研究报告

超高温瞬时杀菌对苏派黄酒风味物质的影响

  • 姬中伟 ,
  • 衡洋洋 ,
  • 周志磊 ,
  • 王俊 ,
  • 毛健
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  • 1(江南大学,粮食发酵工艺与技术国家工程实验室,江苏 无锡,214122)
    2(江南大学 食品学院,江苏 无锡,214122)
    3(江南大学(绍兴)产业技术研究院,浙江 绍兴,312000)
    4(江苏张家港酿酒有限公司,江苏 苏州,215637)
    5(国家黄酒工程技术研究中心,浙江 绍兴,312000)
第一作者:博士研究生,高级实验师(毛健教授为通信作者,E-mail:maojian@jiangnan.edu.cn)

收稿日期: 2021-09-14

  修回日期: 2021-10-06

  网络出版日期: 2022-06-10

基金资助

国家自然科学基金重点项目(22138004);国家自然科学基金青年项目(32001828)

Effect of ultra-high temperature instantaneous sterilization on flavor substances in Supai Huangjiu

  • JI Zhongwei ,
  • HENG Yangyang ,
  • ZHOU Zhilei ,
  • WANG Jun ,
  • MAO Jian
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  • 1(National Engineering Laboratory for Cereal Fermentation Technology, Jiangnan University, Wuxi 214122, China)
    2(School of Food Science and Technology, Jiangnan University, Wuxi 214122, China)
    3(Jiangnan University (Shaoxing) Industrial Technology Research Institute, Shaoxing 312000, China)
    4(Jiangsu Zhangjiagang Brewery Co. Ltd., Suzhou 215637, China)
    5(National Engineering Research Center for Huangjiu, Shaoxing 312000, China)

Received date: 2021-09-14

  Revised date: 2021-10-06

  Online published: 2022-06-10

摘要

为探究超高温瞬时杀菌对黄酒中风味物质的影响,该研究以苏派黄酒(江苏地区黄酒)为研究对象,考察不同条件的超高温瞬时杀菌处理后黄酒中挥发性风味化合物以及非挥发性风味物质含量的变化情况。结果表明,(1)超高温瞬时杀菌处理后,2种黄酒的挥发性风味化合物含量均显著降低(P<0.05),在135 ℃ 5 s处理条件下,甜黄酒挥发性风味化合物总量降低了17.5%;半干黄酒挥发性风味化合物总量降低了49.4%;(2)甜黄酒的有机酸总量较对照组有所增加,其中135 ℃ 5 s处理后有机酸总量显著性增加(相比对照增加了101.5%)(P<0.05);半干黄酒分别在120、130、135 ℃处理5 s后,有机酸总量均出现增加,其中120 ℃处理后显著性增加(相比对照组增加了39.9%)(P<0.05);(3)甜黄酒中17种游离氨基酸的含量无显著变化(P>0.05);而半干黄酒的氨基酸总量显著性下降(P<0.05),其中在125 ℃ 5 s处理条件下,氨基酸含量下降幅度最大(相比对照组降低了17.6%)。说明超高温瞬时杀菌对苏派黄酒中的风味物质均有不同程度的影响,从而会改变黄酒中的原有风味。

本文引用格式

姬中伟 , 衡洋洋 , 周志磊 , 王俊 , 毛健 . 超高温瞬时杀菌对苏派黄酒风味物质的影响[J]. 食品与发酵工业, 2022 , 48(10) : 16 -21 . DOI: 10.13995/j.cnki.11-1802/ts.029350

Abstract

To explore the effect of ultra-high temperature instantaneous sterilization on the flavor substances in Huangjiu, Supai Huangjiu (Huangjiu from Jiangsu region) was used as the research object, and the changes in the content of volatile flavor compounds and non-volatile compounds in Huangjiu were detected. The results showed that, after ultra-high temperature instantaneous sterilization, the content of volatile flavor compounds of Huangjiu samples significantly reduced (P<0.05). Under the condition of 135 ℃ for 5 s, the total amount of volatile flavor compounds of sweet Huangjiu was reduced by 17.5%; that of the semi-dry Huangjiu was reduced by 49.4%. Compared with the control group, the total amount of organic acids in sweet Huangjiu increased, and it increased significantly after treatment at 135 ℃ (increased 101.5%) (P<0.05). Compared with the control, the total amount of organic acids in semi-dry Huangjiu increased after sterilization at 120 ℃ for 5 s, 130 ℃ for 5 s, 135 ℃ for 5 s, among which the increase was significant after treatment at 120 ℃ (increased by 39.9%) (P<0.05). The content of free amino acids in sweet Huangjiu had no significant change (P>0.05), while that in the semi-dry type was significantly decreased (P<0.05), and its content decreased the most at 125 ℃ for 5 s. The results indicated that the instantaneous sterilization at ultra-high temperature had different effects on flavor substances in Supai Huangjiu, and thus could change its flavor.

