研究报告

超高压处理对“和尚头”小麦淀粉结构和特性的影响

  • 张晓萌 ,
  • 陈金凤 ,
  • 李建刚 ,
  • 陈瑞喜 ,
  • 周治屹 ,
  • 张盛贵
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  • 1(甘肃农业大学 理学院,甘肃 兰州,730070)
    2(甘肃农业大学 食品科学与工程学院,甘肃 兰州,730070)
第一作者:硕士研究生(张盛贵教授为通信作者,E-mail:zhangshenggui@gsau.edu.cn)

收稿日期: 2022-10-31

  修回日期: 2023-02-01

  网络出版日期: 2024-04-17

基金资助

中央引导地方科技发展专项(ZCYD-2020);甘肃农业大学优秀博士学位论文培育项目(YB2022002)

Effect of ultra-high pressure treatment on starch structure and properties of Heshangtou wheat

  • ZHANG Xiaomeng ,
  • CHEN Jinfeng ,
  • LI Jiangang ,
  • CHEN Ruixi ,
  • ZHOU Zhiyi ,
  • ZHANG Shenggui
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  • 1(College of Science, Gansu Agricultural University, Lanzhou 730070, China)
    2(College of Food Science and Engineering, Gansu Agricultural University, Lanzhou 730070, China)

Received date: 2022-10-31

  Revised date: 2023-02-01

  Online published: 2024-04-17

摘要

该文以西北特产的旱地“和尚头”小麦粉为材料,采用超高压处理对小麦淀粉进行改性,并研究改性淀粉的结构和特性。实验结果表明,与原淀粉相比,100~400 MPa处理下,小颗粒淀粉所占的比重增加(P<0.05),随着处理压力的增加,淀粉颗粒膨胀和聚集,粒径变大;400 MPa处理下的溶解度和膨胀度分别比原淀粉降低了27.32%和8.84%;100 MPa压力处理后,淀粉的TOTPTC及ΔH均显著下降(P<0.05),处理压力达到400 MPa以上,检测不到热力学相关数据,表明此条件下小麦淀粉可能完全凝胶化。综上,压力超过400 MPa时,改性淀粉的结构和特性变化显著。

本文引用格式

张晓萌 , 陈金凤 , 李建刚 , 陈瑞喜 , 周治屹 , 张盛贵 . 超高压处理对“和尚头”小麦淀粉结构和特性的影响[J]. 食品与发酵工业, 2024 , 50(6) : 138 -143 . DOI: 10.13995/j.cnki.11-1802/ts.034152

Abstract

In this paper, the special dryland Heshangtou wheat flour in Northwest China was used as the material to modify the wheat starch with ultra-high pressure equipment, and the structure and characteristics of the modified starch were studied.The experimental results showed that compared with the original starch, the proportion of small granule starch increased at 100-400 MPa (P<0.05).With the increase of treatment pressure, the starch particles expanded and gathered, and the particle size became larger.The solubility and swelling degree of 400 MPa treatment were 27.32% and 8.84% lower than that of raw starch, respectively.TO, TP, TC, and ΔH decreased significantly (P<0.05) and the treatment pressure reached more than 400 MPa.No thermodynamic data were detected, indicating that wheat starch might be completely gel under this condition.To sum up, the structure and properties of modified starch changed significantly when the ultra-high pressure exceeded 400 MPa.

