该文探究对冬枣进行超声、微波、烫漂、汽蒸4种不同物理预处理对喷雾干燥冬枣粉理化性质的影响,在此基础上探究最佳工艺优化参数,主要是通过计算流体力学数值模拟分析了喷雾干燥过程的空气速度分布、温度分布和颗粒轨迹分布以及对冬枣粉集粉率、水分含量和出风温度的影响,并将模拟结果与实际结果进行正交试验。结果显示,超声预处理能显著提高冬枣粉的集粉率、总酚含量和黄酮含量,其中超声360 W、20 min处理效果最好,集粉率较对照组提高了31.87%、总酚含量提高了31.89%,黄酮含量提高了47.18%,同时超声预处理提高了冬枣粉的黄绿色;结合数值模拟和正交试验结果,确定冬枣最佳喷雾干燥工艺参数组合为进风温度120 ℃,进料速度0.45 L/h,进料浓度10%,模拟结果集粉率为91.78%、实验结果集粉率为89.54%。因此,该研究结果表明物理预处理结合喷雾干燥参数优化有利于制备高品质冬枣粉,为冬枣粉在食品工业的进一步应用提供一定的参考价值。
The effects of ultrasound, microwave, blanching, and steaming on the physicochemical properties of spray-dried winter jujube powder were investigated.On this basis, the optimal process optimization parameters were explored, mainly through computational fluid dynamics numerical simulation was used to analyze the air velocity distribution, temperature distribution, and particle trajectory distribution in the spray drying process, as well as the impact on the powder collection rate, moisture content, and air outlet temperature of winter jujube powder.And the article conducted orthogonal experiments between simulated and actual results. Results showed that ultrasonic pretreatment could significantly improve the powder collection rate, total phenol content, and flavonoid content of winter jujube powder.Among them, ultrasound treatment with 360 W and 20 min had the best effect, with a powder collection rate increased by 31.87%, total phenol content increased by 31.89%, and flavonoid content increased by 47.18% compared with the control group.At the same time, ultrasonic pretreatment improved the yellow-green color of winter jujube powder.Combined with the results of numerical simulation and orthogonal experiment, the optimal combination of spray drying process parameters of winter jujube was determined as air inlet temperature of 120 ℃, feed rate of 0.45 L/h, feed concentration of 10%, the powder collection rate of simulation results was 91.78%, and the powder collection rate of experimental results was 89.54%.Therefore, the research results of physical pretreatment combined with spray drying parameters optimization were conducive to the preparation of high-quality winter jujube powder, which provided a certain reference value for the further application of winter jujube powder in the food industry.
[1] RYBAK K, WIKTOR A, WITROWA-RAJCHERT D, et al.The quality of red bell pepper subjected to freeze-drying preceded by traditional and novel pretreatment[J].Foods, 2021, 10(2):226.
[2] NI J B, DING C J, ZHANG Y M, et al.Influence of ultrasonic pretreatment on electrohydrodynamic drying process of goji berry[J].Journal of Food Processing and Preservation, 2020, 44(8):e14600.
[3] MOTHIBE K J, ZHANG M, MUJUMDAR A S, et al.Effects of ultrasound and microwave pretreatments of apple before spouted bed drying on rate of dehydration and physical properties[J].Drying Technology, 2014, 32(15):1848-1856.
[4] KAVEH M, TAGHINEZHAD E, AZIZ M.Effects of physical and chemical pretreatments on drying and quality properties of blackberry (Rubus spp.) in hot air dryer[J].Food Science & Nutrition, 2020, 8(7):3843-3856.
[5] JANISZEWSKA-TURAK E, WITROWA-RAJCHERT D.The influence of carrot pretreatment, type of carrier and disc speed on the physical and chemical properties of spray-dried carrot juice microcapsules[J].Drying Technology, 2021, 39(4):439-449.
[6] FUNK K, ZABIK M E.Comparison of frozen, foam-spray-dried, freeze-dried and spray-dried eggs[J].Journal of Food Science, 1971, 36(5):715-717.
[7] WOJDYŁO A, FIGIEL A, LEGUA P, et al.Chemical composition, antioxidant capacity, and sensory quality of dried jujube fruits as affected by cultivar and drying method[J].Food Chemistry, 2016, 207:170-179.
[8] FELFOUL I, BURGAIN J, PERROUD C, et al.Impact of spray-drying conditions on physicochemical properties and rehydration ability of skim dromedary and cow's milk powders[J].Drying Technology, 2022, 40(3):665-677.
[9] FAKHER DIZAJI M, HAMIDISEPEHR A, CHEGINI G, et al.Influence of hot bed spray dryer parameters on physical properties of peppermint (Mentha piperita L.) tea powder[J].International Journal of Food Engineering, 2015, 11(1):115-125.
[10] MINH N P.Variables influencing to spray drying of Durian (Durio Zibethinus) juice into powder[J].Bioscience Research, 2021, 18(1):936-943.
