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食品与发酵工业  2021, Vol. 47 Issue (24): 56-63    DOI: 10.13995/j.cnki.11-1802/ts.027271
  研究报告 本期目录 | 过刊浏览 | 高级检索 |
不同产地枸杞品质差异研究
李曼祎1,2, 沈天辰1,2, 刘春凤1,2, 郑飞云1,2, 钮成拓1,2, 李崎1,2, 王金晶1,2*
1(江南大学 工业生物技术教育部重点实验室(生物工程学院),江苏 无锡,214122)
2(江南大学 酿酒科学与技术实验室,江苏 无锡,214122)
Research on the quality of wolfberry from different production areas
LI Manyi1,2, SHEN Tianchen1,2, LIU Chunfeng1,2, ZHENG Feiyun1,2, NIU Chengtuo1,2, LI Qi1,2, WANG Jinjing1,2*
1(The Key Laboratory of Industrial Biotechnology, Ministry of Education School of Biotechnology, Jiangnan University, Wuxi 214122, China)
2(Laboratory of Brewing Science and Technology, Jiangnan University, Wuxi 214122, China)
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摘要 该文以宁夏、新疆、青海、内蒙古4个产地枸杞为研究对象,对其理化指标、活性物质含量及风味化合物进行测定,以期为枸杞品质评价及产地鉴别提供参考。结果表明,不同产地枸杞理化指标存在一定差异,宁夏及青海产区枸杞生物活性物质含量处于较高水平。气相离子色谱结合偏最小二乘法判别分析结果表明,四产地枸杞大多数挥发性有机物种类相同,但有16种物质在地区之间有较大的含量差异。正丙醇为内蒙古地区枸杞的特有物质,可用于鉴别内蒙古枸杞。糠醛、1-辛烯-3-醇、叶醇、2-甲基丁醛及异戊醛作为通过变量投影重要性值分析筛选出的标记性物质可以对枸杞产地进行初步区分。
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李曼祎
沈天辰
刘春凤
郑飞云
钮成拓
李崎
王金晶
关键词:  枸杞  活性物质  气相离子迁移谱技术  挥发性物质  偏最小二乘法判别    
Abstract: Wolfberry is a kind of raw material in traditional Chinese medicine. Its quality is related to the producing area. In order to provide a reference for the quality evaluation of wolfberry and identification of their origin,4 kinds of wolfberry from different production areas (Ningxia, Xinjiang, Qinghai and Inner Mongolia) were analyzed in the physio-chemical index, active substance and volatile flavor compounds. The results showed that there were certain differences in the physio-chemical index of wolfberry between different regions and the content of active substances in wolfberry of Ningxia and Qinghai production area showed a high level. The detection of headspace-gas chromatography-ion mobility spectroscopy combined with partial least squares discrimination analysis showed that 16 kinds of substances had significant content differences between producing areas. 1-propanol was a unique substance of the Inner Mongolia area which could be used to identify Inner Mongolia wolfberry. Furfural, 1-octene-3-ol, cis-3-hexen-1-ol, 2-methyl butanal and methyl butyrate selected by variable importance in projection value could be used as marker to distinguish the origin of wolfberry.
Key words:  wolfberry    active substances    headspace-gas chromatography-ion mobility spectroscopy (HS-GC-IMS)    volatiles markers    partial least squares discrimination analysis
收稿日期:  2021-03-08      修回日期:  2021-04-02           出版日期:  2021-12-25      发布日期:  2022-01-21      期的出版日期:  2021-12-25
基金资助: 国家自然科学基金项目(31771963)
作者简介:  硕士研究生(王金晶副教授为通讯作者,E-mail:jjwang@jiangnan.edu.cn)
引用本文:    
李曼祎,沈天辰,刘春凤,等. 不同产地枸杞品质差异研究[J]. 食品与发酵工业, 2021, 47(24): 56-63.
LI Manyi,SHEN Tianchen,LIU Chunfeng,et al. Research on the quality of wolfberry from different production areas[J]. Food and Fermentation Industries, 2021, 47(24): 56-63.
