食品与发酵工业 >

2024 , Vol. 50 >Issue 9: 56 - 63

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.034180

研究报告

响应曲面法优化赤藓糖醇结晶工艺

  • 郭元亨 ,
  • 皮冬伟 ,
  • 陶进 ,
  • 曹敏 ,
  • 武丽达 ,
  • 张媛 ,
  • 王小艳
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  • 1(中粮营养健康研究院有限公司,北京,102209)
    2(营养健康与食品安全北京市重点实验室,北京,102209)
    3(吉林中粮生化有限公司玉米深加工国家工程研究中心,吉林 长春,130033)
    4(武汉中粮食品科技有限公司,湖北 武汉,430415)
第一作者: 博士,高级工程师(王小艳高级工程师为通信作者,E-mail:wangxiaoyani@cofco.com)

收稿日期: 2022-11-02

  修回日期: 2022-12-20

  网络出版日期: 2024-06-11

基金资助

国家重点研发计划项目(2021YFD2101004);吉林省科技发展计划 中青年科技创新领军人才及团队项目(20200301029RQ)

收起

Crystallization process optimization of erythritol by response surface methodology

  • GUO Yuanheng ,
  • PI dongwei ,
  • TAO jin ,
  • CAO Min ,
  • WU Lida ,
  • ZHANG Yuan ,
  • WANG Xiaoyan
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  • 1(Nutrition & Health Research Institute, COFCO Corporation, Beijing 102209, China)
    2(Beijing Key Laboratory of Nutrition, Health and Food Safety, Beijing 102209, China)
    3(National Engineering Research Center of Corn Deep Processing, Jilin COFCO Biochemistry Co.Ltd., Changchun 130033, China)
    4(Wuhan COFCO Food Technology Co.Ltd., Wuhan 430415, China)

Received date: 2022-11-02

  Revised date: 2022-12-20

  Online published: 2024-06-11

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摘要

为了开发一套赤藓糖醇的结晶工艺,该文研究了包括晶种添加量、溶液初始浓度、结晶时间和结晶温度在内的4个主要因素对赤藓糖醇结晶收率的影响。然后根据单因素试验的结果,采用响应曲面法整体优化了赤藓糖醇的结晶工艺参数。响应面优化结果显示,水溶液中赤藓糖醇结晶的最优操作条件为,晶种添加量1.0%,赤藓糖醇溶液初始质量浓度550 mg/mL,结晶时间3 h,结晶温度-4.5 ℃。上述条件下,赤藓糖醇的一次结晶率为52.78%。该文得到的模型可以用来优化赤藓糖醇在水溶液体系中的结晶过程。该模型化的工艺获得了较高的赤藓糖醇结晶收率。

关键词： 赤藓糖醇; 结晶; 响应曲面法; 工艺优化

本文引用格式

郭元亨 , 皮冬伟 , 陶进 , 曹敏 , 武丽达 , 张媛 , 王小艳 . 响应曲面法优化赤藓糖醇结晶工艺[J]. 食品与发酵工业, 2024 , 50(9) : 56 -63 . DOI: 10.13995/j.cnki.11-1802/ts.034180

Abstract

To obtain a crystallization process of erythritol, the effects of four main influencing factors (including seed addition, concentration of erythritol solution, crystallizing time and temperature) on crystallization yield of erythritol were studied.Based on the results of single factor experiments, response surface methodology was carried out to optimize crystallizing process.The results showed that the optimum operating parameters were seed addition of 1%, erythritol solution of 550 mg/mL, crystallizing time of 3 h and temperature of -4.5 ℃.Under these conditions, the erythritol crystallization yield was 52.78%.The above results indicated that the optimized model can be used to crystallize erythritol in aqueous solution.The modeled process can obtain high erythritol crystallization yield.

Key words： erythritol; crystallization; response surface methodology; process optimization

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