Baijiu, renowned for its rich and unique flavor characteristics, occupies a singular position among distilled spirits globally.The flavor is the result of the joint action of the aroma and taste its of its flavor substance, but compared with the research on aroma, the exploration of Baijiu taste is relatively lagging behind.To explore the complex and diverse taste substance basis of Baijiu, the taste threshold of 43 flavor skeleton components in Baijiu were determined by three-alternative forced-choice method with 46%vol ethanol aqueous solution as matrix.The results of threshold determination showed that the taste characteristics of compounds with the same or similar structural formulas were similar, most esters were sweet, and higher alcohols were bitter and organic acids were sour.Compounds with the same taste characteristics also had different flavor characteristics, such as sweetness including fruity sweetness, sour-sweet, or fragrant-sweet.Thus, attention should be paid to the refinement of flavor description when designing product flavor.In addition, the concentration effect and individual differences had an important influence on the determination of taste threshold.The determination of taste threshold should try to keep the determination time consistent with the determination environment, increase the number of tasters appropriately, and strengthen the taste evaluation training of tasters to ensure the accuracy and reliability of the determination results.This study further enriched the research content of Baijiu flavor, provided a more detailed and accurate threshold reference for the research of Baijiu taste, and was of great significance to the sensory evaluation, liquor body design, and quality improvement of Baijiu industry.
[1] 孙宝国, 黄明泉, 王娟.白酒风味化学与健康功效研究进展[J].中国食品学报, 2021, 21(5):1-13.
SUN B G, HUANG M Q, WANG J.Research progress on flavor chemistry and healthy function of Baijiu[J].Journal of Chinese Institute of Food Science and Technology, 2021, 21(5):1-13.
[2] WANG L L, GAO Y C, WU L, et al.Characterization of key aging aroma compounds in aged jiangxiangxing Baijiu and their formation influencing factors during the storge process[J].Journal of Agricultural and Food Chemistry, 2024, 72(3):1695-1707.
[3] WU F, FAN S H, HE G L, et al.Comparison of aroma compounds and sensory characteristics between two different types of rice-based Baijiu[J].Foods, 2024, 13(5):681.
[4] 倪兴婷, 孙细珍, 刘怀臣, 等.浓香型白酒异嗅味-糠味物质解析[J].中国酿造, 2024, 43(7):41-49.
NI X T, SUN X Z, LIU H C, et al.Analysis of off-flavor-bran flavor substances in strong-flavor Baijiu[J].China Brewing, 2024, 43(7):41-49.
[5] 李孟涛, 许德富, 敖宗华, 等.浓香型基酒中糊味特征物质解析[J].食品科学, 2024, 45(13):173-180.
LI M T, XU D F, AO Z H, et al.Analysis of burnt flavor substances in nongxiangxing base Baijiu[J].Food Science, 2024, 45(13):173-180.
[6] 李培, 倪斌, 高洪霞, 等.泸型酒中关键“窖香”风味物质确定及其馏出规律研究[J].食品与发酵工业, 2024, 50(16):202-210.
LI P, NI B, GAO H X, et al.Identification of key Jiao-aroma compounds and their distillation characteristics in Luzhou-flavor Baijiu[J].Food and Fermentation Industries, 2024, 50(16):202-210.
[7] 范文来, 徐岩.白酒79个风味化合物嗅觉阈值测定[J].酿酒, 2011, 38(4):80-84.
FAN W L, XU Y.Determination of odor thresholds of volatile aroma compounds in Baijiu by a forced-choice ascending concentration series method of limits[J].Liquor Making, 2011, 38(4):80-84.
[8] SUN X Z, QIAN Q Q, XIONG Y Q, et al.Characterization of the key aroma compounds in aged Chinese Xiaoqu Baijiu by means of the sensomics approach[J].Food Chemistry, 2022, 384:132452.
[9] YAN Q, ZHANG K Z, ZOU W, et al.Three main flavour types of Chinese Baijiu:Characteristics, research, and perspectives[J].Journal of the Institute of Brewing, 2021, 127(4):317-326.
[10] 杨会. 白酒中不挥发呈味有机酸和多羟基化合物研究[D].无锡:江南大学, 2017.
YANG H.Characterization of non-volatile gustatory organic acids and polyhydroxy compounds in Chinese liquors[D].Wuxi:Jiangnan University, 2017.
[11] 陆力华. 两种香型白酒中甜味物质的初步研究[D].贵阳:贵州大学, 2022.