[11] 付晓伟, 吴晓, 姜莉莉, 等.紫外分光光度法测定水果中维生素C含量[J].山东化工, 2020, 49(24):102-103;105.
FU X W, WU X, JIANG L L, et al.Deter mination of vitamin C in fruits by UV spectrophotometry[J].Shandong Chemical Industry, 2020, 49(24):102-103;105.
[12] WU F, SHI S L, LIU C, et al.Optimization of the extraction of total phenols from medicago sativa and its antioxidant capacity[J].Chemistry & Biodiversity, 2022, 19(4):e202100898.
[13] SUN L J, ZHANG J B, LU X Y, et al.Evaluation to the antioxidant activity of total flavonoids extract from persimmon (Diospyros kaki L.) leaves[J].Food and Chemical Toxicology, 2011, 49(10):2689-2696.
[14] LANGRISH T A G, FLETCHER D F.Spray drying of food ingredients and applications of CFD in spray drying[J].Chemical Engineering and Processing: Process Intensification, 2001, 40(4):345-354.
[15] 杜静, 刘滔, 徐泽, 等.柿果浆低温喷雾干燥数值模拟与试验[J].食品工业科技, 2015, 36(21):237-241;248.
DU J, LIU T, XU Z, et al.Numberical simulation and experiment verification study on low temperature spray-drying of persimmon pulp[J].Science and Technology of Food Industry, 2015, 36(21):237-241;248.
[16] MIANO A C, IBARZ A, AUGUSTO P E D.Mechanisms for improving mass transfer in food with ultrasound technology:Describing the phenomena in two model cases[J].Ultrasonics Sonochemistry, 2016, 29:413-419.
[17] GALOBURDA R, KUKA M, CAKSTE I, et al.The effect of blanching temperature on the quality of microwave-vacuum dried mushroom Cantharellus cibarius[J].Agronomy Research, 2015, 13(4):929-938.
[18] BASSEY E J, CHENG J H, SUN D W.Thermoultrasound and microwave-assisted freeze-thaw pretreatments for improving infrared drying and quality characteristics of red dragon fruit slices[J].Ultrasonics Sonochemistry, 2022, 91:106225.
[19] HAN H Y, WANG X H, WANG N L, et al.Lignans isolated from Campylotropis hirtella (Franch.) schindl.decreased prostate specific antigen and androgen receptor expression in LNCaP cells[J].Journal of Agricultural and Food Chemistry, 2008, 56(16):6928-6935.
[20] YUE Y M, ZANG Z P, WAN F X, et al.Effect of ultrasonic pretreatment on radio frequency vacuum drying characteristics and quality of Codonopsis pilosula slices[J].Agriculture, 2022, 13(1):72.
[21] DENG L Z, MUJUMDAR A S, ZHANG Q, et al.Chemical and physical pretreatments of fruits and vegetables:Effects on drying characteristics and quality attributes—A comprehensive review[J].Critical Reviews in Food Science and Nutrition, 2019, 59(9):1408-1432.
[22] 魏淑萍, 何易东.不同微波参数对真空微波膨化哈密瓜干的影响[J].食品科技, 2022, 47(12):60-66.
WEI S P, HE Y D.Effects of different microwave parameters on vacuum microwave puffing of dried cantaloupe[J].Food Science and Technology, 2022, 47(12):60-66.
[23] 裴昱鹏, 杨恺雯, 李栋, 等.高温高湿气体射流冲击烫漂对辣椒粉品质的影响[J].食品与发酵工业, 2023, 49(9):276-282.
PEI Y P, YANG K W, LI D, et al.Effects of high-humidity hot air impingement blanching on quality attributes of red pepper powder[J].Food and Fermentation Industries, 2023, 49(9):276-282.
[24] SALEH S N, HAMEED L A.CFD simulation of air flow patterns in a spray dryer fitted with a rotary disk[J].Iraqi Journal of Chemical and Petroleum Engineering, 2016, 17(2):69-77.
[25] XU M, CHEN Q S, KONG X B, et al.Heavy metal contamination and risk assessment in winter jujube (Ziziphus jujuba Mill.cv.Dongzao)[J].Food and Chemical Toxicology, 2023, 174:113645.
[26] 赵林林, 郭效德, 黄珊珊, 等.硝基胍连续喷雾干燥数值模拟研究[J].爆破器材, 2021, 50(5):21-27.
ZHAO L L, GUO X D, HUANG S S, et al, Numerical simulation of continuous spray drying of nitroguanidine[J].Explosive Materials, 2021, 50(5):21-27.
[27] GOULA A M, ADAMOPOULOS K G.Effect of maltodextrin addition during spray drying of tomato pulp in dehumidified air:I.drying kinetics and product recovery[J].Drying Technology, 2008, 26(6):726-737.
[28] TONON R V, BRABET C, HUBINGER M D.Influence of process conditions on the physicochemical properties of açai (Euterpe oleraceae Mart.) powder produced by spray drying[J].Journal of Food Engineering, 2008, 88(3):411-418.