参考文献

[1] CHEN S, WANG C C, QIAN M, et al.Characterization of the key aroma compounds in aged Chinese Huangjiu by comparative aroma extract dilution analysis, quantitative measurements, aroma recombination,and omission studies[J].Journal of Agricultural and Food Chemistry, 2019, 67(17):4 876-4 884.
[2] 王培璇, 毛健, 李晓钟, 等.不同地区黄酒挥发性物质差异性分析[J].食品科学, 2014, 35(6):83-89.
WANG P X, MAO J, LI X Z, et al.Comparative analysis of volatile components of Chinese Rice Wines from different areas[J].Food Science, 2014, 35(6):83-89.
[3] 周颖, 黄锐.超高温瞬时灭菌工艺优化[J].中国乳业, 2020, 31(2):81-84.
ZHOU Y, HUANG R.Optimization of instantaneous ultrahigh temperature sterilization process[J].China Dairy, 2020, 31(2):81-84.
[4] SAMARRA I, MASDEVALL C, FOGUET-ROMERO E, et al.Analysis of oxylipins to differentiate between organic and conventional UHT milks[J].Food Chemistry, 2021,343:128477.
[5] 胡秦佳宝, 刘璇, 毕金峰, 等.非热加工与传统热处理对苹果汁品质的影响[J].食品与发酵工业, 2016, 42(1):102-107.
HU Q J B, LIU X, BI J F, et al.The impact of the nonthermal and thermal sterilization on the quality of apple juices[J].Food and Fermentation Industries, 2016, 42(1):102-107.
[6] LUND P, NIELSEN S B, NIELSEN C F, et al.Impact of UHT treatment and storage on liquid infant formula:Complex structural changes uncovered by centrifugal field-flow fractionation with multi-angle light scattering[J].Food Chemistry, 2021, 2(34):129145.
[7] 房子舒, 易俊洁, 张雅洁, 等.超高压和高温瞬时杀菌对蓝莓汁品质影响的比较[J].食品与发酵工业, 2012, 38(12):7-10.
FANG Z S, YI J J, ZHANG Y J, et al.Effect of sterilization with high hydrostatic pressure and high temperature on the quality of blueberry juice[J].Food and Fermentation Industries, 2012, 38(12):7-10.
[8] 王嵩, 张乃斌, 张文杰, 等.高温瞬时灭菌技术对啤酒质量影响的研究[J].酿酒科技, 2013(8):33-35.
WANG S, ZHANG N B, ZHANG W J,et al.Effect of high temperature instant sterilization on beer quality[J].Liquor-Making Science and Technology, 2013(8):33-35.
[9] 陈志宏, 张汆, 郭宏宝.HS-SPME-GC-MS法分析芡实原酒中挥发性风味物质[J].武汉轻工大学学报, 2021, 40(1):22-29.
CHEN Z H, ZHANG C, GUO H B.The analysis of volatile flavor compounds in Euryale Ferox base liquor by HS-SPME-GC-MS method[J].Jortnal of Wuhan Polytechnic University,2021, 40(1):22-29.
[10] 张陈, 郑晓敏, 马长中, 等.高效液相色谱法对青稞酒中有机酸、醇及糖含量的测定[J].食品科技, 2020, 45(7):317-323.
ZHANG C, ZHENG X M, MA C Z, et al.Determination of organic acids, alcohols and glucose content in barley wine by HPLC[J].Food Science and Technology, 2020, 45(7):317-323.
[11] 曾玩娴, 刘天质.高效液相色谱法同时测定糯米酒中17种氨基酸[J].酿酒科技, 2011(11):120-121.
ZENG W X, LIU T Z.Simultaneous determination of 17 kinds of amino acids contentin yellow rice wine by RP-HPLC with post-column derivatization[J].Liquor-Making Science and Technology, 2011(11):120-121.
[12] 刘奕, 吴琼, 吴庆园, 等.气相色谱-质谱法比较分析巴氏杀菌前后沙参糯米酒中的香气成分[J].食品科学, 2016, 37(20):108-112.
LIU Y, WU Q, WU Q Y, et al.Comparative analysis of aroma compounds in Glutinous Rice Wine added with Adenophora stricta roots before and after pasteurization by GC-MS[J].Food Science, 2016, 37(20):108-112.
[13] 张丽华, 李珍珠, 王维静, 等.不同杀菌方式对低醇枣酒品质的影响[J].中国酿造, 2018, 37(12):106-111.
