研究报告

基于两种窨制工艺的茉莉绿片特征风味表征

  • 黄怡雯 ,
  • 安会敏 ,
  • 陈圆 ,
  • 刘佳顺 ,
  • 江游仓 ,
  • 应佳淇 ,
  • 陈宏宇 ,
  • 李适 ,
  • 刘仲华 ,
  • 黄建安
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  • 1(湖南农业大学 教育部茶学重点实验室,湖南 长沙,410128)
    2(国家植物功能成分利用工程技术研究中心,湖南 长沙,410128)
    3(湖南省植物功能成分利用省部共建协同创新中心,湖南 长沙,410128)
    4(农业农村部园艺作物基因资源评价利用重点实验室,湖南 长沙,410128)
第一作者: 硕士研究生(刘仲华教授和黄建安教授为共同通信作者,E-mail:larkin-liu@163.com;Jian7513@hunau.edu.cn)

收稿日期: 2024-08-14

  修回日期: 2024-11-20

  网络出版日期: 2025-08-01

基金资助

湖南千亿茶产业链关键技术创新与示范项目(2021NK1020-2,2021NK1020-4)茉莉花茶窨制新技术研究项目(湘财农指[2023]0053号)茉莉花茶加工关键技术创新与示范项目(2020NK2026)国家茶叶产业技术体系岗位科学家-功能成分利用项目(CARS-19)

Characteristic flavor of Jasmine Lvpian tea scented with two processes

  • HUANG Yiwen ,
  • AN Huimin ,
  • CHEN Yuan ,
  • LIU Jiashun ,
  • JIANG Youcang ,
  • YING Jiaqi ,
  • CHEN Hongyu ,
  • LI Shi ,
  • LIU Zhonghua ,
  • HUANG Jianan
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  • 1(Key Laboratory of Tea Science, Ministry of Education, Hunan Agricultural University, Changsha 410128, China)
    2(National Research Center of Engineering Technology for Utilization Ingredients from Botanical, Changsha 410128, China)
    3(Co-Innovation Center of Education Ministry for Utilization of Botanical Functional Ingredients, Changsha 410128, China)
    4(Key Laboratory for Evaluation and Utilization of Gene Resources of Horticultural Crops, Ministry of Agriculture and Rural Affairs, Hunan Agricultural University, Changsha 410128, China)

Received date: 2024-08-14

  Revised date: 2024-11-20

  Online published: 2025-08-01

摘要

茉莉绿片是以绿茶片茶和茉莉花为原料窨制而成的一种茉莉花茶,在茶饮料研发、茶产品升级和茶叶国际贸易中扮演重要角色。为探究窨制工艺对茉莉绿片特征风味的影响,该研究采用固相微萃取、高效液相色谱、全二维气相色谱-四极杆-飞行时间质谱等技术对控温拼合窨制的茉莉绿片(KWT)和隔离窨制的茉莉绿片(GLT)进行滋味和香气成分检测,并进行多元统计分析。结果表明,KWT香气和滋味感官评分均高于GLT;绿片和茉莉绿片中共鉴定出253种挥发性成分,其中乙酸苄酯、α-法呢烯、水杨酸甲酯等34种挥发性成分是区分绿片茶窨制前后香气差异的特征挥发性成分;吲哚、苯甲醛、苯甲酸甲酯等7种化合物被进一步鉴定为影响2种窨制工艺茉莉绿片香气特征的关键挥发性成分,其中KWT中含量较高的吲哚、邻氨基苯甲酸甲酯、顺式-3-己烯基苯甲酸酯和顺式-3-己烯酸顺式-3-己烯酯与“茉莉花香”强度显著正相关,有利于茉莉绿片香气品质;GLT中含量较高的苯甲酸甲酯、苯甲醛和乙酸叶醇酯与“青气”、“陈气”和“闷浊感”强度正相关,不利于茉莉绿片香气品质。JTF指数和XFJTF指数结果显示,KWT得分远高于GLT,控温拼合窨制技术更有利于茉莉绿片风味。该研究结果为茉莉花茶加工技术创新、品质提升提供了理论依据。

