食品与发酵工业 >

2024 , Vol. 50 >Issue 1: 232 - 240

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.033572

研究报告

贻贝蒸煮液美拉德反应制备海鲜调味基料工艺研究及其挥发性风味分析

  • 柯志刚 ,
  • 吴涛 ,
  • 陈慧 ,
  • 周绪霞 ,
  • 金友定 ,
  • 戴央章 ,
  • 邓尚贵 ,
  • 周小敏 ,
  • 丁玉庭 ,
  • 刘书来 ,
  • 相兴伟
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  • 1(浙江工业大学 食品科学与工程学院,浙江 杭州,310014)
    2(浙江省深蓝渔业资源高效开发利用重点实验室,浙江 杭州,310014)
    3(国家远洋水产品加工技术研发分中心(杭州),浙江 杭州,310014)
    4(海洋食品精深加工关键技术省部共建协同创新中心,大连工业大学,辽宁 大连,116034)
    5(嵊泗县景晟贻贝产业发展有限公司,浙江 嵊泗,316000)
    6(浙江海洋大学 食品与药学学院,浙江 舟山,316000)
    7(浙江兴业集团有限公司,浙江 舟山,316000)
    8(宁海县浙工大科学技术研究院,浙江 宁波,315600)
第一作者:博士,副研究员(相兴伟教授为通信作者,E-mail:xxw11086@zjut.edu.cn)

收稿日期: 2022-09-08

  修回日期: 2022-10-11

  网络出版日期: 2024-01-31

基金资助

国家重点研发计划项目(2020YFD0900902);舟山科技项目(2023C61001)

收起

Study on preparation of seafood-like seasoning base by Maillard reaction from mussel cooking liquid and analysis of volatile flavor compounds

  • KE Zhigang ,
  • WU Tao ,
  • CHEN Hui ,
  • ZHOU Xuxia ,
  • JIN Youding ,
  • DAI Yangzhang ,
  • DENG Shanggui ,
  • ZHOU Xiaomin ,
  • DING Yuting ,
  • LIU Shulai ,
  • XIANG Xingwei
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  • 1(College of Food Science and Technology, Zhejiang University of Technology, Hangzhou 310014, China)
    2(Key Laboratory of Marine Fishery Resources Exploitment & Utilization of Zhejiang Province, Hangzhou 310014, China)
    3(National R&D Branch Center for Pelagic Aquatic Products Processing (Hangzhou), Hangzhou 310014, China)
    4(Collaborative Innovation Center of Seafood Deep Processing, Dalian Polytechnic University, Dalian 116034, China)
    5(Shengsi County Jingsheng Mussel Industry Development Co.Ltd., Shengsi 316000, China)
    6(College of Food Science and Pharmacy, Zhejiang Ocean University, Zhoushan 316000, China)
    7(Zhejiang Xingye Industrial Group Co.Ltd., Zhoushan 316000, China)
    8(Ninghai ZJUT Academy of Science Technology, Ningbo 315600, China)

Received date: 2022-09-08

  Revised date: 2022-10-11

  Online published: 2024-01-31

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摘要

为提高贻贝加工过程中产生的副产物利用率,该文以贻贝蒸煮液为原料,经浓缩、酶解后进行美拉德反应,以期制备一种贻贝风味的调味基料。通过单因素试验结合Friedman排序检验法、吸光度测定和响应曲面结合模糊数学感官评价法,探究贻贝蒸煮酶解液美拉德反应最佳工艺条件,并采用GC-MS测定美拉德反应产物的挥发性风味成分。结果表明,贻贝蒸煮液美拉德反应的最佳条件为:还原糖添加量3%(质量分数)、反应温度115 ℃、反应时间2 h、反应初始pH 7.5。GC-MS分析结果显示,醛类、酮类是美拉德反应产物的主要风味物质,吡嗪类、呋喃类等物质丰富了风味层次,提高了美拉德反应产物的整体香气。该研究结果可为贻贝加工副产物高值化利用提供一定参考。

