Effects of different fixation methods on flavoring substances of Rosa roxburghii Tratt leaves tea

  • TU Qing ,
  • CHEN Qiuhui ,
  • MU Xian ,
  • LU Hongmei ,
  • YANG Shuangquan ,
  • CHEN Li ,
  • HUANG Yongguang
Expand
  • 1(Guizhou Key Lab of Fermentation and Biological Pharmacy, Guizhou University, Guiyang 550025, China)
    2(School of Liquor and Food Engineering, Guizhou University, Guiyang 550025, China)
    3(School of Chemistry and Chemical Engineering, Guizhou University, Guiyang 550025, China)

Received date: 2023-06-04

  Revised date: 2023-06-27

  Online published: 2023-11-20

Abstract

Rosa roxburghii Tratt leaves contain a variety of nutritional functional components, which have good development and utilization value. Rosa roxburghii Tratt leaves tea is a substitute tea prepared by green tea technology from the spring leaves of Rosa roxburghii Tratt leaves. It has good taste and health care effects. The flavor of the tea is one of the main sensory characteristics to reflect the quality of tea, and the production technology will have a certain influence on the formation of tea flavor substances. To explore the influence of different fixation methods on the flavor substances of Rosa roxburghii Tratt leaves tea, headspace solid phase microextraction-gas chromatography-mass spectrometry and electronic tongue were used to study the differences of flavor substances in three different fixation methods, including microwave fixation (WB), steam fixation (ZQ), and thermal fixation (RL). Results showed that WB samples had the strongest bitter, umami, and saltiness, and the weakest sour and astringent taste. ZQ samples had moderate sour, astringent, umami, and saltiness, and the weakest bitter taste. RL samples had the strongest sour and astringent taste, moderate bitter taste, and the weakest umami and saltiness. 213 (WB), 205 (ZQ), and 209 (RL) volatile flavor compounds were identified from Rosa roxburghii Tratt leaves tea prepared by different fixation methods, and aldehydes, alanes, and alcohols were the main flavor compounds. Based on odor activity value analysis, 35 aroma compounds were selected that had a great impact on the aroma of Rosa roxburghii Tratt leaves tea. Through principal component analysis of 35 aroma substances, it was determined that dodecyl alcohol was the key aroma component of WB sample, acetophenone was the key aroma component of ZQ sample, linalool and acetaldehyde were the key aroma component of RL sample. According to the results of various studies, microwave fixation is more suitable for the preparation of Rosa roxburghii Tratt leaves tea. The results provided a theoretical reference for flavor chemistry research and product development of Rosa roxburghii Tratt leaves tea.

Cite this article

TU Qing , CHEN Qiuhui , MU Xian , LU Hongmei , YANG Shuangquan , CHEN Li , HUANG Yongguang . Effects of different fixation methods on flavoring substances of Rosa roxburghii Tratt leaves tea[J]. Food and Fermentation Industries, 2023 , 49(20) : 140 -150 . DOI: 10.13995/j.cnki.11-1802/ts.036360

