研究报告

黑果枸杞香气成分和多酚类物质的组成研究

  • 武芸 ,
  • 程振玉 ,
  • 王丽朋 ,
  • 胡浩斌 ,
  • 胡文杰 ,
  • 蒙勇辰
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  • 1(陇东学院 石油化工学院,甘肃 庆阳,745000)
    2(陇东学院,甘肃省陇东油气资源高效利用重点实验室,甘肃 庆阳,745000)
第一作者:硕士,教授(通信作者,E-mail:405436718@qq.com)

收稿日期: 2024-02-24

  修回日期: 2024-04-15

  网络出版日期: 2024-08-02

基金资助

甘肃省自然科学基金项目(23JRRM740);庆阳市科技人才专项计划项目 (QY-STK-2022A-007,QY-STK-2023A-015)

Study on composition of aroma components and polyphenols in Lycium ruthenicum Murr.

  • WU Yun ,
  • CHENG Zhenyu ,
  • WANG Lipeng ,
  • HU Haobin ,
  • HU Wenjie ,
  • MENG Yongchen
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  • 1(College of Petroleum and Chemical Engineering, Longdong University, Qingyang 745000, China)
    2(Gansu Key Laboratory of Efficient Utilization of Oil and Gas Resources in Longdong, Longdong University, Qingyang 745000, China)

Received date: 2024-02-24

  Revised date: 2024-04-15

  Online published: 2024-08-02

摘要

随着人类对健康和养生重视程度的不断提高,具有良好功效的药食同源植物黑果枸杞受到越来越多的关注,研究黑果枸杞中具有药理活性物质的化学成分,对其深加工和进一步开发利用具有重要的意义。该文对甘肃酒泉产的黑果枸杞鲜果的香气成分及多酚类物质的化学组成进行分析,采用顶空固相微萃取-气相色谱-质谱联用技术定性定量分析黑果枸杞鲜果香气成分;采用超高效液相色谱-电喷雾四级杆串联飞行时间质谱技术定性分析黑果枸杞鲜果中多酚类物质的组成。从黑果枸杞香气成分中鉴定出醇类、醛酮类、酯类、烃类等挥发性化学成分63种,占香气成分总量的95.4%,其中25种化合物为我国国家标准GB 2760—2014《食品安全国家标准 食品添加剂使用标准》规定的食品用合成香料;香气成分中醇类化合物共计26种,总含量占比最高(44.98%)。黑果枸杞多酚经提取和HPD-500大孔吸附树脂纯化后进行液相色谱-质谱联用测试,定性鉴别出73种多酚化合物,其主要由黄酮类和酚酸类等化合物组成。该研究初步确定了黑果枸杞香气和多酚类物质的化学成分,为黑果枸杞药用及食用功效的深入研究奠定了基础。

本文引用格式

武芸 , 程振玉 , 王丽朋 , 胡浩斌 , 胡文杰 , 蒙勇辰 . 黑果枸杞香气成分和多酚类物质的组成研究[J]. 食品与发酵工业, 2024 , 50(14) : 212 -219 . DOI: 10.13995/j.cnki.11-1802/ts.038952

Abstract

Lycium ruthenicum Murr., a medicinal and edible plant with good efficacy, has attracted more and more interest as human beings pay more and more attention to health and health care in the 21 st century.It is of great significance to study the chemical constituents of pharmacologically active substances in Lycium ruthenicum Murr., which is beneficial for its further processing, development and utilization in the fields of food industry and pharmaceuticals industry.The aim of this work is to analyze the aroma components and chemical composition of polyphenols in fresh fruit of Lycium ruthenicum Murr.from Jiuquan city, Gansu province.Headspace solid phase microextraction coupled with gas chromatography-mass spectrometry was used to qualitatively and quantitatively analyze the aroma components of fresh fruits of Lycium ruthenicum Murr.The chemical composition of polyphenols in fresh fruits was qualitatively analyzed by ultra-high performance liquid chromatography- electrospray ionization-qudropole time-of-flight mass spectrometry.A total of 63 volatile chemical components, including alcohols, aldehydes, ketones, esters, and hydrocarbons and other types of compounds were identified from the aroma components, accounting for 95.4% of the total aroma components.Among them, 25 compounds were the synthetic flavors for food in the National Standard GB 2760—2014 National Food safety Standard-Standard for the Use of Food Additives.There were 26 kinds of alcohols in the aroma components, and the total content accounted for the highest proportion (44.98%).After extraction and purification by HPD-500 macroporous adsorption resin, 73 polyphenol compounds were qualitatively identified by liquid-mass, which were mainly composed of flavonoids and phenolic acids.In this study, the chemical constituents of the aroma and polyphenols of were analyzed, which lay a foundation for the further study of the medicinal and edible effects of Lycium ruthenicum Murr.

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