Analysis of flavor substance in cold eating beef

  • WAN Xiaoyu ,
  • XIANG Yuzhou ,
  • ZHOU Yingru ,
  • LIU Zijian ,
  • LIN Hongbin ,
  • YUAN Xianling
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  • 1(College of Bio-engineering, Sichuan University of Science and Engineering, Yibin 644000, China)
    2(Zigong Tanbaye Food Factory, Zigong 643000, China)
    3(College of Food and Bio-engineering, Xihua University, Chengdu 610039, China)

Received date: 2021-07-21

  Revised date: 2021-11-14

  Online published: 2022-11-01

Abstract

There are many kinds of cold eating beef products, however, no standard characteristic flavor substance for it. In this study, headspace-solid phase microextraction combined with gas chromatography-mass spectrometry (HS-SPME-GC-MS) was used to determine the volatile flavor substances of cold eating beef. The results showed that a total of 54 flavor compounds were identified in different cold eating beef, including 11 hydrocarbons, 10 alcohols, 10 acids, 5 esters, 8 aldehydes, 5 phenols, and 3 ethers. According to odor activity value analysis, the flavor characteristics of cold eating beef were summarized as flower flavor, anise flavor, fat flavor, and mushroom flavor. Furthermore, the principal component analysis showed that the cumulative contribution rate of three principal components of volatile flavor compounds in cold eating beef reached 100%. After the comprehensive score of four kinds of cold eating beef indicated that N2 had the highest score (68). Sensory analysis showed that N1 and N2 were more prominent.

Cite this article

WAN Xiaoyu , XIANG Yuzhou , ZHOU Yingru , LIU Zijian , LIN Hongbin , YUAN Xianling . Analysis of flavor substance in cold eating beef[J]. Food and Fermentation Industries, 2022 , 48(19) : 272 -279 . DOI: 10.13995/j.cnki.11-1802/ts.028619