LU L H.Preliminary study on sweeteners in two kinds of Baijiu[D].Guiyang:Guizhou University, 2022.
[12] SUN Y L, MA Y, CHEN S, et al.Exploring the mystery of the sweetness of Baijiu by sensory evaluation,compositional analysis and multivariate data analysis[J].Foods, 2021, 10(11):2843.
[13] KING E S, DUNN R L, HEYMANN H.The influence of alcohol on the sensory perception of red wines[J].Food Quality and Preference, 2013, 28(1):235-243.
[14] CRETIN B N, DUBOURDIEU D, MARCHAL A.Influence of ethanol content on sweetness and bitterness perception in dry wines[J].LWT, 2018, 87:61-66.
[15] 向玉萍. 白酒中糖和糖醇类物质的解析[D].贵阳:贵州大学, 2022.
XIANG Y P.Analysis of sugar and alcohols in Baijiu[D].Guiyang:Guizhou University, 2022.
[16] 郭世鑫. 酱香型白酒苦味成因与改善措施的研究[D].天津:天津科技大学, 2024.
GUO S X.Causes and improvement measures of bitterness of maitai-flavor Baijiu[D].Tianjin:Tianjin University of Science and Technology, 2024.
[17] WANG L H, ZHU L, ZHENG F P, et al.Determination and comparison of flavor (retronasal) threshold values of 19 flavor compounds in Baijiu[J].Journal of Food Science, 2021, 86(5):2061-2074.
[18] 何菲, 孙宝国, 李贺贺, 等.白酒中风味物质味觉阈值的测定[J].中国食品学报, 2024, 24(10):371-383.
HE F, SUN B G, LI H H, et al.Determination of taste threshold of flavor compounds in Baijiu[J].Journal of Chinese Institute of Food Science and Technology, 2024, 24(10):371-383.
[19] 何英霞, 谢凯筠, 王高伟, 等.白酒口感特征的描述性分析及其口感轮的构建[J].食品科学, 2025, 46(9):63-68.
HE Y X, XIE K J, WANG G W, et al.Descriptive analysis of taste characteristics of Baijiu and construction of its taste wheel[J].Food Science, 2025, 46(9):63-68.
[20] AN F Y,CAO K X, JI S Q, et al.Identification, taste characterization, and molecular docking study of a novel microbiota-derived umami peptide[J].Food Chemistry, 2023, 404:134583.
[21] WANG X X, FAN W L, XU Y.Comparison on aroma compounds in Chinese soy sauce and strong aroma type liquors by gas chromatography-olfactometry, chemical quantitative and odor activity values analysis[J].European Food Research and Technology, 2014, 239(5):813-825.
[22] 吴天祥, 杨海龙, 章克昌.白酒香型风格与白酒色谱骨架成分关系的初步研究[J].酿酒, 2002,29(3):25-28.
WU T X, YANG H L, ZHANG K C.The basic study on Liquor aroma related to Chromatograph skeleton components in Liquor[J].Liquor-making, 2002, 29(3):25-28.
[23] SUN J Y, ZHAO D R, ZHANG F G, et al.Joint direct injection and GC-MS chemometric approach for chemical profile and sulfur compounds of sesame-flavor Chinese Baijiu (Chinese liquor)[J].European Food Research and Technology, 2018, 244(1):145-160.
[24] CHEN P P, FENG X X, ZHU Y W, et al.Sweetness science of Baijiu:Unraveling flavor compounds, perception and analytical techniques[J].Food Chemistry Advances, 2023, 3:100463.
[25] BARBA C, BENO N, GUICHARD E, et al.Selecting odorant compounds to enhance sweet flavor perception by gas chromatography/olfactometry-associated taste (GC/O-AT)[J].Food Chemistry, 2018, 257:172-181.
[26] LUO X, FAN W L, XU Y, et al.Characterization of volatile bitter off-taste compounds in Maotai-flavor Baijiu (Chinese liquor)[J].LWT, 2025, 217:117363.
[27] 苏永平. 有机酸对酒醅发酵过程中风味组成及微生物群落结构动态变化的影响研究[D].宜宾:四川轻化工大学, 2022.
SU Y P.Effects of organic acids on flavorcomposition and microbialcommunity structure duringfermentation of fermented grains[D].Yibin:Sichuan University of Science & Engineering, 2022.
[28] SCHARBERT S, HOFMANN T.Molecular definition of black tea taste by means of quantitative studies, taste reconstitution, and omission experiments[J].Journal of Agricultural and Food Chemistry, 2005, 53(13):5377-5384.