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http://sf1970.cnif.cn/CN/10.13995/j.cnki.11-1802/ts.027271  或          http://sf1970.cnif.cn/CN/Y2021/V47/I24/56
[1] POTTERAT O.Goji (Lycium barbarum L.Chinese):phytochemistry, pharmacology and safety in the perspective of traditional uses and recent popularity[J].Planta Medica, 2010, 76(1):7-19.
[2] CHEN S Y, LIANG L N, WANG Y, et al.Synergistic immunotherapeutic effects of Lycium barbarum polysaccharide and interferon-α2b on the murine Renca renal cell carcinoma cell line in vitro and in vivo[J].Molecular Medicine Reports, 2015, 12 (5):6 727-6 737.
[3] AHN M, PARK J S, CHAE S, et al.Hepatoprotective effects of Lycium Chinese Miller fruit and its constituent betaine in CCl4-induced hepatic damage in rats[J].Acta histochemica, 2014, 116(6):1 104-1 112.
[4] GAMBOA G, VSQUEZ V, QUIROZ C, et al.Carignan phenolic composition in wines from ten sites of the Maule Valley (Chile):Location and rootstock implications[J].Scientia Horticulturae, 2018, 234:63-73.
[5] ZHANG S S, WEI Y M, WEI S, et al.Authentication of Zhongning wolfberry with geographical indication by mineral profile[J].International Journal of Food Science & Technology, 2017, 52(2):457-463.
[6] GALLEGOS J, ARCE C, JORDANO R, et al.Target identification of volatile metabolites to allow the differentiation of lactic acid bacteria by gas chromatography ion mobility spectrometry[J].Food Chemistry, 2017, 220:362-370.
[7] PUTON J, NAMIESNIK J.Ion mobility spectrometry:Current status and application for chemical warfare agents detection[J].Trac Trends in Analytical Chemistry, 2016, 85(Part B):10-20.
[8] LI M Q, YANG R W, ZHANG H, et al.Development of a flavor fingerprint by HS-GC-IMS with PCA for volatile compounds of Tricholoma matsutake Singer[J].Food Chemistry, 2019, 290:32-39.
[9] ARROYO M N, MARTIN G A, JURADO C N, et al.Target vs spectral fingerprint data analysis of Iberian ham samples for avoiding labelling fraud using headspace-gas chromatography-ion mobility spectrometry[J].Food Chemistry, 2018, 246:65-73.
[10] CHANG M, ZHAO P Z, ZHANG T, et al.Characteristic volatiles fingerprints and profiles determination in different grades of coconut oil by HS-GC-IMS and HS-SPME-GC-MS[J].International Journal of Food Science and Technology, 2020, 55(12):3 670-3 679.
[11] 吴有锋, 马世震, 谭亮, 等.柴达木枸杞化学成分的测定[J].中成药, 2017, 39(5):984-989.WU Y F, MA S Z, TAN L, et al.Determination of chemical consituents in Lycii Fructus from Qaidam Basin[J].Chinese Traditional Patent Medicine, 2017, 39(5):984-989.
[12] FANG Y, LIU Y, WANG B, et al.Screening of the volatile compounds in fresh and thermally treated watermelon juice via headspace-gas chromatographyion mobility spectrometry and comprehensive two-dimensional gas chromatography-olfactory-mass spectrometry analysis[J].LWT, 2021, 137:110478.
[13] 孙达, 张红艳, 程运江, 等.11个产地纽荷尔脐橙果实风味物质含量差异[J].植物科学学报, 2015, 33(4):513-520.SUN D, ZHANG HY, CHENG Y J, et al.Contents of flavor components in Newhall Navel Oranges (Citrus sinensis) harvested from eleven production areas of China [J].Plant Science Journal, 2015, 33(4):513-520.
[14] 伊兴凯. 果实香气物质代谢谱及单糖转运体功能的研究[D].合肥:安徽农业大学, 2015.YI X K.Aromatic metabolite profiling and functional analysis for monosaccharide transporters in fruit[D].Hefei:Anhui Agricultural University, 2015.
[15] 王元基. 干旱对苹果品质的影响及其与糖代谢的关系[D].杨凌:西北农林科技大学, 2017.WANG Y J.Effects of drought on apple quality and its relationship with sugar metabolism[D].Yangling:Northwest A&F University, 2015.