References

[1] 李欣燃,朱淼,韩世明,等.刺梨叶总黄酮超声辅助提取工艺优化[J].食品研究与开发,2019,40(12):189-193.
LI X R, ZHU M, HAN S M, et al.Optimization of ultrasonic-assisted extraction of flavonoids from Rosa roxburghii leaves[J].Food Research and Development, 2019,40(12):189-193.
[2] 王媛媛,雷艳,马雪,等.刺梨叶质量标准研究[J].中国药业,2019,28(13):36-38.
WANG Y Y, LEI Y, MA X, et al.Quality standard of Rosa Roxburghii leaves[J].China Pharmaceuticals, 2019,28(13):36-38.
[3] 李福明,汪洋,韦敏.刺梨叶醇提物体外抗氧化活性和α-葡萄糖苷酶抑制活性研究[J].中国现代应用药学,2015,32(6):685-688.
LI F M, WANG Y, WEI M.Study on in vitro antioxidant and α-glucosidase inhibitory activities of ethanol extract from Rosae roxburghii leaves[J].Chinese Journal of Modern Applied Pharmacy, 2015,32(6):685-688.
[4] 樊卫国,周禹佳.刺梨叶、花瓣和果实的多酚及三萜组分、含量及其提取物的抗氧化特性[J].贵州大学学报(自然科学版), 2022,39(5):13-21.
FAN W G, ZHOU Y J.Composition and content of polyphenols and triterpenoids in leaves, petals and fruits of Rosa roxburghii and antioxidant properties of their extracts[J].Journal of Guizhou University (Natural Sciences), 2022,39(5):13-21.
[5] 汪庆华,刘新.解读代用茶行业标准及存在的问题[J].茶叶,2019,45(2):90-92.
WANG Q H, LIU X.Interpretation of herbal tea industry standards and existing problems[J].Journal of Tea, 2019,45(2):90-92.
[6] 宋勤飞,杨琦宏,牛素贞,等.原料嫩度和加工工艺对刺梨叶茶品质的影响[J].南方农业,2022,16(9):214-219.
SONG Q F, YANG Q H, NIU S Z, et al.Effects of raw material tenderness and processing technology on the quality of Rosa roxburghii Tratt leaves tea[J].South China Agriculture, 2022,16(9):214-219.
[7] 宋勤飞,牛素贞,杨琦宏,等.不同加工工艺下刺梨叶茶品质研究与评价[J].农产品加工,2022(9):32-37.
SONG Q F, NIU S Z, YANG Q H, et al.Study and evaluation on quality of Rosa roxburghii leaves tea with different processing technology[J].Farm Products Processing, 2022(9):32-37.
[8] ZHAO P Q, WANG J D, YAN X Y, et al.Functional chitosan/zein films with Rosa roxburghii Tratt leaves extracts prepared by natural deep eutectic solvents[J].Food Packaging and Shelf Life,2022,34:101001.
[9] 张倩,徐丽萍,高新鹏,等.3种不同加工方式对桑叶茶挥发性成分的影响[J].食品安全质量检测学报,2023,14(2):307-315.
ZHANG Q, XU L P, GAO X P, et al.Effects of 3 kinds of different processing methods on volatile components of mulberry leaf tea[J].Journal of Food Safety and Quality, 2023,14(2):307-315.
[10] 吴全金,周喆,漆思雨,等.炭焙和电焙白茶的关键风味物质和品质差异[J/OL].食品科学,2023.http://kns.cnki.net/kcms/detail/11.2206.TS.20221229.1856.005.html
WU Q J, ZHOU Z, QI S Y, et al.Analysis of the difference of key flavor substances and quality between charcoal-baked and electric-baked white tea[J/OL].Food Science,2023.http://kns.cnki.net/kcms/detail/11.2206.TS.20221229.1856.005.html.
[11] 邵淑贤,王淑燕,王丽,等.基于ATD-GC-MS技术的不同品种白牡丹茶香气成分分析[J].食品工业科技,2022,43(1):261-268.
SHAO S X, WANG S Y, WANG L, et al.Analysis of aroma components of different cultivars of white peony tea based on ATD-GC-MS[J].Science and Technology of Food Industry, 2022,43(1):261-268.
[12] 王永伦,李兴,杨苗,等.干燥方式对真姬菇菌柄和菌盖挥发性风味物质的影响[J].食品科学,2023,44(8):268-276.
WANG Y L, LI X, YANG M, et al.Effect of drying methods on volatile flavor compounds of the pileus and stipe of Hypsizygus marmoreus[J]. Food Science, 2023,44(8):268-276.
