Please wait a minute...
 
 
食品与发酵工业  2021, Vol. 47 Issue (7): 146-152    DOI: 10.13995/j.cnki.11-1802/ts.025710
  生产与科研应用 本期目录 | 过刊浏览 | 高级检索 |
提取方法对马铃薯渣果胶结构特征及特性的影响
杨月娇, 马智玲, 白英*
(内蒙古农业大学 食品科学与工程学院,内蒙古 呼和浩特,010018)
Extraction methods on structure and properties of pectin from potato residue
YANG Yuejiao, MA Zhiling, BAI Ying*
(Food Science and Engineering College,Inner Mongolia Agricultural University,Hohhot 010018,China)
下载:  HTML   PDF (2744KB) 
输出:  BibTeX | EndNote (RIS)      
摘要 对酸处理提取(acid-treated extraction, ATE)、酶处理提取(enzyme-treated extraction, ETE)和盐沉析提取(salt-treated extraction, STE)的马铃薯渣果胶抗氧化活性及其特性进行研究,发现3种提取方法中,STE果胶提取率最高。流变特性结果显示,ATE果胶具有最高的初始黏度。结构特征表明,STE多糖呈光滑致密的块状结构;ETE果胶呈不规则褶皱的形状;ATE多糖呈棉絮片状,较其他2种其表面结构松软。3种多糖的单糖组成各不相同,ATE的果胶主要由葡萄糖、半乳糖、阿拉伯糖以及少量的鼠李糖和木糖组成;ETE的果胶主要的单糖组成为葡萄糖和半乳糖;STE的果胶主要的单糖组成为葡萄糖、半乳糖、阿拉伯糖。ATE果胶(51 481 Da)分子质量最大,其次为ETE果胶(14 593 Da)、STE果胶(11 669 Da)。抗氧化特性显示,ATE果胶表现出较高的清除DPPH自由基的能力,STE具有较高的清除·OH和·O-2的能力。
服务
把本文推荐给朋友
加入引用管理器
E-mail Alert
RSS
作者相关文章
杨月娇
马智玲
白英
关键词:  马铃薯渣  果胶  提取方法    
Abstract: The effects of salt-extraction (STE), acid-treated extraction (ATE), and enzyme-treated extraction (ETE) on the antioxidant activities and characteristics of pectin from potato residue were investigated in this study.Among different methods, the extraction rate of pectin from STE was the highest.And the results of rheological properties showed that ATE pectin had the highest initial viscosity.The STE pectin showed smooth and dense block structure, and ETE pectin exhibited an irregular fold shape;meanwhile, the ATE pectin showed a cotton wadding sheet shape, as observed by scanning electron microscopy (SEM).The surface structure of the ATE pectin was softer than the other two.The monosaccharide composition of the three pectins was different.The pectin of ATE was mainly composed of glucose, galactose, arabinose and a small amount of rhamnose and xylose;the main monosaccharide groups of ETE pectin were glucose and galactose, and STE pectin mainly consisted of glucose, galactose and arabinose.The ATE pectin had the largest molecular weight (51 481 Da), reduced by the order of the ETE pectin (14 593 Da) and STE pectin (11 669 Da).The antioxidant properties showed that ATE pectin showed higher DPPH scavenging ability, and STE had higher scavenging capacity of hydroxyl radical and superoxide anion.
Key words:  potato residue    pectin    extraction methods
收稿日期:  2020-09-19      修回日期:  2020-10-14           出版日期:  2021-04-15      发布日期:  2021-05-20      期的出版日期:  2021-04-15
作者简介:  博士研究生(白英教授为通讯作者,E-mail:baiying77@sina.com)
引用本文:    
杨月娇,马智玲,白英. 提取方法对马铃薯渣果胶结构特征及特性的影响[J]. 食品与发酵工业, 2021, 47(7): 146-152.
YANG Yuejiao,MA Zhiling,BAI Ying. Extraction methods on structure and properties of pectin from potato residue[J]. Food and Fermentation Industries, 2021, 47(7): 146-152.
链接本文:  
http://sf1970.cnif.cn/CN/10.13995/j.cnki.11-1802/ts.025710  或          http://sf1970.cnif.cn/CN/Y2021/V47/I7/146
[1] 张欣萌,吕春茂,孟宪军,等.盐析法制备寒富苹果渣果胶及其抗氧化性研究[J].食品工业科技,2019,40(8):176-182;189.ZHANG X M,LV C M,MENG X J,et al.Study on pectin from Hanfu apple pomace by salting out method and the antioxidation of pectin[J].Science and Technology of Food Industry,2019,40(8):176-182;189.
