研究报告

柠檬籽油复合微胶囊的制备及对牛肉干的保鲜效果

  • 杨丽华 ,
  • 张永东 ,
  • 李维正 ,
  • 韩玲 ,
  • 余群力 ,
  • 韩明山 ,
  • 冯伟平 ,
  • 韩广星
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  • 1(甘肃农业大学 食品科学与工程学院,甘肃 兰州,730070)
    2(张掖市畜牧兽医推广站,甘肃 张掖,734000)
    3(山东绿润食品有限公司,山东 临沂,276000)
    4(甘肃中天羊业股份有限公司,甘肃 定西,743000)
    5(内蒙古科尔沁牛业股份有限公司,内蒙古 通辽,028000)
第一作者:硕士研究生(韩玲教授和余群力教授为共同通信作者,E-mail:hltgggyx@163.com;yuqunlihl@163.com)

收稿日期: 2021-07-16

  修回日期: 2021-08-02

  网络出版日期: 2022-07-15

基金资助

甘肃省高等学校产业支撑计划项目(2020C-18);国家现代农业(肉牛牦牛)产业技术体系建设专项(CARS-37);甘肃省重点研发计划(2019-0202-NCC-0149)

Preparation of lemon seed oil complex microcapsules and effect of preservation of beef jerky

  • YANG Lihua ,
  • ZHANG Yongdong ,
  • LI Weizheng ,
  • HAN Ling ,
  • YU Qunli ,
  • HAN Mingshan ,
  • FENG Weiping ,
  • HAN Guangxing
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  • 1(College of Food Science and Engineering, Gansu Agricultural University, Lanzhou 730070, China)
    2(Zhangye Animal Husbandry and Veterinary Extension Station, Zhangye 734000, China)
    3(Shandong Lvrun Foodstuffs Co.Ltd., Linyi 276000, China)
    4(Gansu Zhongtian Sheep Industry Co.Ltd., Dingxi 743000, China)
    5(Inner Mongolia Horqin Cattle Industry Co.Ltd., Tongliao 028000, China)

Received date: 2021-07-16

  Revised date: 2021-08-02

  Online published: 2022-07-15

摘要

该实验以柠檬籽油为芯材,酵母细胞和辛烯基琥珀酸酐酯化淀粉为壁材,采用双层包埋法制备柠檬籽油复合微胶囊。通过双包埋微胶囊结构的观察和分析以及牛肉干的贮藏实验,研究双包埋微胶囊的包埋效果和对牛肉干保鲜作用的影响。结果表明,双包埋微胶囊的载油量最大为193.003 mg/g;其表面粗糙,结构完整;红外光谱分析结果表明,双包埋微胶囊在包埋过程中形成新的氢键,说明双包埋是成功的;差示扫描量热法测得双包埋后的微胶囊热稳定性提高。与传统干燥剂和空白组相比,双包埋微胶囊组能够显著抑制牛肉干的挥发性盐基总氮和硫代巴比妥酸反应物(P<0.05)含量升高,延缓感官品质的下降。因此,柠檬籽油复合微胶囊是一种良好的牛肉干传统干燥剂替代品,具有较大的市场开发潜力。

本文引用格式

杨丽华 , 张永东 , 李维正 , 韩玲 , 余群力 , 韩明山 , 冯伟平 , 韩广星 . 柠檬籽油复合微胶囊的制备及对牛肉干的保鲜效果[J]. 食品与发酵工业, 2022 , 48(12) : 105 -110 . DOI: 10.13995/j.cnki.11-1802/ts.028666

Abstract

The aim of this study was to prepare a safe and effective preservative for beef jerky. In this experiment, lemon seed oil was used as the core material, yeast cells and octenyl succinic anhydride esterified starch were used as the wall material to prepare lemon seed oil composite microcapsules by the double embedding method. The effect of the double-embedded microcapsules on the freshness of beef jerky was investigated by observation and analysis of the structure of the microcapsules and the storage of beef jerky. The results showed that the maximum oil loading of the double-embedded microcapsules was 193.003 mg/g; the surface was rough and the structure was intact; the infrared spectra showed that the double-embedded microcapsules formed new hydrogen bonds during the embedding process, which indicating that the double-embedding was successful. The thermal stability of the double-embedded microcapsules was improved as measured by differential scanning calorimetry. Compared with the conventional desiccant and blank groups, the double-embedded microcapsule group was able to significantly inhibit the volatile salt-based total nitrogen and thiobarbituric acid reactants of beef jerky (P<0.05) and delayed the decline of sensory quality. Therefore, lemon seed oil composite microcapsules are a good alternative to traditional desiccants for beef jerky and have greater potential for market development.