[13] 朱文政,严顺阳,徐艳,等.顶空固相微萃取-气质联用分析不同烹制时间红烧肉挥发性风味成分[J].食品与发酵工业,2021,47(2):247-253.
ZHU W Z, YAN S Y, XU Y, et al.Analysis of volatile flavor components of braised pork with different cooking time by SPME-GC-MS[J].Food and Fermentation Industries, 2021,47(2):247-253.
[14] 王星月,杨潇然,张紫涵,等.赶黄草叶茶制备工艺及其对风味、功效成分溶出的影响[J].中国食品学报,2022,22(2):241-252.
WANG X Y, YANG X R, ZHANG Z H, et al.Preparation technology of penthorum Chinense leaf tea and its effect on flavor and dissolution of effective components[J].Journal of Chinese Institute of Food Science and Technology, 2022,22(2):241-252.
[15] 侯晓慧,张婷,张萌,等.基于GC-IMS和HS-SPME-GC-MS分析泾阳茯砖茶的特征风味物质[J/OL].食品科学,2022.http://kns.cnki.net/kcms/detail/11.2206.ts.20221104.1710.014.html.
HOU X H, ZHANG T, ZHANG M, et al.Identification of characteristic flavor substances of Jingyang Fu Brick tea based on GC-IMS and HS-SPME-GC-MS[J/OL]. Food Science,2022.http://kns.cnki.net/kcms/detail/11.2206.ts.20221104.1710.014.html.
[16] 罗红玉,王奕,谷雨,等.干燥工艺对重庆沱茶及其毛茶风味品质的影响[J].食品科学,2022,43(22):259-266.
LUO H Y, WANG Y, GU Y, et al.Effect of drying process on the flavor quality of Chongqing Tuo tea and crude tea for making it[J].Food Science, 2022,43(22):259-266.
[17] 邵淑贤,徐梦婷,林燕萍,等.基于电子鼻与HS-SPME-GC-MS技术对不同产地黄观音乌龙茶香气差异分析[J].食品科学,2023,44(4):232-239.
SHAO S X, XU M T, LIN Y P, et al.Differential analysis of aroma components of Huangguanyin Oolong tea from different geographical origins using electronic nose and headspace solid-phase microextraction-gas chromatography-mass spectrometry[J]. Food Science, 2023,44(4):232-239.
[18] 刘倩,袁越,张杰,等.不同菌种发酵对诺丽果酵素的抗氧化性及风味物质的影响[J].食品工业科技,2023,44(4):129-137.
LIU Q, YUAN Y, ZHANG J, et al.Effects of different fermentation strains on the antioxidant activities and flavor substances of Morinda citrifolia L.(Noni) fruit jiaosu[J].Science and Technology of Food Industry, 2023,44(4):129-137.
[19] 陆晨浩, 王曦如, 仲梦涵, 等.基于GC-MS和电子感官技术分析发芽对黑麦茶风味的影响[J].食品科学, 2020, 41(10):192-197.
LU C H, WANG X R, ZHONG M H, et al.Effects of germination on the flavor of rye tea as evaluated by GC-MS and electronic sensor techniques[J].Food Science, 2020, 41(10):192-197.
[20] 马园园,曹青青,高一舟,等.绿茶苦味研究进展[J].茶叶科学,2023,43(1):1-16.
MA Y Y, CAO Q Q, GAO Y Z, et al.Research progress on the bitterness of green tea[J].Journal of Tea Science, 2023,43(1):1-16.
[21] 刘忠英,冉乾松,潘科,等.基于电子舌的3种氨基酸单体呈味特性研究[J].食品科技,2022,47(4):296-302.
LIU Z Y, RAN Q S, PAN K, et al.Flavor characteristics of three amino acid monomers based on electronic tongue[J].Food Science and Technology, 2022,47(4):296-302.
[22] ZHAO C J, SCHIEBER A, GÄNZLE M G.Formation of taste-active amino acids, amino acid derivatives and peptides in food fermentations—A review[J].Food Research International, 2016, 89:39-47.
[23] 黄东竹,李梦茹,陈琪,等.绿茶香气及茶叶中香气物质提取与检测方法研究进展[J].茶叶通讯,2021,48(4):589-597;605.