参考文献

[1] LI W H, GAO J M, WU G L, et al.Physicochemical and structural properties of A-and B-starch isolated from normal and waxy wheat:Effects of lipids removal[J].Food Hydrocolloids, 2016, 60:364-373.
[2] KIM H S, HUBER K C.Simple purification (desalting) procedure to facilitate structural analysis of an alkali-solubilized/ neutralized starch solution by intermediate-pressure size-exclusion chromatography[J].Journal of Agricultural and Food Chemistry, 2007, 55(13):4944-4948.
[3] PIECYK M, DRUYŃSKA B, OŁTARZEWSKA A, et al.Effect of hydrothermal modifications on properties and digestibility of grass pea starch[J].International Journal of Biological Macromolecules, 2018, 118:2113-2120.
[4] ZHANG D L, XU H S, JIANG B, et al.Effects of ultra-high pressure on the morphological and physicochemical properties of lily starch[J].Food Science & Nutrition, 2020, 9(2):952-962.
[5] LI W H, TIAN X L, LIU L P, et al.High pressure induced gelatinization of red adzuki bean starch and its effects on starch physicochemical and structural properties[J].Food Hydrocolloids, 2015, 45:132-139.
[6] KIM S, YANG S Y, CHUN H H, et al.High hydrostatic pressure processing for the preparation of buckwheat and tapioca starch films[J].Food Hydrocolloids, 2018, 81:71-76.
[7] GUO Z B, ZENG S X, LU X, et al.Structural and physicochemical properties of lotus seed starch treated with ultra-high pressure[J].Food Chemistry, 2015, 186:223-230.
[8] LARREA-WACHTENDORFF D, TABILO-MUNIZAGA G, FERRARI G.Potato starch hydrogels produced by high hydrostatic pressure (HHP):A first approach[J].Polymers, 2019, 11(10):1673.
[9] 孙小凡, 曾庆华.小麦淀粉实验室制备工艺研究[J].粮油加工, 2008(1):96-98.
SUN X F, ZENG Q H. Study on laboratory preparation technology of wheat starch[J]. Cereals and Oils Processing, 2008(1): 96-98.
[10] 张晶, 张美莉.超高压处理对燕麦淀粉颗粒特性、热特性及流变学特性的影响[J].食品科学, 2020, 41(23):114-121.
ZHANG J, ZHANG M L.Effect of high hydrostatic pressure treatment on morphological, thermal and rheological properties of oat starch[J].Food Science, 2020, 41(23):114-121.
[11] OVANDO-MARTÍNEZ M, OSORIO-DÍAZ P, WHITNEY K, et al.Effect of the cooking on physicochemical and starch digestibility properties of two varieties of common bean (Phaseolus vulgaris L.) grown under different water regimes[J].Food Chemistry, 2011, 129(2):358-365.
[12] ZHANG B J, LI X X, LIU J, et al.Supramolecular structure of A- and B-type granules of wheat starch[J].Food Hydrocolloids, 2013, 31(1):68-73.
[13] WANG S J, YU J L, ZHU Q H, et al.Granular structure and allomorph position in c-type Chinese yam starch granule revealed by SEM, 13C CP/MAS NMR and XRD[J].Food Hydrocolloids, 2009, 23(2):426-433.
[14] 郭泽镔, 曾绍校, 郑宝东.超高压处理对莲子淀粉理化特性的影响[J].中国食品学报, 2014, 14(11):118-123.
GUO Z B, ZENG S X, ZHENG B D.Effect of ultra high pressure processing on the physicochemical properties of lotus-seed starch[J].Journal of Chinese Institute of Food Science and Technology, 2014, 14(11):118-123.
[15] ZHANG B, WU H, GOU M, et al.The comparison of structural, physicochemical, and digestibility properties of repeatedly and continuously annealed sweet potato starch[J].Journal of Food Science, 2019, 84(8):2050-2058.
[16] 张晶, 张美莉.燕麦淀粉提取工艺优化及其相关特性研究[J].食品科技, 2019, 44(9):295-302.
ZHANG J, ZHANG M L.Extraction and related properties of oat starch[J].Food Science and Technology, 2019, 44(9):295-302.
[17] LI H, WANG R R, LIU J, et al.Effects of heat-moisture and acid treatments on the structural, physicochemical, and in vitro digestibility properties of lily starch[J].International Journal of Biological Macromolecules, 2020, 148:956-968.
[18] HU X P, ZHANG B, JIN Z Y, et al.Effect of high hydrostatic pressure and retrogradation treatments on structural and physicochemical properties of waxy wheat starch[J].Food Chemistry, 2017, 232:560-565.
[19] VALLONS K J R, ARENDT E K.Effects of high pressure and temperature on buckwheat starch characteristics[J].European Food Research and Technology, 2009, 230(2):343-351.
[20] FLORES-MORALES A, JIMÉNEZ-ESTRADA M, MORA-ESCOBEDO R.Determination of the structural changes by FT-IR, Raman, and CP/MAS 13C NMR spectroscopy on retrograded starch of maize tortillas[J].Carbohydrate Polymers, 2012, 87(1):61-68.
[21] YANG Y, ZHENG S S, LI Z, et al.Influence of three types of freezing methods on physicochemical properties and digestibility of starch in frozen unfermented dough[J].Food Hydrocolloids, 2021, 115:106619.
[22] 王金荣. 退火及超高压对三种不同结晶类型的淀粉结构和功能性质的影响[D].天津:天津科技大学, 2016.
WANG J R.The effect of annealing and ultra-high pressure treatment on structural and functional of three starches with different polymorphs[D].Tianjin:Tianjin University of Science and Technology, 2016.
[23] ZHANG B J, CHEN L, LI X X, et al.Understanding the multi-scale structure and functional properties of starch modulated by glow-plasma:A structure-functionality relationship[J].Food Hydrocolloids, 2015, 50:228-236.
[24] LINDEBOOM N, CHANG P R, TYLER R T.Analytical, biochemical and physicochemical aspects of starch granule size, with emphasis on small granule starches:A review[J].Starch-Stärke, 2004, 56(3-4):89-99.
[25] ZHU F, LI H.Effect of high hydrostatic pressure on physicochemical properties of quinoa flour[J].LWT, 2019, 114:108367.
[26] LIU M, WU N N, YU G P, et al.Physicochemical properties, structural properties, and in vitro digestibility of pea starch treated with high hydrostatic pressure[J].Starch-Stärke, 2018, 70(1-2):1700082.
[27] YE J P, HU X T, ZHANG F, et al.Freeze-thaw stability of rice starch modified by improved extrusion cooking technology[J].Carbohydrate Polymers, 2016, 151:113-118.
[28] 缪铭. 慢消化淀粉的特性及形成机理研究[D].无锡:江南大学, 2009.
MIAO M.Characteristic and formation mechanism of slowly digestible starch[D].Wuxi:Jiangnan University, 2009.
[29] LI W H, BAI Y F, MOUSAA S A S, et al.Effect of high hydrostatic pressure on physicochemical and structural properties of rice starch[J].Food and Bioprocess Technology, 2012, 5(6):2233-2241.
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