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食品与发酵工业  2021, Vol. 47 Issue (16): 181-187    DOI: 10.13995/j.cnki.11-1802/ts.026389
  生产与科研应用 本期目录 | 过刊浏览 | 高级检索 |
乳清分离蛋白-普鲁兰多糖复合气凝胶的制备及性能优化
曹庆龙1, 雷桥1,2,3*, 吴浩1, 高文婧1
1(上海海洋大学 食品学院,上海,201306)
2(上海水产品加工及贮藏工程技术研究中心,上海,201306)
3(农业部水产品贮藏保鲜质量安全风险评估实验室(上海),上海,201306)
Preparation and performance optimization of whey protein isolate pullulan composite aerogel
CAO Qinglong1, LEI Qiao1,2,3*, WU Hao1, GAO Wenjing1
1(College of Food Science and Technology, Shanghai Ocean University, Shanghai 201306, China)
2(Shanghai Engineering Research Center of Aquatic-Product Processing & Preservation, Shanghai 201306, China)
3(Laboratory of Quality and Safety Risk Assessment for Aquatic Products on Storage and Preservation(Shanghai), Ministry of Agriculture, Shanghai 201306, China)
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摘要 采用响应面法对乳清分离蛋白(whey protein isolate,WPI)-普鲁兰多糖(pullulan,PUL)复合气凝胶的制备进行优化,测试并分析了其吸湿性、抗压性能、微观结构、热力学性能及精油装载释放性能,旨在探求多糖-蛋白类气凝胶在装载及缓释领域的可行性。结果表明,最优制备条件为PUL添加量55 mg/mL, pH值7.9,凝胶温度84 ℃。该条件下制得的复合气凝胶样品对丁香精油有着良好的装载性能及缓释性能,最大装载率为254.23%。蒸馏水中,最大释放率为48.94%;95%(体积分数)乙醇中,最大释放率为65.59%。平衡吸湿率为11.41%。装载丁香精油前压缩模量21.745 MPa,有着较好的抗压性能,装载后压缩模量仍有11.247 MPa,可满足正常应用需求。
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曹庆龙
雷桥
吴浩
高文婧
关键词:  乳清分离蛋白  普鲁兰多糖  复合气凝胶  丁香精油  制备条件优化    
Abstract: The aim of this study was to explore the feasibility of polysaccharide-protein aerogels in loading and sustained release fields. Response surface methodology was used to optimize the preparation of whey protein isolate (WPI)-pullulan (PUL) composite aerogels. And the hygroscopicity, compressive properties, microstructure, thermodynamic properties and essential oil loading and releasing properties of the aerogels were tested and analyzed. The results showed that the optimum preparation conditions were with the PUL addition of 55 mg/mL at pH 7.9 and the gel temperature was 84 ℃. Under these conditions, the composite aerogel samples had good loading properties and sustained releasing properties for clove essential oil, and the maximum loading rate was 254.23%. Furthermore, the maximum release rate was 48.94% in distilled water and 65.59% in 95% ethanol. The equilibrium moisture was 11.41%. And the compression modulus was 21.745 MPa of clove essential oil, and after loading it was 11.247 MPa, which can meet the normal application requirements.
Key words:  whey protein isolate    pullulan    composite aerogel    clove essential oil    preparation conditions optimization
收稿日期:  2020-12-07      修回日期:  2021-01-14                发布日期:  2021-09-10      期的出版日期:  2021-08-25
基金资助: 上海市教育委员会产学研项目(15cyx69)
作者简介:  硕士研究生(雷桥副教授为通讯作者,E-mail:qlei@shou.edu.cn)
引用本文:    
曹庆龙,雷桥,吴浩,等. 乳清分离蛋白-普鲁兰多糖复合气凝胶的制备及性能优化[J]. 食品与发酵工业, 2021, 47(16): 181-187.
CAO Qinglong,LEI Qiao,WU Hao,et al. Preparation and performance optimization of whey protein isolate pullulan composite aerogel[J]. Food and Fermentation Industries, 2021, 47(16): 181-187.
链接本文:  
http://sf1970.cnif.cn/CN/10.13995/j.cnki.11-1802/ts.026389  或          http://sf1970.cnif.cn/CN/Y2021/V47/I16/181
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