HUANG D Z, LI M R, CHEN Q, et al.Research progress on aroma of green tea and extraction and detection methods of aroma substances in green tea[J].Journal of Tea Communication, 2021,48(4):589-597;605.
[24] 黎轩铭,李洪军,肖旭,等.挂糊油炸大球盖菇菌柄加工过程中挥发性风味物质变化研究[J].食品与发酵工业,2023,49(16):68-75.
NI X M, LI H J, XIAO X, et al.Study on the change of volatile flavor substances during the processing of deepfried and battered mushroom stalks of Stropharia rugoso-annulata[J].Food and Fermentation Industries,2023,49(16):68-75.
[25] 李欢康,杨佳玮,刘文玉,等.不同工艺核桃油挥发性物质比对及关键香气成分表征[J].食品科学,2021,42(16):185-192.
LI H K, YANG J W, LIU W Y, et al.Comparison of volatile components and characterization of key aroma components of walnut oil produced by different processes[J].Food Science, 2021,42(16):185-192.
[26] 吴艳艳. 黄茶、白茶的化学成分研究[D].大连:辽宁师范大学,2013.
WU Y Y.The research on the composition of Yellow tea and White tea[D].Dalian:Liaoning Normal University,2013.
[27] 郭雯飞,孟小环,罗永此,等.白牡丹与白毫银针香气成分的研究[J].茶叶,2007,33(2):78-81.
GUO W F,MENG X H, LUO Y C, et al.Analysis of the volatile constituents in the baimudan tea and Baihaoyinzhen tea[J].Journal of Tea, 2007,33(2):78-81.
[28] PHAM A J, SCHILLING M W, MIKEL W B, et al.Relationships between sensory descriptors, consumer acceptability and volatile flavor compounds of American dry-cured ham[J].Meat Science,2008,80(3):728-737.
[29] SABIO E, VIDAL-ARAGÓN M C, BERNALTE M J, et al.Volatile compounds present in six types of dry-cured ham from south European countries[J].Food Chemistry,1998,61(4):493-503.
[30] MAHDI G V, CONSTANTIN A, JESUS L, et al.Potential use of electronic noses, electronic tongues and biosensors as multisensor systems for spoilage examination in foods[J].Trends in Food Science & Technology,2018,80:71-92.
[31] MARUŠIĆ N, PETROVIĆ M, VIDAČEK S, et al.Characterization of traditional istrian dry-cured ham by means of physical and chemical analyses and volatile compounds[J].Meat Science, 2011, 88(4):786-790.
[32] 林良静,蔡惠钿,包涵,等.潮汕特色佛手香黄的特征挥发性风味成分分析[J].现代食品科技,2021,37(7):238-249.
LIN L J, CAI H T, BAO H, et al.Analysis of the characteristic volatile flavor components of preserved Lao-Xiang-Huang of Chaozhou[J].Modern Food Science and Technology, 2021,37(7):238-249.
[33] 尤秋爽,石亚丽,朱荫,等.不同加工工艺对绿茶关键呈香成分的影响[J/OL].食品科学,2022.http://kns.cnki.net/kcms/detail/11.2206.TS.20221110.2102.022.html.
YOU Q S, SHI Y L, ZHU Y, et al.Influence of different manufacturing processes on the key aroma-active compounds of green tea[J/OL].Food Science,2022.http://kns.cnki.net/kcms/detail/11.2206.TS.20221110.2102.022.html.
[34] 田维芬,周君,明庭红,等.基于电子鼻和GC-MS的不同品牌橄榄油挥发性风味物质研究[J].食品工业科技,2017,38(7):285-292.
TIAN W F, ZHOU J, MING T H, et al.Analysis of volatile flavor components from different regions of olive oil by electronic nose and gas chromatography technology[J].Science and Technology of Food Industry, 2017,38(7):285-292.
[35] 李芳. 硬脂鱼油的品质特征及在火锅底料中的应用研究[D].重庆:西南大学,2021.
LI F.Study on the quality characteristics of fish oil stearin and its application in hotpot seasoning[D].Chongqing:Southwest University, 2021.
Outlines

/