食品与发酵工业 >

2022 , Vol. 48 >Issue 13: 285 - 289

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.028912

分析与检测

紫穗槐蜂蜜理化指标及挥发性成分测定与分析

  • 王桃红 ,
  • 祖铁红 ,
  • 郑军红 ,
  • 贾光群 ,
  • 曹彦忠 ,
  • 陈辉 ,
  • 崔宗岩
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  • 1(秦皇岛海关技术中心,河北 秦皇岛,066004)
    2(山东宝来利来生物工程股份有限公司,山东 泰安,271000)
    3(中国检验检疫科学研究院,北京,100176)
第一作者：硕士(崔宗岩高级工程师为通信作者,E-mail:ciqqhd@126.com)

收稿日期: 2021-08-04

  修回日期: 2021-08-30

  网络出版日期: 2022-08-03

基金资助

海关总署科研项目(2019HK090)

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Determination and analysis of physicochemical parameters and volatile compounds in Amorpha fruticosa honey

  • WANG Taohong ,
  • ZU Tiehong ,
  • ZHENG Junhong ,
  • JIA Guangqun ,
  • CAO Yanzhong ,
  • CHEN Hui ,
  • CUI Zongyan
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  • 1(Technology Center of Qinhuangdao Customs, Qinhuangdao 066004, China)
    2(Shandong BaoLai-LeeLai Bioengineering Co.Ltd., Tai’an 271000, China)
    3(Chinese Academy of Inspection and Quarantine, Beijing 100176, China)

Received date: 2021-08-04

  Revised date: 2021-08-30

  Online published: 2022-08-03

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摘要

为研究中国特色紫穗槐蜂蜜的品质特性,采用现有标准方法对紫穗槐蜜的理化指标(水分、酸度、淀粉酶值、5-羟甲基糠醛、还原糖、蔗糖)进行测定。采用顶空固相微萃取气相色谱-质谱技术对紫穗槐蜜的挥发性成分进行测定。通过对理化指标和挥发性成分进行分析,结果表明,8批紫穗槐蜂蜜样品水分含量为15.5%~17.8%,酸度为14.8~25.8 mL/kg,淀粉酶值为27.2~70.6 mL/(g·h),5-羟甲基糠醛含量不超过28.7 mg/kg,还原糖含量为65.9%~71.1%,蔗糖含量不超过2.42%,各项指标均符合国家和行业标准要求。紫穗槐蜂蜜中共发现挥发性物质78种,主要包括醛类、醇类、酸类、萜烯类、芳香类等,含量较高的物质为苯乙醇、苯乙醛、壬醛等。综合而言,紫穗槐蜂蜜具有酶值高、挥发性成分丰富的特点。

关键词： 紫穗槐蜜; 理化指标; 挥发性成分; 顶空固相微萃取; 气相色谱-质谱法

本文引用格式

王桃红 , 祖铁红 , 郑军红 , 贾光群 , 曹彦忠 , 陈辉 , 崔宗岩 . 紫穗槐蜂蜜理化指标及挥发性成分测定与分析[J]. 食品与发酵工业, 2022 , 48(13) : 285 -289 . DOI: 10.13995/j.cnki.11-1802/ts.028912

Abstract

The physical and chemical parameters of Amorpha fruticosa honey were determined based on several published standards in this study. The volatile compounds in A. fruticosa honey were detected by headspace solid-phase micro-extraction coupled with gas chromatography and mass spectrometry. The results showed that the contents of moisture, acidity, diastase number were in the range of 15.5%-17.8%, 14.8-25.8 mL/kg, 27.2-70.6 mL/(g·h), respectively. The 5-hydroxymethylfurfural concentration was less than 28.7 mg/kg. The sum of the fructose and the glucose ranged from 65.9% to 71.1%, and the sucrose content was less than 2.42%. The physical and chemical parameters of A. fruticosa honey all meet the requirements of national and industry standards. Seventy-eight different volatile compounds were tentatively identified in A. fruticosa honey, and the aldehydes, alcohols, acids, terpenes, and aromatics were the main components of volatile compounds, and the dominant compounds were phenylethyl alcohol, benzeneacetaldehyde and nonanal. In summary, the A. fruticosa honey has the characteristics of high diastase and abundant volatile compounds.

Key words： Amorpha fruticosa honey; physical and chemical parameters; volatile compounds; headspace solid phase microextraction (HS-SPME); GC-MS

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