[2] 刘娜, 黄雪松.果胶的生物活性及其用于包装材料的研究进展[J/OL].食品工业科技:1-11[2020-09-17].http://kns.cnki.net/kcms/detail/11.1759.TS.20200810.1756.018.html.LIU N,HUANG X S.Research progress on bioactivity of pectin and its application in packaging materials[J/OL].Science and Technology of Food Industry:1-11[2020-09-17].
[3] 台建祥,范鸿雁,薛慧,等.菠萝蜜果皮果胶提取工艺的优化[J].食品科技,2014,39(1):236-239.TAI J X,FAN H Y,XUE H,et al.The optimum extraction process of pectin from jackfruit peel[J].Food Science and Technology,2014,39(1):236-239.
[4] 杨希娟,党斌.马铃薯渣中提取果胶的工艺优化及产品成分分析[J].食品科学,2011,32(4):25-30.YANG X J,DANG B.Optimization of pectin extraction from potato pulp and product composition analysis[J].Food Science,2011,32(4):25-30.
[5] 王文霞,张显斌,张慧君,等.不同提取方法对马铃薯果胶多糖组成特性的影响[J].食品与发酵工业,2017,43(12):150-156.WANG W X,ZHANG X B,ZHANG H J,et al.Effect of different extraction methods on the compositions of potato pectin polysaccharides[J].Food and Fermentation Industries,2017,43(12):150-156.
[6] 王锐,黄翔,邓仕英.柑橘皮中果胶的提取研究[J].化工管理,2020(7):36-37.WANG R,HUANG X,DENG S Y.Study on extraction of pectin from citrus peel[J].Chemical Enterprise Management,2020(7):36-37.
[7] 童丹,韩黎明,党雄英.马铃薯渣中提取果胶生产技术研究[J].畜牧兽医杂志,2016,35(5):30-33.TONG D,HAN L M,DANG X Y.A Technical study on the extraction from potato residue[J].Journal of Animal Science and Veteriary Medicine,2016,35(5):30-33.
[8] 李文茜,刘鑫,么恩悦,等.马铃薯渣的开发利用与研究进展[J].饲料工业,2019,40(1):17-22.LI W X,LIU X,YAO E Y,et al.The development,utilization and research progress of potato pulp[J].Feed Industry,2019,40(1):17-22.
[9] 李芳蓉,王英,安志刚.马铃薯渣的资源化开发利用[J].粮食与饲料工业,2018(7):43-48.LI F R,WANG Y,AN Z G.Potato pulp development and resourceful utilization[J].Cereal & Feed Industry,2018(7):43-48.
[10] 傅迎军.马铃薯的营养成份分析及发展前景[J].北方园艺,1996(2):41-42.FU Y J.Analysis and development prospect of potato nutrition component[J].Northern Horticulture,1996(2):41-42.
[11] 许馨予,毛小雨,杨鹄隽,等.天然植物果胶的提取及其在食品工业中的应用现状[J].中国食品添加剂,2020,31(8):115-122.XU X Y,MAO X Y,YANG H J,et al.Extraction of natural plant pectin and its application in food industry[J].China Food Additives,2020,31(8):115-122.
[12] ARACHCHIGE M P M,MU T,MA M.Structural,physicochemical,and emulsifying properties of sweet potato pectin treated by high hydrostatic pressure and/or pectinase:A comparative study[J].Journal of the Science of Food and Agriculture,2020,100(13):4 911-4 920.
[13] LIM S J,CHOI A H,KWON M S,et al.Evaluation of antioxidant activities of various solvent extract from Sargassum serratifolium and its major antioxidant components[J].Food Chemistry,2019,278:178-184.
[14] CHEN X,WU G,HUANG Z.Structural analysis and antioxidant activities of polysaccharides from cultured Cordyceps militaris[J].International Journal of Biological Macromolecules,2013,58:18-22.
[15] JIN L,GUAN X,LIU W,et al.Characterization and antioxidant activity of a polysaccharide extracted from Sarcandra glabra[J].Carbohydrate Polymers,2012,90(1):524-532.
[16] 杭瑜瑜,王玉杰,孙国铮.菠萝皮渣果胶的盐析法提取及理化性质研究[J].中国食品添加剂,2016(7):103-110.HANG Y Y,WANG Y J,SUN G Z.Extraction of pectin from pineapple peels by salting out and its physicochemical properties[J].China Food Additives,2016(7):103-110.