关键词： 贻贝蒸煮液; 美拉德反应; 模糊数学; GC-MS

本文引用格式

柯志刚 , 吴涛 , 陈慧 , 周绪霞 , 金友定 , 戴央章 , 邓尚贵 , 周小敏 , 丁玉庭 , 刘书来 , 相兴伟 . 贻贝蒸煮液美拉德反应制备海鲜调味基料工艺研究及其挥发性风味分析[J]. 食品与发酵工业, 2024 , 50(1) : 232 -240 . DOI: 10.13995/j.cnki.11-1802/ts.033572

Abstract

To prepare a mussel-like seasoning base, mussel cooking liquid was concentrated and enzymatically hydrolyzed, and then carried out by Maillard reaction in this study. The optimal conditions for the Maillard reaction were determined through a single-factor experiment combined with the Friedman ranking test, absorbance measurement, response surface optimization, and fuzzy mathematical sensory evaluation. Results showed that the optimal conditions for the Maillard reaction were 3% reducing sugar, a reaction temperature of 115 ℃, a reaction time of 2 h, and an initial pH of 7.5. Analysis of the volatile compounds in the Maillard reaction product by GC-MS showed that aldehydes and ketones were the main volatile flavor compounds, and pyrazines, furans, and other compounds enriched the overall aroma of the Maillard reaction products. The results in this work provide a reference for the high-value utilization of mussel processing by-products.

