[1] JI X F, JIN C H, XIAO Y P, et al.Natural occurrence of regulated and emerging mycotoxins in wheat grains and assessment of the risks from dietary mycotoxins exposure in China[J].Toxins, 2023, 15(6):389.
[2] HONG X, MAO Y H, YANG C Q, et al.Contamination of Zearalenone from China in 2019 by a visual and digitized immunochromatographic assay[J].Toxins, 2020, 12(8):521.
[3] 赵柬云, 韩小敏, 徐文静, 等.2019年中国四省小麦中12种真菌毒素污染情况调查[J].中国食品卫生杂志, 2021, 33(6):765-770.
ZHAO J Y, HAN X M, XU W J, et al.Investigation of 12 mycotoxins in wheat grains from four provinces of China in 2019[J].Chinese Journal of Food Hygiene, 2021, 33(6):765-770.
[4] 唐占敏. 长三角地区谷物中典型真菌毒素识别及污染研究[D].上海:上海海洋大学, 2020.
TANG Z M.Identification and pollution of typical mycotoxins in cereals in Yangtze River Delta region[D].Shanghai:Shanghai Ocean University, 2020.
[5] 任贝贝, 王丽英, 路杨, 等.河北省小麦、玉米及其制品中16种真菌毒素污染水平调查与分析[J].食品安全质量检测学报, 2021, 12(5):1669-1676.
REN B B, WANG L Y, LU Y, et al.Investigation and analysis of 16 kinds of mycotoxins pollution levels in wheat, corn and products in Hebei province[J].Journal of Food Safety & Quality, 2021, 12(5):1669-1676.
[6] ZHAO J Y, CHENG T X, XU W J, et al.Natural co-occurrence of multi-mycotoxins in unprocessed wheat grains from China[J].Food Control, 2021, 130:108321.
[7] 程天笑, 韩小敏, 王硕, 等.2018年中国4省脱粒小麦中9种真菌毒素污染情况调查[J].食品安全质量检测学报, 2020, 11(12):3992-3999.
CHENG T X, HAN X M, WANG S, et al.Investigation on contamination situation of 9 mycotoxins in wheat kernel from 4 provinces of China in 2018[J].Journal of Food Safety & Quality, 2020, 11(12):3992-3999.
[8] LIN X H, ZHANG Q, ZHANG Y, et al.Further data on the levels of emerging Fusarium mycotoxins in cereals collected from Tianjin, China[J].Food Additives & Contaminants:Part B, Surveillance, 2021, 14(1):74-80.
[9] 王瑞虎, 李萌萌, 关二旗, 等.乙酰化脱氧雪腐镰刀菌烯醇污染、毒性及转化研究进展[J].食品科学, 2023, 44(1):345-352.
WANG R H, LI M M, GUAN E Q, et al.Progress in research on contamination, toxicity and transformation of acetylated deoxynivalenol[J].Food Science, 2023, 44(1):345-352.
[10] OVANDO-MARTÍNEZ M, OZSISLI B, ANDERSON J, et al.Analysis of deoxynivalenol and deoxynivalenol-3-glucoside in hard red spring wheat inoculated with Fusarium graminearum[J].Toxins, 2013, 5(12):2522-2532.
[11] WANG R H, LI M M, JIN R, et al.Interactions among the composition changes in fungal communities and the main mycotoxins in simulated stored wheat grains[J].Journal of the Science of Food and Agriculture, 2024, 104(1):373-382.
[12] SHEPHARD G S, VAN DER WESTHUIZEN L, GATYENI P M, et al.Do fumonisin mycotoxins occur in wheat?[J].Journal of Agricultural and Food Chemistry, 2005, 53(23):9293-9296.
[13] 张林炜. 市售小麦制品中链格孢霉毒素残留和膳食暴露评估[D].合肥:安徽农业大学, 2023.
ZHANG L W.Assessment of Alternaria toxin residues and dietary exposure in wheat products on the market[D].Hefei:Anhui Agricultural University, 2023.
[14] WANG X D, YANG D J, QIN M, et al.Risk assessment and spatial analysis of deoxynivalenol exposure in Chinese population[J].Mycotoxin Research, 2020, 36(4):419-427.
[15] 杨晓倩, 刘岚铮, 曹小丽, 等.2022年山东省市售小麦粉真菌毒素污染情况调查[J].预防医学论坛, 2023, 29(8):577-581.