[17] 应姗姗.火龙果皮中果胶提取及改性研究[D].杭州:浙江大学,2014.YING S S.Study on the extraction and modification of pectin from the peel of dragon fruit[D].Hangzhou:Zhejiang university,2014.
[18] ABOU ZEID A H,ABOUTABL E A,SLEEM A A,et al.Water soluble polysaccharides extracted from Pterocladia capillacea and Dictyopteris membranacea and their biological activities[J].Carbohydrate Polymers,2014,113:62-66.
[19] SUN R C,TOMKINSON J.Characterization of hemicelluloses obtained by classical and ultrasonically assisted extractions from wheat straw[J].Carbohydrate Polymers,2002,50(3):263-271.
[20] SUN L,WANG L,ZHOU Y.Immunomodulation and antitumor activities of different-molecular-weight polysaccharides from Porphyridium cruentum[J].Carbohydrate Polymers,2012,87(2):1 206-1 210.
[21] SHENG J,SUN Y.Antioxidant properties of different molecular weight polysaccharides from Athyrium multidentatum (Doll.) Ching[J].Carbohydrate Polymers,2014,108:41-45.
[22] HU Z Y,WANG P H,ZHOU H L,et al.Extraction,characterization and in vitro antioxidant activity of polysaccharides from Carex meyeriana Kunth using different methods[J].International Journal of Biological Macromolecules,2018,120:2 155-2 164.
[23] KANMANI P,KUMAR R S,YUVARAJ N,et al.Production and purification of a novel exopolysaccharide from lactic acid bacterium Streptococcus phocae PI80 and its functional characteristics activity in vitro[J].Bioresour Technol,2011,102(7):4 827-4 833.
[24] SANANDIYA NARESH D,SIDDHANTA A K.Chemical studies on the polysaccharides of Salicornia brachiata.[J].Carbohydrate polymers,2014,112:300-307.
[25] MARÉCHAL Y.Observing the water molecule in macromolecules using infrared spectrometry:Structure of the hydrogen bond network and hydration mechanism[J].Journal of Molecular Structure,2003,700(1):217-223.
[26] 潘润森,张丽芬,陈复生.超声波协同钙浸渍处理对草莓果胶结构特性的影响[J].河南工业大学学报(自然科学版),2019,40(2):9-14.PAN R S,ZHANG L F,CHEN F S.Effect of ultrasound combined with calcium impregnation treatment on structural properties of strawberry pectin[J].Journal of Henan University of Technology(Natural Science Edition),2019,40(2):9-14.
[27] LIN L,XIE J,LIU S,et al.Polysaccharide from Mesona chinensis:Extraction optimization,physicochemical characterizations and antioxidant activities[J].International Journal of Biological Macromolecules,2017,99:665-673.
[28] MOLLET J C,RAHAOUI A,LEMOINE Y.Yield,chemical composition and gel strength of agarocolloids of Gracilaria gracilis,Gracilariopsis longissima and the newly reported Gracilaria cf.vermiculophylla from Roscoff (Brittany,France)[J].Journal of Applied Phycology,1998,10(1):59.
[29] SATHIYANARAYANAN G,VIGNESH V,SAIBABA G,et al.Synthesis of carbohydrate polymer encrusted gold nanoparticles using bacterial exopolysaccharide:A novel and greener approach[J].RSC Advances,2014,4(43):22 817.
[30] 白英,刘乃齐.Enterococcus faecium AS8及其胞外多糖对发酵乳流变学特性的影响[J].食品科学,2019,40(10):70-76.BAI Y,LIU N Q.Rheological properties of fermented milk as affected by addition of Enterococcus faecium AS8 and its exopolysaccharides[J].Food Science,2019,40(10):70-76.
[31] 田玉霞,乔书涛,仇农学,等.不同分子量级苹果果胶的流变性评价[J].陕西师范大学学报(自然科学版),2010,38(1):104-108.TIAN Y X,QIAO S T,QIU N X,et al.Rheological properties of apple pectins with different molecular weights[J].Journal of Shaanxi Normal University(Natural Science Edition),2010,38(1):104-108.
[32] QIN Y,YUAN F,PAN Y X,et al.Structural characterization,antioxidant activity,and antiglycation activity of polysaccharides from different chrysanthemum teas[J].RSC Advances,2019,9(61):35 443-35 451.
[33] LIU Y,ZHOU Y,LIU M,et al.Extraction optimization,characterization,antioxidant and immunomodulatory activities of a novel polysaccharide from the wild mushroom Paxillus involutus[J].International Journal of Biological Macromolecules,2018,112:326-332.
