为比较不同品牌道口烧鸡的香气差异,利用电子鼻和气质联用技术(gas chromatography-mass spectrometer, GC-MS)对其香气成分进行分析。结果表明,电子鼻结合线性判别分析(linear discriminant analysis, LDA)可实现对不同品牌道口烧鸡香气的快速区分;采用气质联用技术共检出道口烧鸡中的51种挥发性物质,其在各品牌样品中的组成和比例不同,分别形成了各品牌烧鸡的独特风味;采用相对气味活度值法(relative odor activity value, ROAV)分析得到13种关键香气化合物,包括2种醇类物质、6种醛类物质、4种萜烯类物质和2-戊基呋喃,它们是样品香气差异的主要物质。通过对关键香气化合物的主成分分析(principal component analysis, PCA),这13种关键香气化合物可以区分不同品牌道口烧鸡样品。
[1] PETRIČEVĆS, MARUŠIĆR N, LUKIĆK, et al. Differentiation of dry-cured hams from different processing methods by means of volatile compounds, physico-chemical and sensory analysis[J]. Meat Science, 2017, 137(3): 217-227.
[2] TIAN H X, LI F H, QIN L, et al. Discrimination of chicken seasonings and beef seasonings using electronic nose and sensory evaluation[J]. Journal of Food Science, 2014, 79(11): 2 346-2 353.
[3] SUN L X, CHEN J P, Li M Y, et al. Effect of star anise (Illiciumverum) on the volatile compounds of stewed chicken[J]. Journal of Food Process Engineering, 2014, 37(2): 131-145.
[4] TIAN X J, WANG J, CUI S Q. Analysis of pork adulteration in minced mutton using electronic nose of metal oxide sensors[J]. Journal of Food Engineering, 2013, 119(4): 744-749.
[5] 易宇文, 刘阳, 彭毅秦, 等. 东坡肘子风味电子鼻分析与感官评价相关性探究[J]. 食品与发酵工业, 2018, 44(1): 238-244.
[6] 贾洪锋, 卢一, 何江红, 等. 电子鼻在牦牛肉和牛肉猪肉识别中的应用[J]. 农业工程学报, 2011, 27(5): 358-363.
[7] 王勇勤, 郭新, 黄笠原, 等. 基于电子鼻和气质联用技术分析不同贮藏时间羊肉火腿香气成分[J]. 食品科学, 2019, 40(2): 215-221.
[8] 荣建华, 熊诗, 张亮子, 等. 基于电子鼻和SPME-GC-MS联用分析脆肉鲩鱼肉的挥发性风味成分[J]. 食品科学, 2015, 36(10): 124-128.
[9] 程华峰, 林琳, 葛孟甜, 等. 3种生态环境中华绒螯蟹肉挥发性风味特征的比较[J]. 食品与发酵工业, 2019, 45(23):247-256.
[10] YANG W J, YU J, PEI F, et al. Effect of hot air drying on volatile compounds of Flammulina velutipes detected by HS-SPME-GC-MS and electronic nose[J]. Food Chemistry, 2016, 196(4): 860-866.
[11] 谭椰子, 周光宏, 徐幸莲, 等. 中国三大干腌火腿皮下脂肪挥发性风味比较分析[J]. 食品科学, 2018, 39(4): 199-205.
[12] 段艳, 郑福平, 杨梦云, 等. ASE-SAFE/GC-MS/GC-O法分析德州扒鸡风味化合物[J]. 中国食品学报, 2014, 14(4): 222-230.
[13] 熊国远, 刘源, 高韶婷, 等. 符离集烧鸡加工过程中挥发性风味成分变化研究[J]. 南京农业大学学报, 2014, 37(6): 103-110.
[14] 张逸君, 郑福平, 张玉玉, 等. MAE-SAFE-GC-MS法分析道口烧鸡挥发性成分[J]. 食品科学, 2014, 35(22): 130-134.
[15] 李娜. 烧鸡挥发性风味物质分析及货架期延长技术研究[D]. 天津: 天津科技大学, 2017.
[16] MELUCCI D, BENDINI A, TESINI F, et al. Rapid direct analysis to discriminate geographic origin of extra virgin olive oils by flash gas chromatography electronic nose and chemometrics[J]. Food Chemistry, 2016, 204(8): 263-273.
[17] WETTASINGHE M, VASANTHAN T, TEMELLI F, et al. Volatiles from roasted byproducts of the poultry processing industry [J]. Journal of Agriculture and Food Chemistry, 2000, 48(8): 3 485-3 492.
[18] CALKINS C R, HODGEN J M. A fresh look at meat flavor [J]. Meat Science, 2007, 77(1): 63-80.
[19] NOLEAU I, TOULEMONDE B. Quantitative study of roast chicken fat[J]. Food Science Technology, 1987, 20(5): 37-41.
[20] ElMORE J S, MOTTRAM D S, ENSER M, et al.Effect of the polyunsaturated fatty acid composition of beef muscle on the pro?le of aroma volatiles[J]. Journal of Agricultural and Food Chemistry, 1999, 47(4): 1 619-1 625.
[21] MOTTRAM D S, EDWARDS R A. The role of triglycerides and phospholipids in the aroma of cooked beef [J]. Journal of the Science of Food and Agriculture. 1983, 34: 517-522.
[22] WHITFIELD F B. Volatiles from interactions of Maillard reactions and lipids[J]. C R C Critical Reviews in Food Technology, 1992, 31(1-2):1-58.
[23] SHAHIDI F. 肉制品与水产品的风味 [M]. 北京:中国轻工业出版社, 2002.
[24] SCHINDLER S, KRING U, BERGER R G, et al. Aroma development in high pressure treated beef and chicken meat compared to raw and heat treated[J]. Meat Science, 2010, 86(2): 317-323.
[25] SONG S Q, ZHANG X M, HAYAT K, et al. Formation of the beef flavor precursors and their correlation with chemical parameters during the controlled thermal oxidation of tallow[J]. Food Chemistry, 2011, 124: 203-209.
[26] 刘登勇, 周光宏, 徐幸莲. 金华火腿主体风味成分及其确定方法[J]. 南京农业大学学报, 2009, 32(2): 173-176.
[27] 武苏苏, 赵改名, 柳艳霞, 等. 基于主成分分析法的煮制时间对卤制鸡肉风味的影响分析[J]. 食品与发酵工业, 2014, 40(10): 194-199.
[28] 林诗宇, 杜夏夏, 冉崇霖, 等. 舍饲与林地放养混合模式下寿光鸡、固始鸡和罗曼蛋鸡蛋品质及肉品质的比较[J]. 动物营养学报, 2017, 29(6): 2 116-2 123.
[29] 高素敏. 品种、饲养方式对鸡肉中主要营养成分及风味前体物质的影响[D]. 郑州: 河南农业大学, 2008.
[30] 谢恬, 王丹, 马明娟, 等. OAV和GC-O-MS法分析五香驴肉风味活性物质[J]. 食品科学, 2018, 39 (8): 123-128.