877-879.
CHEN G Z, LIN Y, WU J M, et al.Investigation and analysis of four food additives in pickled vegetables in Tongxiang city in 2018[J].Chinese Journal of Health Laboratory Technology, 2020, 30(7):877-879.
[18] 厉晨皓, 陆春燕, 朱吕, 等.平湖市市售酱腌菜添加剂检测结果分析[J].现代食品, 2021 (2):216-218;222.
LI C H,LU C Y, ZHU L, et al.Analysis of testing results of additives for pickled vegetables in Pinghu city[J].Modern Food, 2021(2):216-218;222.
[19] 高科, 王俭, 潘雪良.常熟市售酱腌菜防腐剂调查及关键控制环节分析[J].职业与健康, 2009, 25(13):1 376-1 377.
GAO K, WANG J, PAN X L.Preservatives survey and critical control segments analysis of pickled vegetables[J].Occupation and Health, 2009, 25(13):1 376-1 377.
[20] 张玉梅, 许炼.华容县酱腌菜二氧化硫残留问题的调查[J].食品安全质量检测学报, 2016, 7(7):3 006-3 009.
ZHANG Y M, XU L.Investigation of sulfur dioxide residue in pickles in Huarong County[J].Journal of Food Safety & Quality, 2016, 7(7):3 006-3 009.
[21] 魏静, 申艳琴.市售酱腌菜中亚硝酸盐含量的监测结果分析[J].中国卫生检验杂志, 2017, 27(23):3 484-3 485.
WEI J, SHEN Y Q.Surveillance results analysis of nitrite content in pickles on market[J].Chinese Journal of Health Laboratory Technology, 2017, 27(23):3 484-3 485.
[22] 董桂贤, 王朝霞, 宫春波, 等.烟台市市售散装酱腌菜中7种防腐剂含量状况调查[J].中国食品卫生杂志, 2013, 25(3):264-267.
DONG G X, WANG Z X, GONG C B, et al.Investigation of 7 food preservative residuals from 300 pickled vegetables in bulk at retail[J].Chinese Journal of Food Hygiene, 2013, 25(3):264-267.