食品与发酵工业 >

2021 , Vol. 47 >Issue 6: 121 - 126

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.025146

研究报告

阿维菌素和氟啶胺在柑橘汁加工过程中的残留行为及加工因子研究

  • 康霞丽 ,
  • 赵其阳 ,
  • 左巍 ,
  • 张耀海 ,
  • 刘浩然 ,
  • 王成秋 ,
  • 焦必宁
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  • 1(西南大学 中国农业科学院柑桔研究所,重庆,400712)
    2(农业农村部柑桔产品质量安全风险评估实验室,重庆,400712)
    3(农业农村部柑桔及苗木质量监督检验测试中心,重庆,400712)
硕士研究生(焦必宁研究员和王成秋副研究员为共同通讯作者,E-mail:jiaobining@cric.cn;citruszhx@163.com)

收稿日期: 2020-07-23

  修回日期: 2020-09-29

  网络出版日期: 2021-04-15

基金资助

农业农村部现代农业(柑桔)产业技术体系建设专项项目(CARS-26);国家农产品质量安全风险评估专项项目(GJFP2019012)

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The residual behavior and processing factors of abamectin and fluazinam in citrus juice processing

  • KANG Xiali ,
  • ZHAO Qiyang ,
  • ZUO Wei ,
  • ZHANG Yaohai ,
  • LIU Haoran ,
  • WANG Chengqiu ,
  • JIAO Bining
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  • 1(Citrus Research Institute,Southwest University & Chinese Academy of Agricultural Sciences, Chongqing 400712, China)
    2(Laboratory of Risk Assessment for Citrus Quality and Safety, Ministry of Agriculture and Rural Affairs, Chongqing 400712, China)
    3(Quality Supervision and Testing Center for Citrus and Seedling, Ministry of Agriculture and Rural Affairs, Chongqing 400712, China)

Received date: 2020-07-23

  Revised date: 2020-09-29

  Online published: 2021-04-15

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摘要

为评价阿维菌素和氟啶胺在柑橘汁商业化加工过程中的残留行为及加工因子,以普通甜橙为试验材料,以5倍最高推荐施药剂量在重庆和湖南进行田间试验,按照橙汁典型商业化加工过程进行加工,采用QuEChERS前处理结合超高效液相色谱-串联质谱联用技术(UPLC-MS/MS)对各加工单元的农药残留进行检测分析。结果表明,在柑橘汁加工过程中,榨汁是降低阿维菌素和氟啶胺残留最有效的过程;除柑橘皮精油中2种农药发生明显富集外,其余加工产品中农药残留加工因子均小于1。该研究结果可为监测阿维菌素和氟啶胺在柑橘及其制品中的农药残留行为及膳食暴露风险评估提供参考。

关键词： 农药残留; 阿维菌素; 氟啶胺; 加工因子

本文引用格式

康霞丽 , 赵其阳 , 左巍 , 张耀海 , 刘浩然 , 王成秋 , 焦必宁 . 阿维菌素和氟啶胺在柑橘汁加工过程中的残留行为及加工因子研究[J]. 食品与发酵工业, 2021 , 47(6) : 121 -126 . DOI: 10.13995/j.cnki.11-1802/ts.025146

Abstract

To evaluate the residual behavior and processing factors of abamectin and fluazinam in the commercial processing of citrus juice, the field trials were carried out by spraying with the solution of 5 times the concentration of the maximum recommended dosages in Chongqing and Hunan. The two pesticide residues were determined by liquid chromatography-tandem mass spectrometry technology (UPLC-MS/MS) based on QuEChERS pretreatment technology. The results showed that the juice extraction process was the most effective method to reduce the residue of abamectin and fluazinam in citrus. In addition to abamectin and fluazinam were enriched in citrus peel essential oil, the processing factors of abamectin and fluazinam in each processed product were less than 1.0. The results of the study can provide a reference for monitoring pesticide residue behavior as well as dietary exposure assessment of abamectin and fluazinam in citrus and its products.

Key words： pesticide residue; abamectin; fluazinam; processing factors

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