参考文献

[1] 朱效兵, 郭瑞.传统中式风味牛肉干的生产工艺[J].现代食品科技, 2020, 36(6):235-242;154.
ZHU X B, GUO R.Optimization of process parameters for Chinese-style beef jerky production[J].Modern Food Science and Technology, 2020, 36(6):235-242;154.
[2] SHAHIDI F, ZHONG Y.Novel antioxidants in food quality preservation and health promotion[J].European Journal of Lipid Science and Technology, 2010, 112(9):930-940.
[3] 何贤培. 干燥剂吸湿率测试方法的探讨[J].广东化工, 2019, 46(9):85-86.
HE X P.Test method of water absorption of desiccant[J].Guangdong Chemical Industry, 2019, 46(9):85-86.
[4] YILMAZ E, GÜNEŞER B A.Cold pressed versus solvent extracted lemon (Citrus limon L.) seed oils:Yield and properties[J].Journal of Food Science and Technology, 2017, 54(7):1 891-1 900.
[5] CHENG J R, LIU X M, ZHANG Y S, et al.Protective effects of Momordica grosvenori extract against lipid and protein oxidation-induced damage in dried minced pork slices[J].Meat Science, 2017, 133:26-35.
[6] BAH M G, BILAL H M, WANG J T.Fabrication and application of complex microcapsules:A review[J].Soft Matter, 2020, 16(3):570-590.
[7] FIORAMONTI S A, STEPANIC E M, TIBALDO A M, et al.Spray dried flaxseed oil powdered microcapsules obtained using milk whey proteins-alginate double layer emulsions[J].Food Research International, 2019, 119:931-940.
[8] PARAMERA E I, KONTELES S J, KARATHANOS V T.Microencapsulation of curcumin in cells of Saccharomyces cerevisiae[J].Food Chemistry, 2011, 125(3):892-902.
[9] DADKHODAZADE E, MOHAMMADI A, SHOJAEE-ALIABADI S, et al.Yeast cell microcapsules as a novel carrier for cholecalciferol encapsulation:Development, characterization and release properties[J].Food Biophysics, 2018, 13(4):404-411.
[10] XIAO Z B, KANG Y X, HOU W J, et al.Microcapsules based on octenyl succinic anhydride (OSA)-modified starch and maltodextrins changing the composition and release property of rose essential oil[J].International Journal of Biological Macromolecules, 2019, 137:132-138.
[11] 崔秋兵, 李景洪, 王碧.溶剂法提取柠檬籽油的研究[J].中国粮油学报, 2012, 27(10):67-69.
CUI Q B, LI J H, WANG B.Study on the solvent-extraction method of lemon seed oil[J].Journal of the Chinese Cereals and Oils Association, 2012, 27(10):67-69.
[12] FU J J, SONG L, GUAN J J, et al.Encapsulation of Antarctic krill oil in yeast cell microcarriers:Evaluation of oxidative stability and in vitro release[J].Food Chemistry, 2021, 338:128089.
[13] MEHRAN M, MASOUM S, MEMARZADEH M.Microencapsulation of Mentha spicata essential oil by spray drying:Optimization, characterization, release kinetics of essential oil from microcapsules in food models[J].Industrial Crops & Products, 2020, 154:112694.
[14] 关文强, 刘敬斌, 杨宏柳, 等.牛肉冰温保鲜效果研究[C].第六届中国冷冻冷藏新技术.新设备研讨会论文集,2013:174-178.
GUAN W Q, LIU J B, YANG H L, et al.Effect of ice temperature storage on the quality of fresh beef[C].Proceedings of the Sixth China Refrigeration and Cold Storage New Technology. New Equipment Seminar,2013:174-178.
[15] KAVOSI M, MOHAMMADI A, SHOJAEE-ALIABADI S, et al.Characterization and oxidative stability of purslane seed oil microencapsulated in yeast cells biocapsules[J].Journal of the Science of Food & Agriculture, 2018, 98(7):2 490-2 497.
[16] 冯涛, 荣志伟.直链淀粉薄荷酮微胶囊的制备、表征及应用[J].上海应用技术学院学报(自然科学版), 2012, 12(4):261-265;269.
FENG T, RONG Z W.Preparation and structure characterization of amylose-menthone microcapsules and their application[J]. Journal of Shanghai Institute of Technology:Natural Science, 2012, 12(4):261-265;269.
[17] XIAO Z B, KANG Y X, HOU W J, et al.Microcapsules based on octenyl succinic anhydride (OSA)-modified starch and maltodextrins changing the composition and release property of rose essential oil[J].International Journal of Biological Macromolecules, 2019, 137:132-138
[18] ZHU J J, SUN W Z, MENG Z Y, et al.Preparation and characterization of a new type of porous starch microspheres (PSM) and effect of physicochemical properties on water uptake rate[J].International Journal of Biological Macromolecules, 2018, 116:707-714.
[19] BHOWMIK M, HALDAR S, DHARMALINGAM K, et al.Evaluation of thermo-kinetic and absorption characteristics of pure desiccants and desiccant mixtures[J].Materials Today:Proceedings, 2020, 26:1 967-1 971.
[20] MENCHETTI L, BRECCHIA G, BRANCIARI R, et al.The effect of Goji berries (Lycium barbarum) dietary supplementation on rabbit meat quality[J].Meat Science, 2020, 161:108018.
[21] TSIKAS D.Assessment of lipid peroxidation by measuring malondialdehyde (MDA) and relatives in biological samples:Analytical and biological challenges[J].Analytical Biochemistry, 2017, 524:13-30.
[22] GUO Z L, HAN L, YU Q L, et al.Effect of a sea buckthorn pomace extract-esterified potato starch film on the quality and spoilage bacteria of beef jerky sold in supermarket[J].Food Chemistry, 2020, 326:127001.
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