YANG X Q, LIU L Z, CAO X L, et al.Investigation on mycotoxin pollution of wheat flour on market in Shandong province in 2022[J].Preventive Medicine Tribune, 2023, 29(8):577-581.
[16] ZHOU H Y, XU A Q, LIU M C, et al.Mycotoxins in wheat flours marketed in Shanghai, China:Occurrence and dietary risk assessment[J].Toxins, 2022, 14(11):748.
[17] 张欣烨, 彭靖, 张洁, 等.2019—2020年河南省谷类食品中7种真菌毒素污染状况调查[J].中国卫生检验杂志, 2021, 31(18):2274-2276.
ZHANG X Y, PENG J, ZHANG J, et al.Investigation into contamination status of 7 mycotoxins in cereals in Henan Province from 2019 to 2020[J].Chinese Journal of Health Laboratory Technology, 2021, 31(18):2274-2276.
[18] 李俊玲, 王书舟, 吴俊威, 等.河南省粮食及其制品中真菌毒素污染情况调查[J].中国食品卫生杂志, 2020, 32(4):418-421.
LI J L, WANG S Z, WU J W, et al.Investigation of mycotoxins in grain and its products in Henan Province[J].Chinese Journal of Food Hygiene, 2020, 32(4):418-421.
[19] ZHANG Y Y, PEI F, FANG Y, et al.Comparison of concentration and health risks of 9 Fusarium mycotoxins in commercial whole wheat flour and refined wheat flour by multi-IAC-HPLC[J].Food Chemistry, 2019, 275:763-769.
[20] ANDRÉ A, MÜLLER N, CHETSCHIK I.Occurrence of Zearalenone and enniatin B in Swiss wheat grains and wheat flours[J].Applied Sciences, 2022, 12(20):10566.
[21] GETAHUN M, FININSA C, MOHAMMED A, et al.Fungal species and multi-mycotoxin in bread wheat (Triticum aestivum L.) in Ethiopia[J].World Mycotoxin Journal, 16(2):179-194.
[22] GAVRILOVA O P, GAGKAEVA T Y, ORINA A S, et al.Diversity of Fusarium species and their mycotoxins in cereal crops from the Asian territory of Russia[J].Doklady Biological Sciences, 2023, 508(1):9-19.
[23] KOLETSI P, SCHRAMA J W, GRAAT E A M, et al.The occurrence of mycotoxins in raw materials and fish feeds in Europe and the potential effects of deoxynivalenol (DON) on the health and growth of farmed fish species-a review[J].Toxins, 2021, 13(6):403.
[24] BRYŁA M, KSIENIEWICZ-WOÖNIAK E, YOSHINARI T, et al.Contamination of wheat cultivated in various regions of Poland during 2017 and 2018 agricultural seasons with selected trichothecenes and their modified forms[J].Toxins, 2019, 11(2):88.
[25] IQBAL S Z, USMAN S, RAZIS A F A, et al.Assessment of deoxynivalenol in wheat, corn and its products and estimation of dietary intake[J].International Journal of Environmental Research and Public Health, 2020, 17(15):5602.
[26] IQBAL S Z, REHMAN B, SELAMAT J, et al.Assessment of fumonisin B1 concentrations in wheat and barley products in the punjab region of Pakistan[J].Journal of Food Protection, 2020, 83(8):1284-1288.
[27] GOLGE O, KABAK B.Occurrence of deoxynivalenol and Zearalenone in cereals and cereal products from Turkey[J].Food Control, 2020, 110:106982.
[28] KARLSSON I, MELLQVIST E, PERSSON P.Temporal and spatial dynamics of Fusarium spp.and mycotoxins in Swedish cereals during 16 years[J].Mycotoxin Research, 2023, 39(1):3-18.
[29] SHI H T, SCHWAB W, YU P Q.Natural occurrence and co-contamination of twelve mycotoxins in industry-submitted cool-season cereal grains grown under a low heat unit climate condition[J].Toxins, 2019, 11(3):160.
[30] SALMAN M K, MUDALAL S.Quality control and mycotoxin levels in food in the Palestinian market[J].Food Additives & Contaminants: Part B, 2022,15(2):123-128.