Key words： mussel cooking liquid; Maillard reaction; fuzzy mathematics; GC-MS

参考文献

[1] PANAYOTOVA V, MERDZHANOVA A, STANCHEVA R, et al.Farmed mussels (Mytilus galloprovincialis) from the Black Sea reveal seasonal differences in their neutral and polar lipid fatty acids profile[J].Regional Studies in Marine Science, 2021, 44:101782.
[2] 陶美洁, 孟粉, 董烨, 等.贻贝蒸煮液酶解工艺的优化[J].中国食品学报, 2020, 20(12):209-220.
TAO M J, MENG F, DONG Y, et al.Optimization of enzymatic hydrolysis conditions of mussel cooking liquor[J].Journal of Chinese Institute of Food Science and Technology, 2020, 20(12):209-220.
[3] 王欣, 孙孟辉, 霍健聪, 等.贻贝蒸煮液添加对酱油品质的影响[J].食品工业, 2020, 41(9):146-150.
WANG X, SUN M H, HUO J C, et al.Effect of boiling mussel juice addition on quality of soy sauce[J].The Food Industry, 2020, 41(9):146-150.
[4] ZHANG N L, YANG Y F, WANG W L, et al.A potential flavor seasoning from aquaculture by-products:An example of Takifugu obscurus[J].LWT, 2021, 151:112160.
[5] 侯钰柯, 蒋宇飞, 康明丽, 等.美拉德反应制备鸡肉风味基料工艺优化及呈味特性分析[J].食品与发酵工业, 2022, 48(17):198-206.
HOU Y K, JIANG Y F, KANG M L, et al.Optimization of Maillard reaction for the preparation of chicken flavor base material and the analysis of its flavor[J].Food and Fermentation Industries, 2022, 48(17):198-206.
[6] 韩科研, 黄继超, 刘冬梅, 等.鸭骨汤酶解液的美拉德反应条件优化[J].食品科学, 2018, 39(4):261-267.
HAN K Y, HUANG J C, LIU D M, et al.Optimization of Maillard reaction conditions for enzymatic hydrolysate of duck bone protein[J].Food Science, 2018, 39(4):261-267.
[7] CHIANG J H, EYRES G T, SILCOCK P J, et al.Changes in the physicochemical properties and flavour compounds of beef bone hydrolysates after Maillard reaction[J].Food Research International, 2019, 123:642-649.
[8] LAN X H, LIU P, XIA S Q, et al.Temperature effect on the non-volatile compounds of Maillard reaction products derived from xylose-soybean peptide system:Further insights into thermal degradation and cross-linking[J].Food Chemistry, 2010, 120(4):967-972.
[9] XU Y Y, XIANG P, QIU W Q, et al.Dielectric properties of the Maillard reaction solution formed between enzymatic hydrolysate of Antarctic krill and glucose under microwave heating[J].LWT, 2022, 161:113355.
[10] XIAO Q, WOO M W, HU J W, et al.The role of heating time on the characteristics, functional properties and antioxidant activity of enzyme-hydrolyzed rice proteins-glucose Maillard reaction products[J].Food Bioscience, 2021, 43:101225.
[11] 邢贵鹏, 孙申宇, 黄卉, 等.美拉德反应改良罗非鱼加工副产物熬煮液风味[J].食品与发酵工业, 2022, 48(5):165-172.
XING G P, SUN S Y, HUANG H, et al.Flavor improvement of tilapia-broth extraction by Maillard reaction[J].Food and Fermentation Industries, 2022, 48(5):165-172.
[12] ZHANG Z Y, ELFALLEH W, HE S D, et al.Heating and cysteine effect on physicochemical and flavor properties of soybean peptide Maillard reaction products[J].International Journal of Biological Macromolecules, 2018, 120:2137-2146.
[13] KAEWTATHIP T, WATTANA-AMORN P, BOONSUPTHIP W, et al.Maillard reaction products-based encapsulant system formed between chitosan and corn syrup solids:Influence of solution pH on formation kinetic and antioxidant activity[J].Food Chemistry, 2022, 393:133329.
[14] CAO J R, YAN H X, LIU L.Optimized preparation and antioxidant activity of glucose-lysine Maillard reaction products[J].LWT, 2022, 161:113343.
[15] HAN J R, YAN J N, SUN S G, et al.Characteristic antioxidant activity and comprehensive flavor compound profile of scallop (Chlamys farreri) mantle hydrolysates-ribose Maillard reaction products[J].Food Chemistry, 2018, 261:337-347.
[16] TIAN H Y, ZHANG J, SUN B G, et al.Preparation of natural isovaleraldehyde by the Maillard reaction[J].Chinese Chemical Letters, 2007, 18(9):1049-1052.
[17] GAO X L, FENG T, SHENG M J, et al.Characterization of the aroma-active compounds in black soybean sauce, a distinctive soy sauce[J].Food Chemistry, 2021, 364:130334.
[18] WANG Y Q, LI C S, ZHAO Y Q, et al.Novel insight into the formation mechanism of volatile flavor in Chinese fish sauce (Yu-lu) based on molecular sensory and metagenomics analyses[J].Food Chemistry, 2020, 323:126839.
[19] YE Y K, YE S S, WANYAN Z X, et al.Producing beef flavors in hydrolyzed soybean meal-based Maillard reaction products participated with beef tallow hydrolysates[J].Food Chemistry, 2022, 378:132119.
[20] ZHANG X R, GUAN H, ZHAO Q, et al.Effect of thermal treatment on the flavor quality of Chinese spicy cabbage[J].Food Control, 2023, 144:109338.
[21] XI J Z, XU D, WU F F, et al.The aroma compounds of Chinese steamed bread fermented with sourdough and instant dry yeast[J].Food Bioscience, 2020, 38:100775.
[22] YU P, YANG Y N, SUN J Y, et al.Identification of volatile sulfur-containing compounds and the precursor of dimethyl sulfide in cold-pressed rapeseed oil by GC-SCD and UPLC-MS/MS[J].Food Chemistry, 2022, 367:130741.
[23] SUN A, WU W, SOLADOYE O P, et al.Maillard reaction of food-derived peptides as a potential route to generate meat flavor compounds:A review[J].Food Research International, 2022, 151:110823.
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