研究报告

浓香型白酒窖泥特性与原酒风味品质相关性分析

  • 简何 ,
  • 简江 ,
  • 周娜 ,
  • 简晓平 ,
  • 喻顶松 ,
  • 马绍坤 ,
  • 王松
展开
  • 1(宜宾学院 农林与食品工程学部,四川 宜宾,644000)
    2(四川省宜宾高洲酒业有限责任公司,四川 宜宾,645178)
第一作者:学士,高级工程师(王松副教授为通信作者,E-mail:wangsongybxy@yibinu.edu.cn)

收稿日期: 2025-10-22

  修回日期: 2025-12-29

  网络出版日期: 2026-09-10

基金资助

宜宾学院启航计划项目(2023QH21)

Correlation analysis between characteristics of pit mud and flavor quality of Nongxiangxing Baijiu

  • JIAN He ,
  • JIAN Jiang ,
  • ZHOU Na ,
  • JIAN Xiaoping ,
  • YU Dingsong ,
  • MA Shaokun ,
  • WANG Song
Expand
  • 1(Faculty of Agriculture, Forestry and Food Engineering, Yibin University, Yibin 644000, China)
    2(Sichuan Yibin Gaozhou liquor Co.Ltd., Yibin 645178, China)

Received date: 2025-10-22

  Revised date: 2025-12-29

  Online published: 2026-09-10

摘要

采集宜宾某酒企15个窖池的窖泥样品,分析其理化指标,采用高通量测序法检测其细菌区系,同时采用感官及色谱分析检测其对应窖池原酒的感官特征及挥发性风味物质含量,关联分析窖泥特性与原酒风味指标。研究发现,窖泥滴定酸、速效磷含量对原酒感官评分及挥发性风味物质含量影响较大。进一步分析发现,窖泥中发酵单胞菌属(Fermentimonas)、Clostridium_sensu_stricto_12、己酸菌属(Caproiciproducens)、厌氧孢杆菌属(Anaerosporobacter)、norank_f__Caloramatoraceae与白酒感官评分显著相关,特别是Clostridium_sensu_stricto_12、Fermentimonas、氨基酸杆菌属(Aminobacterium)、norank_f__Caloramatoraceae与至少3种挥发性风味物质含量显著相关;窖泥中的辛酸、庚酸、戊酸对原酒感官评分有显著影响,而辛酸、庚酸、戊酸、丁酸、癸酸乙酯、庚酸乙酯对原酒挥发性风味物质含量有显著影响。结果表明,浓香型白酒窖泥特性指标与原酒风味品质之间存在量比关系,可用于窖泥质量评价。

本文引用格式

简何 , 简江 , 周娜 , 简晓平 , 喻顶松 , 马绍坤 , 王松 . 浓香型白酒窖泥特性与原酒风味品质相关性分析[J]. 食品与发酵工业, 2026 , 52(16) : 315 -323 . DOI: 10.13995/j.cnki.11-1802/ts.044906

Abstract

Fifteen pit mud samples were collected from the fermentation pits of a liquor enterprise in Yibin.The physicochemical properties were analyzed, and bacterial community composition was detected using high-throughput sequencing.Simultaneously, sensory evaluation and chromatographic analysis were conducted to detect the sensory characteristics and volatile flavor compound contents of the corresponding pit crude Baijiu.Correlation analysis was performed to examine the relationships between pit mud properties and crude Baijiu flavor quality.The results showed that titratable acidity and available phosphorus content in pit mud significantly influenced both sensory scores and concentrations of volatile flavor compounds in crude Baijiu.Further analysis revealed that Fermentimonas, Clostridium_sensu_stricto_12, Capriciproducens, Anaerosporobacter, and norank_f__Caloramatoraceae were significantly correlated with sensory scores, while Clostridium_sensu_stricto_12, Fermentimonas, Aminobacterium, and norank_f__Caloramatoraceae were significantly associated with at least three volatile flavor compounds.Additionally, octanoic acid, heptanoic acid, and valeric acid concentrations in pit mud substantially enhanced the sensory scores of crude Baijiu.These compounds, along with butyric acid, ethyl decanoate, and ethyl heptanoate, significantly influenced the overall volatile flavor profile.Collectively, these findings establish quantifiable relationships between specific pit mud characteristics and crude Baijiu flavor quality in Nongxiangxing Baijiu, thus providing a scientific basis for pit mud quality evaluation.

