顶空固相微萃取结合气相色谱质谱-嗅闻联用技术鉴定巧克力麦芽中可可特征风味物质

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  • (江南大学 生物工程学院,工业生物技术教育部重点实验室,江苏 无锡,214122)

网络出版日期: 2018-09-06

基金资助

(江苏省现代工业发酵协同创新中心资助项目;国家自然科学基金项目(31571942,31601558和31771963)

Identification of cocoa characteristic flavor compounds in chocolate malt by gas chromatography-olfactometry-mass spectrometry with headspace solid phasemicro-extraction

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  • (The Key Laboratory of Industrial Biotechnology, Ministry of Education, School of Biotechnology,Jiangnan University, Wuxi 214122, China)

Online published: 2018-09-06

摘要

采用顶空固相微萃取(headspace-solid phase micro-extraction, HS-SPME)技术结合气相色谱质谱-嗅闻联用(gas chromatography-olfactometry-mass spectrometer, GC-O-MS)对巧克力麦芽样品中风味化合物进行检测与分析,共检测得到47种风味物质参与构成了巧克力麦芽样品的风味,包括:14种醛、7种醇、5种酮、5种酸、6种吡嗪以及其他一些特殊的风味物质。其中巧克力麦芽中具有可可特征风味的化合物为2,6-二甲基吡嗪、三甲基吡嗪以及2-乙基-3,5-二甲基吡嗪。

本文引用格式

秦奔, 张海鹏, 郑飞云, 等. . 顶空固相微萃取结合气相色谱质谱-嗅闻联用技术鉴定巧克力麦芽中可可特征风味物质[J]. 食品与发酵工业, 2018 , 44(7) : 258 -262 . DOI: 10.13995/j.cnki.11-1802/ts.016780

Abstract

The flavor compounds in chocolate malt sample were analyzed and detected by headspace solid phase microextraction (HS-SPME) combined with GC-O-MS. The results showed that 47 flavor compounds made contribution to the flavor of chocolate malt sample, including 14 aldehydes, 7 alcohols, 5 ketones, 5 acids, 6 pyrazines, and any other special flavor substances. Among the flavor compounds of chocolate malt, three compounds had cocoa characteristic flavor, and they were 2,6-dimethyl pyrazine, trimethyl pyrazine and 2-ethyl-3,5-dimethyl pyrazine.
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