[34] YU Y,SHEN M Y,SONG Q Q,et al.Biological activities and pharmaceutical applications of polysaccharide from natural resources:A review[J].Carbohydrate Polymers,2018,183.
[35] CHEN F,HUANG G L,YANG Z Y,et al.Antioxidant activity of Momordica charantia polysaccharide and its derivatives[J].International Journal of Biological Macromolecules,2019,138:673-680.
[1] 刘昕, 张驰, 薛艾莲, 赵吉春, 曾凯芳, 明建. 超声-酶法提取的豆腐柴低酯果胶理化性质及结构表征[J]. 食品与发酵工业, 2021, 47(8): 108-115.
[2] 牟方婷, 袁美, 石黎琳, 曾凡坤, 陈嘉, 张玉. 超声和微波辅助果胶酶处理对果胶结构的影响[J]. 食品与发酵工业, 2021, 47(4): 215-221.
[3] 王文霞, 杨悦, 张慧君, 刘博, 徐婷婷. 马铃薯果胶流变特性的研究[J]. 食品与发酵工业, 2021, 47(2): 63-69.
[4] 宋煜婷, 王晓芸, 丁筑红, 陈思奇, 杜勃峰, 肖仕芸, 余奕宏, 王翼. 外源菌种和辅助碳源发酵糟辣椒条件优化与品质分析评价[J]. 食品与发酵工业, 2020, 46(3): 131-137.
[5] 吴丽, 冯敏, 尤琳烽. 果胶-壳聚糖聚合物用于制备结肠靶向空心胶囊的工艺研究[J]. 食品与发酵工业, 2020, 46(22): 196-201.
[6] 彭志杰, 杜娇, 张羽婷, 郭东东, 雷佳钰, 耿雪冉, 孟俊龙, 常明昌. 提取方法对灰树花粗蛋白结构及功能特性的影响[J]. 食品与发酵工业, 2020, 46(21): 161-166.
[7] 顾雅昕, 乔柱, 郭行, 王欣, 伊扬磊, 单媛媛, 刘变芳, 周元, 吕欣. 发酵乳杆菌LBM97所产细菌素提取方法的优化及比较[J]. 食品与发酵工业, 2020, 46(19): 111-116.
[8] 白英, 杨月娇, 谢瑞鹏. 果胶-乳清蛋白混合比例和pH值对体系流变学特性的影响[J]. 食品与发酵工业, 2020, 46(18): 61-66.
[9] 陈露, 嵇晶, 金佳颖, 郑丽杰, 韩威, 王欣之, 刘睿, 吴皓. 高效液相色谱-电感耦合等离子体质谱法测定海藻中5种砷形态[J]. 食品与发酵工业, 2020, 46(15): 270-275.
[10] 丁宁, 艾连中, 赖凤羲, 张汇, 宋子波. 百香果皮果胶的分子特征及Ca2+与Zn2+致流变变化的研究[J]. 食品与发酵工业, 2020, 46(14): 77-84.
[11] 任佳琦, 刘昕, 雷琳, 赵吉春, 曾凯芳, 明建. 苹果中有机酸-果胶复合体系的理化特性及稳定性[J]. 食品与发酵工业, 2020, 46(12): 29-36.
[12] 黎英, 周荣池, 刘夏蕾, 梁月霜, 罗正成, 汪美珍. 百香果皮果胶的理化及凝胶特性[J]. 食品与发酵工业, 2020, 46(12): 140-146.
[13] 李帅, 艾连中, 张汇, 宋子波, 赖凤羲. 百香果果胶及其辛烯基琥珀酸酯化物对酸化脱脂乳饮料稳定性的影响[J]. 食品与发酵工业, 2020, 46(11): 151-156.
[14] 郑炯, 余彬彬, 曾瑞琪, 张甫生. 不同盐离子对豌豆淀粉/低酯果胶复配体系理化特性的影响[J]. 食品与发酵工业, 2019, 45(7): 101-108.
[15] 刘江, 张诗琪, 雷激, 苏菲烟, 任倩. 柠檬皮渣干燥工艺探讨[J]. 食品与发酵工业, 2019, 45(7): 242-249.
No Suggested Reading articles found!
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
版权所有 © 《食品与发酵工业》编辑部
地址:北京朝阳区酒仙桥中路24号院6号楼111室
本系统由北京玛格泰克科技发展有限公司设计开发  技术支持:support@magtech.com.cn