Abstract: Lemon juice and coconut water were used as raw materials, these two kinds of juice were mixed and fermented in different proportions to find the optimal condition for compound fruit wine fermentation. The results of sensory evaluation showed that the fermented wine mixed with lemon juice and coconut water with a volume ratio of 1:3 had a more coordinated and balanced aroma, with higher acidity, suitable for brewing sweet fruit wine; the wine fermented with a juice volume ratio of 1:7.5 had delicate fruity aroma, elegant lemon aroma, prominent coconut aroma, refreshing and balanced taste, suitable for brewing dry fruit wine. The aroma components of lemon juice, lemon wine, coconut water, coconut wine and 1:3, 1:7.5 mixed fermented wine were detected by headspace-solid-phase micro-extraction coupled with gas chromatography-mass spectrometry. Four kinds of aroma were obtained by principal component analysis: lemon-based mixed aroma, coconut-based fruity aroma, mixed aroma and lemon-fermented aroma. The characteristic aromas of lemon-coconut complex fruit wine were (-)-4-terpineol, (+)-α-terpineol, isoamyl alcohol, 1,1-diethoxyethane, 2-methylbutanol, linalool, ethyl pelargonate, 2-tetrazol, ethyl benzoate and pinene. These aromas gave the lemon-coconut complex fruit wine a unique flavor.
[1] 涂勋良. 四川安岳8个柠檬品种果实主要有机组分分析研究[D].雅安:四川农业大学,2016. TU X L.Study on analysis of main organic components in fruits of eight lemon(Citrus limon Lindl) cultivars from Anyue county, Sichuan province[D].Ya'an:Sichuan Agricultural University,2016. [2] 张瑶,蒲彪,刘云.柠檬果汁酶解前后香气成分比较研究[J].饮料工业,2009,12(2):40-44. ZHANG Y, PU B, LIU Y.Study on and comparison of aromatic components in lemon juice before and after enzymolysis by GC-MS[J].The Beverage Industry,2009,12(2):40-44. [3] 康尔歌. 椰肉椰水成分及其加工的研究(附年产3000吨椰汁工厂设计)[D].天津:天津科技大学,2003. KANG E G.Study on constituents and processing of coconut meat and water(and design of plant annual output of 3000 ton)[D].Tianjin:Tianjin University of Science and Technology,2003. [4] 张辉. 椰果露酒加工技术及香气成分的研究[D].长沙:中南林业科技大学,2015. ZHANG H.Studies on processing technique and aroma components of coconut Wine[D].Changsha:Central South University of Forestry and Technology,2015. [5] 余泽红,贺小贤,丁勇,等.固相微萃取在食品挥发性组分测定方面研究进展[J].粮食与油脂,2010(7):44-46. YU Z H, HE X X, DING Y, et al.Research progress on solid phase micro-extraction determination of volatile components in foods[J].Cereals&Oils,2010(7):44-46. [6] 黄江艳,李秀娟,潘思轶.固相微萃取技术在食品风味分析中的应用[J].食品科学,2012,33(7):289-298. HUANG J Y, LI X J, PAN S Y.Application of solid-phase microextraction in food flavor analysis:A review[J].Food Science,2012,33(7):289-298. [7] 李建勋,杜丽平,王超,等.顶空固相微萃取-气相色谱-质谱联用法分析黑茶香气成分[J].食品科学,2014,35(2):191-195. LI J X, DU L P, WANG C, et al.Analysis of aroma compounds in dark teas by head space-solid phase micro-extraction coupled with gas chromatography-mass spectrometry[J].Food Science,2014,35(2):191-195. [8] 李大雷,翁彦如,杜丽平,等.电子鼻和气质联用法分析普洱茶香气成分[J].食品与发酵工业,2019,45(3):237-245. LI D L, WENG Y R, DU L P, et al.Detection of volatile compounds in different brands of Puerh tea using electronic nose and GC-MS[J].Food and Fermentation Industries, 2019,45(3):237-245. [9] 李凯,王金晶,李永仙,等.红心火龙果果酒特征香气分析[J].食品与发酵工业,2019,45(13):217-223. LI K, WANG J J, LI Y X, et al.Characteristic aroma components of red pitaya wine[J].Food and Fermentation Industries, 2019,45(13):217-223. [10] 周琦,易鑫,欧阳祝,等.顶空固相微萃取-气相色谱-质谱联用结合多元统计法分析不同品种温州蜜柑汁的香气成分[J].食品与发酵工业,2020,46(10):248-254. ZHOU Q, YI X, OUYANG Z, et al.Analysis of aroma components in different satsuma juices by HS-SPME-GC-MS combined with multivariate statistical methods[J].Food and Fermentation Industries, 2020,46(10):248-254. [11] ZHANG W T, DONG P, LAO F, et al.Characterization of the major aroma-active compounds in Keitt mango juice:Comparison among fresh, pasteurization and high hydrostatic pressure processing juices[J].Food Chemistry,2019,289:215-222. [12] 梅明鑫. 沃尔卡姆柠檬酒酿造工艺研究[D].重庆:西南大学,2018. MEI M X.Study on brewing technology of Volkamer lemon wine[D].Chongqing:Southwest University,2018. [13] 潘永波,杨劲松,李虹蕉,等.椰子酒的酿造技术[J].中国酿造,2008(12):109-110. PAN Y B, YANG J S, LI H J, et al.Brewing technique of coconut wine[D], China Brewing,2008(12):109-110. [14] 袁璐,刘四新,陈文学.椰子水腰果梨复合果酒的研制[J].中国酿造,2011(11):186-189. YUAN L, LIU S X, CHENG W X.Production of fruit wine with coconut water and cashew apple juice[J].China Brewing,2011(11):186-189. [15] 尹爱国,曾霞,程水明,等.白桑椹柠檬果酒发酵工艺研究[J].食品研究与开发,2020,41(8):153-159. YIN A G, ZENG X, CHEGN S M, et al.Optimization of brewing technology for White Mulberry-Lemon wine[J].Food Research and Development, 2020,41(8):153-159. [16] JAN H, SWIEGERS I S P.Yeast modulation of wine flavor[J].Adv Appl Microbiol,2005, 57:131-175. [17] 康明丽,潘思轶,范刚,等.柑橘果酒酿造过程中挥发性风味化合物的变化[J].食品科学,2015,36(18):155-161. KANG M L, PAN S Y, FAN G, et al.Changes in volatile compounds in satsuma mandarin wine with different fermentation periods[J].Food Science,2015,36(18):155-161. [18] MA Y, LI S H, YIN X C, et al.Effects of controlled atmosphere on the storage quality and aroma compounds of lemon fruits using the designed automatic control apparatus[J].BioMed Research International 2019(3):1-17. [19] 谢春梅,焦红茹,曹芳玲.宁夏青铜峡小产区不同品种干红葡萄酒的香气成分分析[J].中国酿造,2018,37(1):170-176. XIE C M, JIAO H R, CAO F L.Analysis on aroma components of dry red wines with different varieties of grape from Ningxia Qingtongxia region[J].China Brewing,2018,37(1):170-176. [20] 张涵,鲁周民,王锦涛,等.4种主要柑橘类香气成分比较[J].食品科学,2017,38(4):192-196. ZHANG H, LU Z M, WANG J T, et al.Comparative aroma components of fruits of four main citrus varieties[J].Food Science, 2017,38(4):192-196. [21] TATUM J H, NAGY S, BERRY R E.Degradation products formed in canned single-strength orange juice during storage[J].Journal of Food Science, 1975, 40(4):707-709.