Traditional Chi flavor Baijiu contains high unsaturated fatty acids after steeping and aging with fat meat, which is easy to be oxidized during storage and cause rancidity. In order to reduce the unpleasant smell, coconut meat with low content of unsaturated fatty acid was used instead of fat meat for steeping and aging of Zhaijiu (raw liquor). The fatty acids in coconut and fat were methylated and then analyzed by GC-MS. The results showed that the content of unsaturated fatty acids in coconut meat was 9.53%, only 21.40% of that in fat meat (44.53%). When comparing the aging effects of different infiltration materials, the transmittance of the aged liquor with raw or cooked coconut meat was better than that with fat meat, the content of unsaturated fatty acids decreased by 26.09% and 30.21% respectively, and the stability of the liquor body was increased. The optimal aging process was: coconut addition of 200 g/L Zhaijiu, aging time 2.5 months. Under these conditions, the liquor was clear and transparent, with mellow taste in mouth and refreshing after taste. At the same time, coconut gave elegant coconut flavor to the finished liquor, which improved the quality of the Chi flavor Baijiu.
[1] 金佩璋, 袁艳雯.毛细管直接进样测定豉香型白酒中高沸点香味物质[J].酿酒科技, 2002 (1):68-69;71.
JIN P Z, YUAN Y W.Direct sample injection in capillary to determine high boiling point flavoring components in fermented soybean-flavor liquor[J].Liquor-Making Science & Technology, 2002 (1):68-69;71.
[2] 谭莹, 陈炳荣, 梁思宇.一种豉香型白酒酿造新工艺的研究[J].酿酒科技, 2020(3):65-69.
TAN Y, CHEN B R, LIANG S Y.Study on a new production technique of Chixiang Baijiu[J].Liquor-Making Science & Technology, 2020(3):65-69.
[3] 方毅斐. 豉香型白酒中二元酸的形成机制研究[D].广州:华南理工大学,2012.
FANG Y F.Study of formation mechanism on dibasic acid in soybean-flavor liquor[D].Guangzhou:South China University of Technology, 2012.
[4] 李玲芳. 泡酒肥肉成熟指标及高效浸制工艺研究[D].广州:华南理工大学,2018.
LI L F.Study on maturity indicators and high-efficiency techniques of soaking fat pork[D].Guangzhou:South China University of Technology, 2018.
[5] 朱氏黎花. 泡酒肥肉高效浸制工艺及催陈技术[D].广州:华南理工大学,2016.
ZHU S L H.Rice wine soaking fat efficient manufacturing and catalytic aging technology[D].Guangzhou:South China University of Technology, 2016.
[6] 黄清意, 李湘銮, 费永涛, 等.陈肉酝浸对豉香型白酒风味影响的研究进展[J].食品与发酵工业, 2020, 46(19):284-288.
HUANG Q Y, LI X L, FEI Y T, et al.Advances on the meat immersion and its effect on Chi flavor Baijiu[J].Food and Fermentation Industries, 2020, 46(19):284-288.
[7] 张五九, 何松贵,韩兴林, 等.豉香型白酒风味成分分析研究[J].酿酒科技, 2010(12):58-64.
ZHANG W J, HE S G, HAN X L, et al.Analysis of flavor components of soybean-flavor liquor[J].Liquor-Making Science & Technology, 2010(12):58-64.
[8] 李丹丹, 蒲丽, 罗章.气相色谱法测定不同产地发酵藏猪肉中脂肪酸[J].高原农业, 2020, 4(1):63-68;88.
LI D D, PU L, LUO Z.Determination of fatty acids in fermented Tibetan pork from different regions by gas chromatography[J].Journal of Plateau Agriculture, 2020, 4(1):63-68;88.
[9] 孙晓菊. 十八碳不饱和脂肪酸对乳腺上皮细胞脂肪代谢的影响及其机制研究[D].呼和浩特:内蒙古农业大学, 2012.
SUN X J.Effects of C18 unsaturated fatty acids on lipid metabolism and its mechanisms in mammary epithelial cells[D].Hohhot:Inner Mongolia Agricultural University, 2012.
