研究报告

黑豆皮乙醇提取物/玉米淀粉/卡拉胶复合膜的物化性质及生物活性表征

  • 杨丽 ,
  • 李子钰 ,
  • 张福娟 ,
  • 杜国军 ,
  • 孙敬明 ,
  • 王存堂
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  • 1(齐齐哈尔大学 食品与生物工程学院,黑龙江 齐齐哈尔,161006)
    2(朝阳师范高等专科学校 生化工程系,辽宁 朝阳,122000)
第一作者:讲师(王存堂教授为通信作者,E-mail:robbertwang@163.com)

收稿日期: 2021-12-21

  修回日期: 2022-01-13

  网络出版日期: 2022-06-10

基金资助

黑龙江省属高校基本业务专项(YSTSXK201812;135509224)

Physicochemical properties and biological activity characterization of ethanol extract of black soybean coat/corn starch/carrageenan composite films

  • YANG Li ,
  • LI Ziyu ,
  • ZHANG Fujuan ,
  • DU Guojun ,
  • SUN Jingming ,
  • WANG Cuntang
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  • 1(College of Food and Biological Engineering, Qiqihar University, Qiqihar 161006, China)
    2(Department of Biochemical Engineering, Chaoyang Teachers College, Chaoyang 122000, China)

Received date: 2021-12-21

  Revised date: 2022-01-13

  Online published: 2022-06-10

摘要

该研究以玉米淀粉为基材,卡拉胶作为增强剂,甘油作为增塑剂,制备复合膜,并探讨了不同添加量的黑豆皮乙醇提取物对复合膜的物化性质及生物活性的影响。结果表明,提取物的加入使得复合膜的颜色加深,不透明度增大,并且影响了复合膜的微观结构;红外光谱和X-射线衍射结果表明,提取物的加入可抑制淀粉分子的重结晶现象,影响复合膜的机械性能和水蒸气透过率,并降低复合膜的玻璃化转变温度;改善复合膜的生物活性,提高复合膜的抗氧化性能和抑菌性能。该研究结果可为黑豆皮乙醇提取物/玉米淀粉/卡拉胶复合膜的生产和应用提供理论基础。

本文引用格式

杨丽 , 李子钰 , 张福娟 , 杜国军 , 孙敬明 , 王存堂 . 黑豆皮乙醇提取物/玉米淀粉/卡拉胶复合膜的物化性质及生物活性表征[J]. 食品与发酵工业, 2022 , 48(10) : 164 -171 . DOI: 10.13995/j.cnki.11-1802/ts.030537

Abstract

Traditional plastic packaging is easy to cause environmental pollution and harm human health. Corn starch, as a rich resources in nature which is a potential good natural polymer packaging material can be used. However, the single corn starch film is insufficient in terms of mechanical properties and biological activity. Therefore, in this study, corn starch was used as the substrate, carrageenan was used as an enhancer, glycerol was used as a plasticizer to prepare the composite films, and the influence of different concentrations of ethanol extract of black soybean coat on the physicochemical properties and biological activity of the composite films were explore. The results showed that the color and opacity of the composite films increased and affected the microstructure of the composite films. The infrared spectrum and X-ray diffraction results showed that the addition of the extract inhibited the recrystallization of the starch molecules. Moreover, the addition of the extracts affected the mechanical properties and water vapor permeability of the composite membrane, and it also reduced the glass transition temperature of the composite films. Furthermore, the addition of the extracts improved the biological activity of the composite films, the antioxidant and antibacterial properties of the composite films. The results could provide the theoretical basis for the production and application of the ethanol extract of black soybean coat/corn starch/carrageenan composite films.

