采用感官品评方法对13款浓香白酒原酒进行分析,将样品按不同绵甜度分成3类。对比样品风味构成得出,乳酸和乳酸乙酯等风味在A类最绵甜的酒样中含量相对较高,其乳己比稳定在1.2~1.5之间,乙乳比稳定在1.0以下,酸酯比稳定在0.6左右,醇酯比控制在0.15~0.20。通过多元线性回归方程建立浓香白酒绵甜型感官指数模型,其中乳己比和酸酯比对白酒的绵甜感官具有正向作用,在一定范围内乳己比和酸酯比越高,酒体绵甜度越高。
13 samples of Strong-flavor Baijiu raw liquor were analyzed by sensory evaluation method, and the samples were divided into 3 categories according to the level of different soft-sweet. By comparing the flavor compounds composition of the samples, it can be concluded that the flavor compounds of lactic acid and ethyl lactate are relatively high in the category A liquor samples with the most soft-sweet flavor. The ethyl lactate to ethyl hexanoate ratio was stably between 1.2 and 1.5, the ethyl acetate to ethyl lactate ratio was stably below 1.0, the acid to ethyl ratio was stable around 0.6, and the alcohol to ethyl ratio was controlled between 0.15 and 0.20. Multiple linear regression equation was used to establish the index model of soft-sweet’s sense in Strong-flavor Baijiu, in which the ethyl lactate to ethyl hexanoate ratio and the acid to ethyl ratio had a positive effect on the sense of soft-sweet in liquor, and the higher ratio had a positive effect on the improvement of soft- sweet’s level in liquor within limits.
[1] 沈怡方. 白酒生产技术全书[M]. 北京: 中国轻工业出版社, 1998.
[2] 辛磊. 白酒微量成分与酒体风格特征关系的探讨[J]. 食品与机械, 2004, 20(2): 49-50.
[3] 沈怡方. 试论浓香型白酒的流派[J]. 酿酒, 1992, 19(5): 10-13.
[4] 范文来, 徐岩. 从微量成分分析浓香型大曲酒的流派[J]. 酿酒科技, 2000(5): 92-94.
[5] 郎召伟. 泸型酒酿造过程中风味物质变化分析[D]. 无锡: 江南大学,2015.
[6] XIANG W L, LI K, LIU S, et al. Microbial succession in the traditional Chinese luzhou-flavor liquor fermentation process as evaluated by ssu rrna profiles[J]. World Journal of Microbiology & Biotechnology, 2013, 29(3): 559-567.
[7] FAN W L, QIAN M C. Headspace solid phase microextraction and gas chromatography-olfactometry dilution analysis of young and aged chinese “yanghe daqu” liquors[J]. J Agric Food Chem, 2005, 53(20): 7 931-7 938.
[8] FAN W L, QIAN M C. Identification of aroma compounds in Chinese “Yanghe Daqu” liquor by normal phase chromatography fractionation followed by gas chromatography olfactometry[J]. Flavour & Fragrance Journal, 2010, 21(2): 333-342.
[9] 李大和. 试论中国白酒的甜味(上) [J]. 酿酒科技, 2004(6): 26-28.
[10] 朱广生, 陈亦清, 陈翔. 绵柔型白酒的创新与实践[J]. 酿酒, 2008, 35(6): 16-18.
[11] 尹爱玲. 中国白酒风格新流派确立——洋河酒厂“中国绵柔型风格白酒的研制与开发”项目技术成果通过鉴定[J]. 新食品, 2010(15):126-127.
[12] 王鹏, 蒋超, 崔磊, 等. 安徽地产白酒风味构成的分析研究[J]. 中国酿造, 2018, 37(5):37-41.
[13] 唐坤甜, 赵彩云, 韩兴林, 等. 白酒味觉成分有机酸含量分析及其对酿造工艺的影响[J]. 食品与发酵工业, 2016, 42(7): 202-208.
[14] 沈怡方. 白酒中四大乙酯在酿造发酵中形成的探讨[J]. 酿酒科技, 2003(5): 28-31.
[15] 张金修, 张雪飞. 探讨浓香型白酒中微量成分与酒质的关系[J]. 酿酒科技, 2013(7): 72-74.
[16] 李莉, 王秋叶, 盛夏, 等. 白酒中酯类对酒质的影响[J]. 食品安全导刊, 2016(12X): 130.
[17] 张方, 张宿义, 苏占元, 等. 有机酸对浓香型白酒品质及其酿造过程影响的研究进展[J]. 酿酒科技, 2016(1): 94-97.
[18] 贾巧唤, 任石苟. 浅述酸、酯、醇等成分对白酒的影响[J]. 食品工程, 2008(4): 12-13.
[19] 曾祖训. 对白酒酒体的认识、体验与创新[J]. 酿酒, 2014, 41(2): 3-5.
[20] 曾朝珍, 张永茂, 康三江, 等. 发酵酒中高级醇的研究进展[J]. 中国酿造, 2015, 34(5): 11-15.
[21] 罗杰, 敖宗华, 王松涛, 等. 浓香型白酒不同类别基酒中杂醇油相关性研究[J]. 酿酒科技, 2015(1): 43-44.
[22] 王成,陈明,涂京霞,等. 啤酒饮后舒适度及其与主要风味成分相关性研究[J]. 中外酒业, 2018,81(23):30-27.