[31] GAB-ALLAH M A, TAHOUN I F, YAMANI R N, et al.Natural occurrence of deoxynivalenol, nivalenol and deoxynivalenol-3-glucoside in cereal-derived products from Egypt[J].Food Control, 2022, 137:108974.
[32] HESHMATI A, MOZAFFARI NEJAD A S, MEHRI F.Occurrence, dietary exposure, and risk assessment of aflatoxins in wheat flour from Iran[J].International Journal of Environmental Analytical Chemistry, 2023, 103(20):9395-9408.
[33] GAB-ALLAH M A, MEKETE K G, CHOI K, et al.Occurrence of major type-B trichothecenes and deoxynivalenol-3-glucoside in cereal-based products from Korea[J].Journal of Food Composition and Analysis, 2021, 99:103851.
[34] PUNTSCHER H, COBANKOVIC I, MARKO D, et al.Quantitation of free and modified Alternaria mycotoxins in European food products by LC-MS/MS[J].Food Control, 2019, 102:157-165.
[35] CIRIO M, VILLARREAL M, SEAL T M L, et al.Incidence of deoxynivalenol in wheat flour in Argentina and GC-ECD method validation[J].Journal of AOAC International, 2019, 102(6):1721-1724.
[36] JAHANBAKHSH M, AFSHAR A, MOMENI FEELI S, et al.Probabilistic health risk assessment (Monte Carlo simulation method) and prevalence of aflatoxin B1 in wheat flours of Iran[J].International Journal of Environmental Analytical Chemistry, 2021, 101(8):1074-1085.
[37] BRYŁA M, KSIENIEWICZ-WOZ′NIAK E, WAS′KIEWICZ A, et al.Natural occurrence of nivalenol, deoxynivalenol, and deoxynivalenol-3-glucoside in Polish winter wheat[J].Toxins, 2018, 10(2):81.
[38] CASU A, LEGGIERI M C, TOSCANO P, et al.Changing climate, shifting mycotoxins:A comprehensive review of climate change impact on mycotoxin contamination[J].Comprehensive Reviews in Food Science and Food Safety, 2024, 23(2):e13323.
[39] 崔东伟. 谷物及其制品中真菌毒素的检测技术研究[D].沈阳:中国医科大学, 2021.
CUI D W.Research on precise detection technology of mycotoxins in grains and their products[D].Shenyang:China Medical University, 2021.
[40] TSAGKARIS A S, PRUSOVA N, DZUMAN Z, et al.Regulated and non-regulated mycotoxin detection in cereal matrices using an ultra-high-performance liquid chromatography high-resolution mass spectrometry (UHPLC-HRMS) method[J].Toxins, 2021, 13(11):783.
[41] SANTINI A, FERRACANE R, SOMMA M C, et al.Multitoxin extraction and detection of trichothecenes in cereals:An improved LC-MS/MS approach[J].Journal of the Science of Food and Agriculture, 2009, 89(7):1145-1153.
[42] GAB-ALLAH M A, CHOI K, KIM B.Development of isotope dilution-liquid chromatography/tandem mass spectrometry for the accurate determination of type-a trichothecenes in grains[J].Food Chemistry, 2021, 344:128698.
[43] HEIDARI G, HASHEMI HAZAVEH S J, DARAEI B, et al.Validation of an UHPLC-MS/MS method for simultaneous analysis of 11 mycotoxins in wheat flour using immunoaffinity column[J].Iranian Journal of Pharmaceutical Research, 2019, 18(Suppl1):182-189.
[44] KOVAC′ M, BULAIČ M, JAKOVLJEVIC′ J, et al.Mycotoxins, pesticide residues, and heavy metals analysis of Croatian cereals[J].Microorganisms, 2021, 9(2):216.
[45] ZHANG L X, HUANG Z H, LUO S Q, et al.Establishment of non-targeted screening database and confirmation method for 18 mycotoxins in grains using ultra performance liquid chromatography-quadrupole-time of flight mass spectrometry[J].Se Pu, 2023, 41(1):66-75.
[46] 张大伟, 高和杨, 周旌, 等.超高效液相色谱-串联质谱法同时检测饲料原料、饲料成品中18种真菌毒素含量[J].食品安全质量检测学报, 2018, 9(22):5867-5876.