References

[1] 李素, 周慧敏, 赵冰, 等.卤汤牛肉贮藏过程中挥发性风味物质分析[J].食品科学, 2020, 41(18):203-209.
LI S, ZHOU H M, ZHAO B, et al.Analysis of volatile flavor compounds in stewed beef with broth during storage[J].Food Science, 2020, 41(18):203-209.
[2] 李娟, 韩东, 米思, 等.北京地区酱卤牛肉中挥发性风味物质剖面分析[J].核农学报, 2020, 34(1):94-103.
LI J, HAN D, MI S, et al.Profile analysis of the volatile flavor compounds from Beijing area of marinated beef[J].Journal of Nuclear Agricultural Sciences, 2020, 34(1):94-103.
[3] ARSHAD M S, SOHAIB M, AHMAD R S, et al.Ruminant meat flavor influenced by different factors with special reference to fatty acids[J].Lipids in Health and Disease, 2018, 17(1):223.
[4] GARDNER K, LEGAKO J F.Volatile flavor compounds vary by beef product type and degree of doneness[J].Journal of Animal Science, 2018, 96(10):4 238-4 250.
[5] 吴倩蓉, 朱宁, 陈松, 等.加工工艺对酱牛肉中蛋白质降解及风味物质的影响[J].食品科学, 2021, 42(12):76-84.
WU Q R, ZHU N, CHEN S, et al.Changes in protein degradation and flavor substance in sauce beef during processing[J].Food Science, 2021, 42(12):76-84.
[6] 毛永强, 李彦虎, 贠建民, 等.传统陇西腊肉制作过程中挥发性风味物质变化分析[J].食品与发酵工业, 2021, 47(4):144-152.
MAO Y Q, LI Y H, YUN J M, et al.The analysis of the volatile flavor compounds in traditional Longxi bacon production[J].Food and Fermentation Industries, 2021, 47(4):144-152.
[7] GONG H, YANG Z, LIU M, et al.Time-dependent categorization of volatile aroma compound formation in stewed Chinese spicy beef using electron nose profile coupled with thermal desorption GC-MS detection[J].Food Science and Human Wellness, 2017, 6(3):137-146.
[8] 谭雪梅, 唐善虎, 李思宁, 等.反复式冻融-风干对风干牦牛肉的理化特性和挥发性成分的影响[J].食品与发酵工业, 2020, 46(4):131-138.
TAN X M, TANG S H, LI S N, et al.Effects of air-drying with repeated freeze-thaw on the physicochemical properties and volatile compounds of dried yak meat[J].Food and Fermentation Industries, 2020, 46(4):131-138.
[9] 尹含靓, 肖何, 邓高文, 等.基于GC-IMS技术分析不同香辛料水煮液的风味物质组成差异[J].食品工业科技, 2021, 42(17):278-284.
YIN H L, XIAO H, DENG G W, et al.Based on GC-IMS technology to analyze the difference in flavor composition of different spice boiling liquids[J].Science and Technology of Food Industry, 2021, 42(17):278-284.
[10] 陈海涛, 张宁, 孙宝国.SPME或SDE结合GC-MS分析贾永信十香酱牛肉的挥发性风味成分[J].食品科学, 2012, 33(18):171-176.
CHEN H T, ZHANG N, SUN B G.Analysis of volatile compounds in Jiayongxin spiced beef by solid phase microextraction or simultaneous distillation extraction coupled with gas chromatography-mass spectroscopy[J].Food Science, 2012, 33(18):171-176.
[11] MOTTRAM D S.Flavour formation in meat and meat products:A review[J].Food Chemistry, 1998, 62(4):415-424.
[12] XIE J C, SUN B G, ZHENG F P, et al.Volatile flavor constituents in roasted pork of Mini-pig[J].Food Chemistry, 2008, 109(3):506-514.
[13] 许刚, 丁浩宸, 张燕平, 等.畜禽肉和鱼肉对南极磷虾凝胶制品挥发性风味成分的影响[J].食品与发酵工业, 2016, 42(5):132-139.
XU G, DING H C, ZHANG Y P, et al.Effect of meat or fish content on volatile flavor components in Antarctic krill gel products[J].Food and Fermentation Industries, 2016, 42(5):132-139.
[14] 周亚军, 张玉, 陈艳, 等.发酵牛肉干加工中理化特性与风味品质分析[J].食品科学, 2021, 42(14):240-247.
ZHOU Y J, ZHANG Y, CHEN Y, et al.Analysis of physicochemical characteristics and flavor quality of fermented beef jerky during its processing[J].Food Science, 2021, 42(14):240-247.
[15] 李儒仁, 陈雨, 张庆永, 等.扒鸡加工过程中挥发性风味物质的变化规律[J].肉类研究, 2019, 33(7):49-55.
LI R R, CHEN Y, ZHANG Q Y, et al.Changes in volatile flavor compounds of Dezhou braised chicken during processing[J].Meat Research, 2019, 33(7):49-55.
[16] 刘梦, 陈松, 张顺亮, 等.微发酵对牛肉干风味的影响[J].食品科学, 2021, 42(14):232-239.
LIU M, CHEN S, ZHANG S L, et al.Effect of light fermentation on the flavor of beef jerky[J].Food Science, 2021, 42(14):232-239.
[17] 倪德让, 叶兴乾, 林琳, 等.基于多酚类化合物HPLC指纹图谱在红缨子高粱原料品质监控中的应用[J].食品科学, 2020, 41(8):250-255.
NI D R, YE X Q, LIN L, et al.Application of high performance liquid chromatographic phenolic compound fingerprint in quality control of “hongyingzi” Sorghum raw material[J].Food Science, 2020, 41(8):250-255.
[18] 李素, 周慧敏, 张顺亮, 等.不同加水量腌制酱牛肉中挥发性风味物质变化[J].食品科学, 2019, 40(10):199-205.
LI S, ZHOU H M, ZHANG S L, et al.Changes of volatile flavor compounds in spiced beef marinated with different water contents[J].Food Science, 2019, 40(10):199-205.
[19] 孙杰. 牛肉干的风味分析及仿香研究[D].北京:北京工商大学, 2017.
SUN J.Analysis and simulation of volatile aroma compounds in beef jerky[D].Beijing:Beijing Technology and Business University, 2017.
[20] 童庆宣, 罗小飞, 梁诗.香辛料植物及香辛料主要化学成分[J].中国野生植物资源, 2009, 28(4):60-65;68.
TONG Q X, LUO X F, LIANG S.Spice plants and the main chemical components of spices[J].Chinese Wild Plant Resources, 2009, 28(4):60-65;68.
[21] 梁建兰, 李晓颍, 赵玉华, 等.SPME-GC-MS结合ROAV分析糖炒燕山早丰板栗中的特征性香气[J].食品科技, 2019, 44(12):300-305.
LIANG J L, LI X Y, ZHAO Y H, et al.Study on characteristic aromatic compounds in ‘Yanshanzaofeng’ chestnut roasted in sugar determined by SPME-GC-MS and ROAV[J].Food Science and Technology, 2019, 44(12):300-305.
[22] 李鹏宇, 张宁, 陈海涛, 等.SDE-GC-MS结合GC-O分析番茄牛腩的挥发性风味成分[J].食品工业科技, 2017, 38(2):89-97.
LI P Y, ZHANG N, CHEN H T, et al.Analysis of volatile compounds in braised beef brisket with tomato by SDE-GC-MS and GC-O[J].Science and Technology of Food Industry, 2017, 38(2):89-97.
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