食品与发酵工业

麦芽三糖基-β-环糊精的结构

  • 于博 ,
  • 柏玉香 ,
  • 金征宇 ,
  • 吴月纯 ,
  • 汤尚文 ,
  • 吴进菊
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网络出版日期: 2013-07-25

Study on the structure of maltotriosyl-β-cyclodextrin

  • YU Bo ,
  • BAI Yu-xiang ,
  • JIN Zheng-yu ,
  • WU Yue-chun ,
  • WU Jin-ju
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Online published: 2013-07-25

摘要

用高效液相色谱法对制备得到的麦芽三糖基-β-环糊精进行纯度分析,应用电喷雾质谱测定了麦芽三糖基-β-环糊精的分子量,用傅里叶变换红外光谱、酶解分析以及1H NMR,13C NMR和HMBC谱分析技术对麦芽三糖基-β-环糊精进行结构表征。结果表明:麦芽三糖基-β-环糊精纯度达到99%以上,分子质量为1 620.5,其结构为单取代-6-O-α-D-麦芽三糖基-β-环糊精。

本文引用格式

于博 , 柏玉香 , 金征宇 , 吴月纯 , 汤尚文 , 吴进菊 . 麦芽三糖基-β-环糊精的结构[J]. 食品与发酵工业, 2013 , 39(07) : 50 -54 . DOI: 10.13995/j.cnki.11-1802/ts.2013.07.033

Abstract

The purity of maltotriosyl-β-cyclodextrin was confirmed by HPLC and the molecular weight was calculated by ESIMS.The chemical composition and structure of maltotriosyl-β-cyclodextrin were elucidated by FTIR,analyzed by enzymatic hydrolysis,1H NMR,13C NMR and HMBC.The results indicated that the purity of maltotriosyl-β-cyclodextrin was more than 99%,its molecular weight was 1620.5 and its structure was mono-6-O-α-D-maltotriosyl-β-cyclodextrin.
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