[10] 刘幼强, 陈燕玲, 刘益新, 等.一种提高豉香型白酒风味并促进其老熟的方法: CN108342288A[P].2018-07-31.
LIU Y Q, CHEN Y L, LIU Y X, et al.A method of improving the flavor and aging of Chi-flavor Baijiu:CN108342288A[P].2018-07-31.
[11] 薛栋升, 梁龙元.一种类豉香型白酒的酿造方法:CN201610067394.1[P].2016-03-30.
XUE D S, LIANG L Y.A brewing method of Similar to Chi-flavor Baijiu:CN201610067394.1[P].2016-03-30.
[12] 刘建福. 椰奶花生颗粒饮料的研制[J]. 食品工业科技, 2005, 26(3):141-142.
LIU J F. The development of Cocosnu cifera and peanut and milk drink[J]. Science and Technology of Food Industry, 2005, 26(3):141-142.
[13] 施祥, 张国.鲜椰肉制油工艺探讨[J].粮食与食品工业, 2018, 25(1):7-8.
SHI X, ZHANG G.Discussion on the process of making oil from fresh coconut[J].Cereal and Food Industry, 2018, 25(1):7-8.
[14] 康尔歌, 赵晋府, 孟旭.椰肉成分的测定及相关比较[J].广州食品工业科技, 2002, 18(4):48-49.
KANG E G, ZHAO J F, MENG X.Determination and comparison of components of coconut meat[J].Guangzhou Food Science and Technology, 2002, 18(4):48-49.
[15] 吴晶晶, 郎春秀, 王伏林,等.我国食用植物油的生产开发现状及其脂肪酸组成改良进展[J].中国油脂, 2020, 45(5):4-10.
WU J J, LANG C X,WANG F L, et al.Production and development status of edible vegetable oils and improvement progresses of their fatty acid compositions in China[J].China Oils and Fats, 2020, 45(5):4-10.
[16] 靳敏, 夏玉宇.食品检验技术[M].北京:化学工业出版社, 2003.
JIN M, XIA Y Y.Food Inspection Technology[M].Beijing:Chemical Industry Press, 2003.
[17] 马夏军, 洪爱华, 梁智渊,等.中国南海总状蕨藻中脂肪酸和甾醇GC-MS分析[J].广东化工, 2005, 32(4):19-21.
MA X J, HONG A H, LIANG Z Y, et al.Analysis of the fatty acid and sterol in Caulerpa racemosa by GC -MS[J].Guangdong Chemical Industry, 2005, 32(4):19-21.
[18] 薄海波, 王霞, 翟宗德,等.碱催化法衍生化气相色谱-质谱法分析青海湖裸鲤鱼油中的脂肪酸[J].色谱, 2006, 24(2):181-184.
BO H B, WANG X, ZHAI Z D, et al.Analysis of fatty acids in Gymnocyprisp rzewalskii oil by gas chromatography-mass spectrometry with base-catalyzed transesterification[J].Chinese Journal of Chromatography, 2006, 24(2):181-184.
[19] 耿薇. 新鲜椰子果肉脂肪酸成分的GC-MS分析[J].广东化工, 2010, 37(1):122-123.
GENG W.The study on the fatty acid compositions in fresh flesh of coconut by GC-MS[J].Guangdong Chemical Industry, 2010, 37(1):122-123.
[20] NUENS Â A, BUCCINI D F, DOS SANTOS JAQUES J A, et al.Effect of dietary Acrocomia aculeata kernel oil rich in medium chain fatty acids on type 2 diabetic rats[J].Journal of Functional Foods,2020,75:104 295.
[21] 范海燕, 范文来, 徐岩.应用GC-O和GC-MS研究豉香型白酒挥发性香气成分[J].食品与发酵工业, 2015,41(4):147-152.
FAN H Y, FAN W L, XU Y.Characetrization of volatile aroma components in Chinese Chixiang aroma type liquor by GC-O and GC-M[J].Food and Fermentation Industries, 2015,41(4):147-152.