食品与发酵工业

二次结晶谷氨酸纯化工艺研究Ⅰ:转晶条件优化

  • 曹付明 ,
  • 张建华 ,
  • 刘中华 ,
  • 张宏建 ,
  • 毛忠贵
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网络出版日期: 2011-06-25

Purifiuction of the Glutamic Acid of Secondary Crystallization Process(GASCP) Ⅰ:Optimization of Solution Mediated Transformation(SMT) Conditions

  • Cao Fu-ming ,
  • Zhang Jian-hua ,
  • Liu Zhong-hua ,
  • Zhang Hong-jian ,
  • Mao Zhong-gui
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Online published: 2011-06-25

摘要

从等电母液中蒸发结晶得到的二次结晶谷氨酸,其硫酸铵、色素等杂质含量高,不能直接精制生产味精,转晶是提高二次结晶谷氨酸质量的途径之一。实验研究了转晶温度、pH值、转晶料水比等因素对谷氨酸转晶的影响,得到比较理想的转晶条件:转晶温度95℃,pH值4.5,转晶料水1∶2.5,活性炭添加量为1%(1g活性炭/100g二次结晶谷氨酸)。

关键词: 谷氨酸; 转晶; 条件优化

本文引用格式

曹付明 , 张建华 , 刘中华 , 张宏建 , 毛忠贵 . 二次结晶谷氨酸纯化工艺研究Ⅰ:转晶条件优化[J]. 食品与发酵工业, 2011 , 37(06) : 11 -15 . DOI: 10.13995/j.cnki.11-1802/ts.2011.06.029

Abstract

GASCP was produced from the isoelectric liquor by evaporative crystallization process,in which a large amount of impurities such as pigments,(NH4)2SO4 remained.This made the product cannot be further purified to produce MSG.The solution mediated transformation(SMT) of L-glutamic acid is one of the ways to improve the quality of the GASCP.The effects of temperature,pH,ratio of GASCP/water and the use of activated carbon on the SMT of GASCP were investigated.Based on the researches,the ideal conditions for SMT of GASCP were determined as follows: temperature was 95℃,pH 4.5,the ratio of GASCP/water was 1∶ 2.5,the mount of activated carbon was 1%.
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