ZHANG D W, GAO H Y, ZHOU J, et al.Simultaneous determination of 18 kinds of mycotoxins in feed ingredients and feed products by ultra performance liquid chromatography-tandem mass spectrometry[J].Journal of Food Safety & Quality, 2018, 9(22):5867-5876.
[47] HALLIER A, CELETTE F, DAVID C.Effects of sampling and extraction on deoxynivalenol quantification[J].Food Chemistry, 2011, 127(1):303-307.
[48] KUMPHANDA J, MATUMBA L, MONJEREZI M, et al.Are sample size and sample preparation for mycotoxin quantitation in grain products getting trivialized?[J].Food Control, 2021, 130:108400.
[49] 王蓓蓓. 复合免疫亲和-液相色谱-串联质谱法测定黑米中真菌毒素的研究[D].汉中:陕西理工大学, 2022.
WANG B B.Determination of mycotoxins in black rice by compound immunoaffinity-liquid chromatography-tandem mass spectrometry[D].Hanzhong:Shaanxi University of Technology, 2022.
[50] SERRANO A B, FONT G, MAÑES J, et al.Comparative assessment of three extraction procedures for determination of emerging Fusarium mycotoxins in Pasta by LC-MS/MS[J].Food Control, 2013, 32(1):105-114.
[51] BIAN Y, ZHANG Y, ZHOU Y, et al.Recent insights into sample pretreatment methods for mycotoxins in different food matrices:A critical review on novel materials[J].Toxins, 2023, 15(3):215.
[52] SULYOK M, BERTHILLER F, KRSKA R, et al.Development and validation of a liquid chromatography/tandem mass spectrometric method for the determination of 39 mycotoxins in wheat and maize[J].Rapid Communications in Mass Spectrometry, 2006, 20(18):2649-2659.
[53] GREER B, CHEVALLIER O, QUINN B, et al.Redefining dilute and shoot:The evolution of the technique and its application in the analysis of foods and biological matrices by liquid chromatography mass spectrometry[J].TrAC Trends in Analytical Chemistry, 2021, 141:116284.
[54] 黎睿, 谢刚, 王松雪.高效液相色谱法同时检测粮食中常见8种真菌毒素的含量[J].食品科学, 2015, 36(6):206-210.
LI R, XIE G, WANG S X.Simultaneous analysis of 8 mycotoxins in grains by high performance liquid chromatography[J].Food Science, 2015, 36(6):206-210.
[55] SANTOS PEREIRA C, C CUNHA S, FERNANDES J O.Prevalent mycotoxins in animal feed:Occurrence and analytical methods[J].Toxins, 2019, 11(5):290.
[56] BERTHILLER F, SCHUHMACHER R, BUTTINGER G, et al.Rapid simultaneous determination of major type A- and B-trichothecenes as well as Zearalenone in maize by high performance liquid chromatography-tandem mass spectrometry[J].Journal of Chromatography. A, 2005, 1062(2):209-216.
[57] VARGAS MEDINA D A, BASSOLLI BORSATTO J V, MACIEL E V S, et al.Current role of modern chromatography and mass spectrometry in the analysis of mycotoxins in food[J].TrAC Trends in Analytical Chemistry, 2021, 135:116156.
[58] DE SANTIS B, DEBEGNACH F, GREGORI E, et al.Development of a LC-MS/MS method for the multi-mycotoxin determination in composite cereal-based samples[J].Toxins, 2017, 9(5):169.
[59] SINGH J, MEHTA A.Rapid and sensitive detection of mycotoxins by advanced and emerging analytical methods:A review[J].Food Science & Nutrition, 2020, 8(5):2183-2204.
[60] SCOTT P M.Gas Chromatography of Mycotoxins [M].Amsterdam:Elsevier.1993:373-425.
[61] STANCIU O, JUAN C, BERRADA H, et al.Study on trichothecene and Zearalenone presence in Romanian wheat relative to weather conditions[J].Toxins, 2019, 11(3):163.
[62] YANG Y, LI G L, WU D, et al.Recent advances on toxicity and determination methods of mycotoxins in foodstuffs[J].Trends in Food Science & Technology, 2020, 96:233-252.
[63] DIB A A, ASSAF J C, DEBS E, et al.A comparative review on methods of detection and quantification of mycotoxins in solid food and feed:A focus on cereals and nuts[J].Mycotoxin Research, 2023, 39(4):319-345.