参考文献

[1] SUN L J, ZHANG X F, LI X S, et al.Quality control strategies for pit mud based on the synergistic effects of flavor, microorganisms and physicochemical factors[J].Foods, 2025, 14(19):3326.
[2] YAN S B, JIA Y L, ZHANG Q, et al.Bacterial diversity associated with volatile compound accumulation in pit mud of Chinese strong-flavor Baijiu pit[J].AMB Express, 2023, 13(1):3.
[3] 邹斐, 叶力, 冯亮, 等.窖泥微生物多样性及窖泥评价与养护研究进展[J].食品科学, 2024, 45(16):320-328.
ZOU F, YE L, FENG L, et al.Research progress on microbial diversity, evaluation and maintenance of Baijiu pit mud[J].Food Science, 2024, 45(16):320-328.
[4] 李学思, 李绍亮, 曹振华, 等.窖池自然老熟过程中窖泥理化指标及产酒质量变化规律的研究[J].酿酒, 2019, 46(3):31-35.
LI X S, LI S L, CAO Z H, et al.Study on the change of physicochemical indexes and quality of wine produced in pit mud during natural aging[J].Liquor Making, 2019, 46(3):31-35.
[5] 游玲, 简晓平, 范方勇, 等.宜宾浓香型白酒产区窖泥生态监测[J].生物技术通报, 2023, 39(7):254-265.
YOU L, JIAN X P, FAN F Y, et al.Ecological monitoring of pit mud in Yibin strong-fragrance Baijiu producing region[J].Biotechnology Bulletin, 2023, 39(7):254-265.
[6] 吴浪涛, 丁文骏, 谢专, 等.不同时期窖泥理化因子、风味物质和细菌组成的相关性[J].微生物学通报, 2022, 49(3):1030-1047.
WU L T, DING W J, XIE Z, et al.Characterization and correlation analysis of the bacterial composition, physicochemical properties and volatiles in Baijiu fermentation pit mud of different ages[J].Microbiology China, 2022, 49(3):1030-1047.
[7] HU X L, DU H, REN C, et al.Illuminating anaerobic microbial community and cooccurrence patterns across a quality gradient in Chinese liquor fermentation pit muds[J].Applied and Environmental Microbiology, 2016, 82(8):2506-2515.
[8] 毕天然, 黄钧, 张宿义, 等.不同窖龄及位置窖泥微生物群落和代谢组分的差异[J].食品与发酵工业, 2022, 48(2):231-237.
BI T R, HUANG J, ZHANG S Y, et al.Difference of the microbial community and metabolite in pit mud with different age and position[J].Food and Fermentation Industries, 2022, 48(2):231-237.
[9] 孟雅静, 王艳丽, 丁峰, 等.浓香型白酒新、老窖池分层池底窖泥菌群总氢代谢与乳酸含量之间的关系[J].食品科学, 2021, 42(18):171-177.
MENG Y J, WANG Y L, DING F, et al.Relationship between microbial total hydrogen metabolism and lactic acid content in layered bottom pit muds from old and young pits used for the production of strong-flavor Baijiu[J].Food Science, 2021, 42(18):171-177.
[10] 党喆, 张永利, 金成勇.凤型酒新老窖泥微生物多样性、理化指标及其相关性分析[J].酿酒科技, 2024(10):80-85.
DANG Z, ZHANG Y L, JIN C Y.Microbial diversity, physicochemical indexes and their correlation analysis of new and old pit mud of Fengxiang Baijiu[J].Liquor-Making Science & Technology, 2024(10):80-85.
[11] ZHOU W, LIAO Z M, WU Z Y, et al.Analysis of the difference between aged and degenerated pit mud microbiome in fermentation cellars for Chinese Luzhou-flavor Baijiu by metatranscriptomics[J].Journal of the Science of Food and Agriculture 2021, 101(11):4621-4631.
[12] 王艳丽, 孟雅静, 何宏魁, 等.不同品质浓香型窖泥理化因子与细菌总量的相关性[J].食品与发酵工业, 2019,45(3):89-94.
WANG Y L, MENG Y J, HE H K, et al.Correlation between physicochemical factors and total bacterial count in different grades of Nongxiang flavored pit mud[J].Food and Fermentation Industries, 2019,45(3):89-94.
[13] 刘梅, 邓杰, 谢军, 等.基于微生物群落结构相关的窖泥品质理化指标的筛选[J].食品科学, 2018, 39(19):44-50.
LIU M, DENG J, XIE J, et al.Screening of physicochemical quality indexes of pit mud based on correlation with microbial community structure[J].Food Science, 2018, 39(19):44-50.
[14] 于学健, 郑佳, 张哲, 等.基于知识图谱的浓香型白酒酿造微生物可视化分析[J].食品与发酵工业, 2024, 50(7):389-399.
YU X J, ZHENG J, ZHANG Z, et al.Visual analysis of strong-flavor Baijiu fermentation microorganisms based on mapping knowledge domain[J].Food and Fermentation Industries, 2024, 50(7):389-399.
[15] CHEN L, LI Y Z, JIN L, et al.Analyzing bacterial community in pit mud of Yibin Baijiu in China using high throughput sequencing[J].PeerJ, 2020, 8:e9122-e00222.