ZHANG L H, LI Z Z, WANG W J, et al.Effect of different sterilization methods on the quality of low-alcohol jujube wine[J].China Brewing, 2018, 37(12):106-111.
[14] 孙方丹, 金铁岩.2种杀菌处理对朝鲜族米酒品质影响的研究[J].延边大学农学学报, 2019, 41(1):73-78; 86.
SUN F D, JIN T Y.Research on the effect of two sterilization treatment methods on the quality of Korean rice wine[J].Journal of Agricultural Science Yanbian University, 2019, 41(1):73-78; 86.
[15] 王琳, 陈双, 徐岩.固相萃取-超高效液相色谱法测定黄酒中的有机酸[J].食品与发酵工业, 2016, 42(10):142-148.
WANG L, CHEN S, XU Y.Determination of organic acids in Chinese rice wine by solid phase extraction-ultra performance liquid chromatography[J].Food and Fermentation Industries, 2016, 42(10):142-148.
[16] 张晶, 刘双平, 周志磊, 等.麦曲添加量对黄酒酿造及其风味的影响[J].食品与机械, 2020, 36(4):56-61.
ZHANG J, LIU S P, ZHOU Z L, et al.Effect of addition of wheat kojiqu on brewing and flavor of yellow rice wine[J].Food and Machinery, 2020, 36(4):56-61.
[17] 马辉, 张海宁, 叶庆, 等.超高压处理对丹阳封缸酒中9种有机酸的影响[J].酿酒科技, 2013(6):43-45; 50.
MA H, ZHANG H N, YE Q, et al.Effects of ultra-high pressure treatment on the content of nine kinds of organic acids in Danyang Fenggang rice wine[J].Liquor-Making Science and Technology, 2013(6):43-45; 50.
[18] 李婉平, 刘敏, 王皆行, 等.炎热气候条件下抗蒸腾剂对酿酒葡萄光合特性与葡萄酒品质的影响[J].中国农业科学, 2019, 52(17):3 008-3 019.
LI W P, LIU M, WANG J X, et al.Influence of anti-transpirant on photosynthesis characteristic and qualities of wines in hot climate[J].Scientia Agricultura Sinica, 2019, 52(17):3 008-3 019.
[19] 张腾, 王世朋, 孙照勇, 等.酿酒废糟中温和高温干式厌氧消化及微生物群落结构的研究[J].河南农业大学学报, 2020, 54(2):295-303; 325.
ZHANG T, WANG S P, SUN Z Y, et al.Study on dry anaerobic digestion of distilled grain waste and microbial community under mesophilic and thermophilic conditions[J].Journal of Henan Agricultural University, 2020, 54(2):295-303; 325.
[20] 张璐, 张昱, 蒲云峰, 等.慕萨莱思葡萄酒酿造过程中的氨基酸组成及含量分析[J].食品工业, 2018, 39(4):260-263.
ZHANG L, ZHANG Y, PU Y F, et al.Analysis of amino acid composition and content in musalais wine through the brewing process[J].The Food Industry, 2018, 39(4):260-263.
[21] SARTOR S, BURIN V M, CALIARI V, et al.Profiling of free amino acids in sparkling wines during over-lees aging and evaluation of sensory properties[J].LWT, 2021,140:110847.
[22] JIN T Y, SARAVANAKUMAR K, WANG M H.Effect of different sterilization methods on physicochemical and microbiological properties of rice wine during the preservation[J].Beni-Suef University Journal of Basic and Applied Sciences, 2018, 7(4):487-491.
[23] 阎文飞, 程凡升, 郭瑞, 等.北方黄酒陈酿过程中主要成分含量及其变化趋势[J].中国酿造, 2017, 36(5):72-75.
YAN W F, CHENG F S, GUO R, et al.Main components and variation tendency of northern Chinese rice wine during aging[J].China Brewing, 2017, 36(5):72-75.
[24] LAN Y B, GUO J X, QIAN X, et al.Characterization of key odor-active compounds in sweet Petit Manseng (Vitis vinifera L.) wine by gas chromatography-olfactometry, aroma reconstitution and omission tests[J].Journal of Food Science, 2021, 86(4):1 258-1 272.
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