[16] 吴中华, 李文丽, 赵丽娟, 等.枸杞分段式变温热风干燥特性及干燥品质[J].农业工程学报, 2015, 31 (11):287-293.WU Z H, LI W L, ZHAO L J, et al.Drying characteristics and product quality of Lycium barbarum under stages-varying temperatures drying process[J].Transactions of the Chinese Society of Agricultural English, 2015, 31 (11):287-293.
[17] ZHANG Q Y, CHEN W W, ZHAO J H, et al.Functional constituents and antioxidant activities of eight Chinese native goji genotypes[J].Food Chemistry, 2016, 200:230-236.
[18] LEA U S, SLIMESTAD R, SMEDVIG P, et al.Nitrogen deficiency enhances expression of specific MYB and bHLH transcription factors and accumulation of end products in the flavonoid pathway[J].Planta, 2007, 225(5):1 245-1 253.
[19] JIA H, WANG J A, YANG Y, et al.Changes in flavonoid content and transcript levels of genes in the flavonoid pathway in tobacco under phosphorus deficiency[J].Plant Growth Regulation, 2014, 76(2):225- 231.
[20] 崔治家, 刘峰林, 张启立, 等.不同产地枸杞子中枸杞多糖含量的比较分析[J].华西药学杂志, 2020, 35(1):59-61.CUI Z J, LIU L F, ZHANG Q L, et al.Comparative analysis of the content of Lycium barbarum polysaccharide in Lycii Fructus from different places[J].West China Journal of Pharmaceutical Science, 2020, 35(1):59-61.
[21] 段毅, 吴保祥, 徐丽, 等.不同纬度地区植物中正构烷烃及其同位素组成[J].地质学报, 2011, 85(2):262-271.DUAN Y, WU B X, XU L, et al.Compositions of n-alkanes and their isotopes in plants from the different latitude regions in China[J].Acta Geologica Sinica, 2011, 85(2):262-271.
[22] GARRIDO D R, DOBAO P M, ARCE L, et al.Determination of volatile compounds by GC-IMS to assign the quality of virgin olive oil[J].Food Chemistry, 2016, 187:572-579.
[23] JIN J Y, ZHAO M Y, ZHANG N, et al.Stable isotope signatures versus gas chromatographyion mobility spectrometry to determine the geographical origin of Fujian Oolong tea (Camellia sinensis) sample[J].European Food Research and Technology, 2020, 246(5):955–964.
[24] JI T, DAMI I E.Characterization of free flavor compounds in traminette grape and their relationship to vineyard training system and location[J].Journal of Food Science, 2008, 73(4):262-267.
[25] RAMBLA J L, TIKUNOV Y M, MONFORTE A J, et al.The expanded tomato fruit volatile landscape[J].Journal of Experimental Botany, 2014, 65 (16):4 613-4 623.
[26] 吴有锋, 谭亮, 沈建伟, 等.柴达木枸杞中17种氨基酸的测定与分析[J].食品工业科技, 2017, 38(1):281-286.WU Y F, TAN L, SHEN J W, et al.Determination and analysis of 17 amino acids in Qaidam Chinese wolfberry[J].Science and Technology of Food Industry, 2017, 38(1):281-286.
[27] EL HADI M A M, ZHANG F J, WU F F, et al.Advances in fruit aroma volatile research[J].Molecules, 2013, 18(7):8 200-8 229.
[28] 申济源. 基于 LOX 途径的果实香气物质形成与调控解析[D].杭州:浙江大学, 2013.SHEN J Y.Biosynthesis and regulation of fruit aroma-related volatiles derived from the LOX pathway[D].Hangzhou:Zhejiang university, 2013.
[29] 张明霞, 吴玉文, 段长青.葡萄与葡萄酒香气物质研究进展[J].中国农业科学, 2008, 41(7):2 098-2 104.ZHANG M X, WU Y W, DUAN C Q.Progress in study of aromatic compounds in grape and wine[J].Scientia Agricultura Sinica, 2008, 41(7):2 098-2 104.
[30] WANG X R, ROGERS K M, LI Y, et al.Untargeted and targeted discrimination of honey collected by Apis cerana and Apis mellifera based on volatiles using HS-GC-IMS and HS-SPME-GC-MS[J].Journal of Agricultural and Food Chemistry, 2019, 67(43):12 144-12 152.
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