参考文献

[1] HAMDAN M A, RAMLI N A, OTHMAN N A, et al.Characterization and property investigation of microcrystalline cellulose (MCC) and carboxymethyl cellulose (CMC) filler on the carrageenan-based biocomposite film[J].Materials Today:Proceedings, 2021, 42:56-62.
[2] SANDHU K S, SHARMA L, KAUR M, et al.Physical, structural and thermal properties of composite edible films prepared from pearl millet starch and carrageenan gum:Process optimization using response surface methodology[J].International Journal of Biological Macromolecules, 2020, 143:704-713.
[3] YUAN G Q, JIA Y N, PAN Y X, et al.Preparation and characterization of shrimp shell waste protein-based films modified with oolong tea, corn silk and black soybean seed coat extracts[J].Polymer Testing, 2020, 81:106235.
[4] WANG X C, YONG H M, GAO L, et al.Preparation and characterization of antioxidant and pH-sensitive films based on chitosan and black soybean seed coat extract[J].Food Hydrocolloids, 2019, 89:56-66.
[5] SUKHIJA S, SINGH S, RIAR C S.Analyzing the effect of whey protein concentrate and Psyllium husk on various characteristics of biodegradable film from Lotus(Nelumbo nucifera) rhizome starch[J].Food Hydrocolloids, 2016, 60:128-137.
[6] MU C D, GUO J M, LI X Y, et al.Preparation and properties of dialdehyde carboxymethyl cellulose crosslinked gelatin edible films[J].Food Hydrocolloids, 2012, 27(1):22-29.
[7] 郭开红, 张蕾蕾, 吴晓翠, 等.鲢鱼皮明胶-海藻酸钠复合膜的制备与性能[J].食品科学, 2018, 39(7):243-248.
GUO K H, ZHANG L L, WU X C, et al.Preparation and properties of silver carp skin gelatin-sodium alginate composite films[J].Food Science, 2018, 39(7):243-248.
[8] 徐晶. 多酚改性胶原纤维-淀粉复合膜的制备及性能研究[D].福州:福建农林大学, 2019.
XU J.Preparation and properties of collagen fiber-starch composite films incorporated with polyphenol[D].Fuzhou:Fujian Agriculture and Forestry University, 2019.
[9] 王丽岩. 壳聚糖基活性包装膜的性能及其在食品贮藏中应用的研究[D].长春:吉林大学, 2013.
WANG L Y.Studies on performance of chitosan based activity packaging films and applications in food storage[D].Changchun:Jilin University, 2013.
[10] MAR AM ADILAH Z, NUE HANANI Z R.Storage stability of soy protein isolate films incorporated with mango kernel extract at different temperature[J].Food Hydrocolloids, 2019, 87:541-549.
[11] 王存堂, 高增明, 姜辰昊, 等.黄色洋葱皮不同溶剂多酚提取物的总酚、总黄酮含量及抗氧化活性[J].食品工业科技, 2019, 40(20):325-328;339.
WANG C T, GAO Z M, JIANG C H, et al.Content of total phenols, flavonoids and its antioxidant activities of various solvent polyphenol extracts from yellow onion peel[J].Science and Technology of Food Industry, 2019, 40(20):325-328;339.
[12] PELISSARI F M, GROSSMANN M V E, YAMASHITA F, et al.Antimicrobial, mechanical, and barrier properties of cassava starch-chitosan films incorporated with oregano essential oil[J].Journal of Agricultural and Food Chemistry, 2009, 57(16):7 499-7 504.
[13] YANG N, SUN Z X, FENG L S, et al.Plastic film mulching for water-efficient agricultural applications and degradable films materials development research[J].Materials and Manufacturing Processes, 2015, 30(2):143-154.
[14] QIN Y, LIU Y P, YUAN L M, et al.Preparation and characterization of antioxidant, antimicrobial and pH-sensitive films based on chitosan, silver nanoparticles and purple corn extract[J].Food Hydrocolloids,2019, 96:102-111.
[15] SPIRIDON I, TEACĂ C A, BODÎRLĂU R, et al.Behavior of cellulose reinforced cross-linked starch composite films made with tartaric acid modified starch microparticles[J].Journal of Polymers and the Environment, 2013, 21(2):431-440.
[16] WANG K, WANG W H, YE R, et al.Mechanical properties and solubility in water of corn starch-collagen composite films:Effect of starch type and concentrations[J].Food Chemistry, 2017, 216:209-216.
[17] PAWLAK A, MUCHA M.Thermogravimetric and FTIR studies of chitosan blends[J].Thermochimica Acta, 2003, 396(1-2):153-166.
[18] MEDINA-JARAMILLO C, BERNAL C, FAMá L.Influence of green tea and basil extracts on cassava starch based films as assessed by thermal degradation, crystalline structure, and mechanical properties[J].Starch-Stärke, 2020, 72(3-4):1900155.
[19] 冯健, 刘文秀, 林亚玲, 等.淀粉抗回生的研究进展[J].食品科学, 2011, 32(9):335-339.
FENG J, LIU W X, LIN Y L, et al.Advance and application prospect in starch anti-retrogradation[J].Food Science, 2011, 32(9):335-339.
[20] KOWALCZYK D, SZYMANOWSKA U, SKRZYPEK T, et al.Corn starch and methylcellulose edible films incorporated with fireweed (Chamaenerion angustifolium L.) extract:Comparison of physicochemical and antioxidant properties[J].International Journal of Biological Macromolecules, 2021, 190:969-977.
[21] OTHMAN S H, NORDIN N, AZMAN N A A, et al.Effects of nanocellulose fiber and thymol on mechanical, thermal, and barrier properties of corn starch films[J].International Journal of Biological Macromolecules, 2021, 183:1 352-1 361.
[22] 曹亚飞, 凌健斌, 黄强.明胶/淀粉可食性复合膜研究进展[J].粮食与饲料工业, 2015,(1):20-22;27.
CAO Y F, LING J B, HUANG Q.Edible composite films based on gelatin and starch[J].Cereal & Feed Industry, 2015,(1):20-22;27.
[23] PAN Y M, WANG K, HUANG S Q, et al.Antioxidant activity of microwave-assisted extract of longan (Dimocarpus Longan Lour.) peel[J].Food Chemistry, 2008, 106(3):1 264-1 270.
[24] WANG C, XIE Y L.Interaction of protein isolate with anthocyanin extracted from black soybean and its effect on the anthocyanin stability[J].Journal of Food Science, 2019, 84(11):3 140-3 146.
[25] 卢俊宇, 朱芮, 吴贺君, 等.茶多酚对可食性马铃薯淀粉/海藻酸钠复合膜性能影响及表征[J].核农学报, 2020, 34(10):2 226-2 234.
LU J Y, ZHU R, WU H J, et al.Effect of tea polyphenols on the properties of edible potato starch/sodium alginate composite films[J].Journal of Nuclear Agricultural Sciences, 2020, 34(10):2 226-2 234.
[26] ZHANG X, LIU J, YONG H M, et al.Development of antioxidant and antimicrobial packaging films based on chitosan and mangosteen (Garcinia mangostana L.) rind powde[J].International Journal of Biological Macromolecules, 2020, 145:1 129-1 139.
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