[16] FANG G Y, CHAI L J, ZHONG X Z, et al.Comparative genomics unveils the habitat adaptation and metabolic profiles of Clostridium in an artificial ecosystem for liquor production[J].mSystems, 2022, 7(3):e0029722.
[17] 吴小丽, 刘桂民, 李新星, 等.CCI多传感器组合土壤水分产品在青藏高原不同地区的适用性[J].土壤, 2021, 53(2):429-438.
WU X L, LIU G M, LI X X, et al.Applicability assessment of multi-sensor CCI soil moisture products in different areas of Qinghai-Tibetan plateau[J].Soils, 2021, 53(2):429-438.
[18] 谷穗, 李贵传, 龙建, 等.一种野外用土壤氮磷钾快速检测装置:中国, CN 202020877564.4[P].2020-12-15.
GU H, LI G C, LONG J, et al.A rapid detection device for soil nitrogen, phosphorus and potassium for field use:China, CN 202020877564.4[P].2020-12-15.
[19] 陈成, 张西良, 张亚磊, 等.栽培基质超亲水pH传感器测量误差影响因素分析与补偿[J].农业机械学报, 2023, 54(3):356-362.
CHEN C, ZHANG X L, ZHANG Y L, et al.Influence and compensation of soilless culture substrates on pH value detection by using super-hydrophilic pH sensor[J].Transactions of the Chinese Society for Agricultural Machinery, 2023, 54(3):356-362.
[20] 郭新明, 林德钰, 陈伟.数能一体化能量自治无线传感器网络:机遇与挑战[J].传感技术学报, 2023, 36(8):1171-1183.
GUO X M, LIN D Y, CHEN W.Energy sustainable wireless information and power transfer sensor networks:Opportunities and challenges[J].Chinese Journal of Sensors and Actuators, 2023, 36(8):1171-1183.
[21] 董成亮, 冯秀娟, 刘增源.土壤VOCs在线监测装置:中国, CN202210699382.6[P].2022-10-11.
DONG C L, FENG X J, LIU Z Y.Soil VOCs online monitoring device:China, CN202210699382.6[P].2022-10-11.
[22] 刘念, 彭奎, 潘建军, 等.浓香型白酒窖池价值评估体系研究(一):窖池的价值构成及影响因素[J].食品与发酵科技, 2021, 57(6):1-3.
LIU N, PENG K, PAN J J, et al.Study on assessment system of strong flavor Baijiu fermentation pit:The value composition of pit and its influencing factors[J].Sichuan Food and Fermentation, 2021, 57(6):1-3.
[23] 田建平, 朱敏, 罗惠波, 等.基于高光谱图像技术的窖泥水分预测模型建立的方法:中国, CN201910853788.3[P].2021-12-28.
TIAN J P, ZHU M, LUO H B, et al.A method for establishing a moisture prediction model of pit mud based on hyperspectral image technology:China, CN201910853788.3[P].2021-12-28.
[24] 罗惠波, 朱敏, 黄丹, 等.基于高光谱图像技术的窖泥总酸预测模型建立的方法:中国, CN201910854782.8[P].2021-12-28.
LUO H B, ZHU M, HUANG D, et al.A method for establishing a prediction model of total acid in pit mud based on hyperspectral image technology:China, CN201910854782.8[P].2021-12-28.
[25] 郭立家, 汤有宏, 高家坤.白酒智能酿造生产管理系统构建的探讨[J].酿酒, 2022,49(2):33-37.
GUO L J, TANG Y H, GAO J K.Discussion on the construction of Baijiu intelligent brewing production management system[J].Liquor Making, 2022,49(2):33-37.
[26] REN H W, LI Z J, ZHOU Q, et al.Multi-omics analysis of microbial spatiotemporal succession and metabolite differences in pit mud of varying cellar ages and spatial positions[J].Food Chemistry:X, 2025, 26:102287.
[27] JIAO K R, DENG B, SONG P, et al.The effects of iron-bearing minerals on the community diversity and physiological activity of prokaryotic microorganisms in pit mud used for strong-flavor Baijiu production[J].Foods, 2025, 14(11):1883.
[28] 刘治国, 方超, 张晓元, 等.浓香型白酒窖泥理化因子、微生物群落、感官质量以及相关性研究进展[J].食品科学, 2023, 44(21):351-358.
LIU Z G, FANG C, ZHANG X Y, et al.Research progress on physicochemical factors, microbial community and sensory quality of Nongxiangxing Baijiu pit mud and correlation among them[J].Food Science, 2023, 44(21):351-358.
[29] WANG Y, FEI Y L, TAO Y, et al.Assembly mechanisms and function features of prokaryotic communities in artificial pit mud related to soil type and inoculum[J].International Journal of Food Microbiology, 2025, 439:111232.
[30] LI Z H, ZHAO C, MAO Z Y, et al.Structure and metabolic function of spatiotemporal pit mud microbiome[J].Environmental Microbiome, 2025, 20(1):10.
文章导航

/

〈 〉