Preparation of cellulose nanocrystals by hydrolysis with different sulfuric acid concentrations and their stabilized Pickering emulsions

  • WANG Yuxi ,
  • GAO Huanqiu ,
  • DAI Difei ,
  • HU Shuhan ,
  • LUO Yuyuan ,
  • HUANG Yue ,
  • ZHANG Yuhao ,
  • YU Yong ,
  • DAI Hongjie
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  • 1(College of Food Science, Southwest University, Chongqing 400715, China)
    2(Chongqing Sericulture Science and Technology Research Institute, Chongqing 400700, China)
    3(National Demonstration Center for Experimental Food Science and Technology Education (Southwest University), Chongqing 400715, China)

Received date: 2023-03-22

  Revised date: 2023-04-17

  Online published: 2024-06-11

Abstract

Cellulose nanocrystals (CNCs) were extracted from pineapple peel cellulose by traditional sulfuric acid hydrolysis method.The effects of sulfuric acid solution concentration (58%, 61%, and 64%, mass fraction) on particle size, morphology, potential, thermal stability, and stable Pickering emulsion properties of the prepared CNCs (CNCs-58%, CNCs-61%, and CNCs-64%) were investigated.Results showed that with the increase of sulfuric acid solution concentration, the diameter and length of CNCs decreased gradually with increased uniformity, and the absolute potential increased gradually (-33.5 mV, -43.6 mV, and -45.7 mV), but the thermal stability decreased.Compared with CNCs-58%, CNCs-61% and CNCs-64% showed better stable Pickering emulsion properties, showing a smaller droplet size, better storage stability, and a relatively larger absolute value of potential.However, at low CNCs concentration (0.2%, mass fraction), the degree of water evolution of CNCs-64% stabilized emulsion was relatively high, which was related to the morphology of CNCs.With the increase in CNCs concentration, the water evolution degree of emulsion decreased significantly.This study provides a reference for the preparation of CNCs from fruit and vegetable peel cellulose hydrolyzed by sulfuric acid and its application in Pickering emulsions.

Cite this article

WANG Yuxi , GAO Huanqiu , DAI Difei , HU Shuhan , LUO Yuyuan , HUANG Yue , ZHANG Yuhao , YU Yong , DAI Hongjie . Preparation of cellulose nanocrystals by hydrolysis with different sulfuric acid concentrations and their stabilized Pickering emulsions[J]. Food and Fermentation Industries, 2024 , 50(9) : 132 -138 . DOI: 10.13995/j.cnki.11-1802/ts.035582

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