本文引用格式

黄怡雯 , 安会敏 , 陈圆 , 刘佳顺 , 江游仓 , 应佳淇 , 陈宏宇 , 李适 , 刘仲华 , 黄建安 . 基于两种窨制工艺的茉莉绿片特征风味表征[J]. 食品与发酵工业, 2025 , 51(14) : 218 -227 . DOI: 10.13995/j.cnki.11-1802/ts.040751

Abstract

Jasmine Lvpian tea is a kind of jasmine tea with Lvpian tea and jasmine flower as the scenting material.Lvpian tea plays an important role in tea beverage research and development, tea product upgrading, and tea international trade.To investigate the effect of the scenting process on the characteristic flavor of Jasmine Lvpian tea, many methods were adopted, such as high performance liquid chromatography, solid-phase microextraction, comprehensive two-dimensional gas chromatography-quadrupole time-of-flight mass spectrometry, and other technologies.These techniques were used to detect the flavor and aroma components of temperature-controlled hybrid Jasmine Lvpian tea (KWT) and isolated scenting Jasmine Lvpian tea (GLT), and multivariate statistical analysis was performed.Results showed that KWT had higher sensory scores for aroma and taste than GLT.A total of 253 volatile components from Lvpian tea and Jasmine Lvpian tea were identified.Among them, 34 volatile components such as acetic acid, phenylmethyl ester, α-farnesene, and methyl salicylate, were identified as characteristic volatile components to distinguish the aroma differences of Lvpian tea before and after scenting.Seven compounds, including indole, benzaldehyde, and benzoic acid, methyl ester, were further identified as the key volatile components affecting the aroma characteristics of Jasmine Lvpian tea in two scenting processes.Among them, the contents of indole, methyl ortho anthranilate, cis-3-hexenyl, and cis-3-hexenoic acid cis-3-hexenyl ester were higher in KWT and were significantly positively correlated with the intensity of jasmine fragrance.It was beneficial to the aroma quality of Jasmine Lvpian tea.The higher content of methyl benzoate, benzaldehyde, and ethyl acetate in GLT was positively correlated with the intensity of grass, stale, and dull odor.It reduced the aroma quality of Jasmine Lvpian tea.The results of the JTF index and XFJTF index showed that the score of KWT was much higher than that of GLT.The temperature-controlled hybrid scenting technique was more beneficial to the flavor of Jasmine Lvpian tea.These research results provided a theoretical basis for the technological innovation and quality improvement of jasmine tea processing.

参考文献

[1] 翁玉宝. 高档茉莉花茶窨制新工艺应用探讨[J].福建茶叶, 1996,18(1):23-24.
WENG Y B.Discussion on the application of new scenting technology of high-grade jasmine tea[J].Tea in Fujian, 1996,18(1):23-24.
[2] 危赛明. 中国茉莉花茶出口现状与发展对策[J].中国茶叶, 2017,39(6):34-36.
WEI S M.Present situation and development countermeasures of jasmine tea export in China[J].China Tea, 2017,39(6):34-36.
[3] 张钰婷, 叶秋萍, 程淑华, 等.茉莉花茶加工技术与吸香机理研究现状[J].热带作物学报, 2016, 37(1):203-207.
ZHANG Y T, YE Q P, CHENG S H, et al.Technology and mechanism of jasmine tea scenting[J].Chinese Journal of Tropical Crops, 2016, 37(1):203-207.
[4] 朱树林. 论茉莉花茶窨制过程中温度的影响与控制[J].广西热作科技, 1999,12(3):6-11.
ZHU S L.On the influence and control of temperature in the process of making jasmine tea[J].Guangxi Science & Technology of Tropical Crops, 1999,12(3):6-11.
[5] 倪昌谋. 浅述茉莉花茶窨制工艺[J].福建茶叶, 2023, 45(6):18-20.
NI C M.Brief discussion on the brewing technology of jasmine tea[J].Tea in Fujian, 2023, 45(6):18-20.
[6] 马静. 茉莉花茶窨制过程香气及其他理化因子变化规律的研究[D].北京:中国农业科学院, 2001.
MA J.Study on changes of aroma and other physical and chemical factors during scenting processes of jasmine tea[D].Beijing:Chinese Academy of Agricultural Sciences, 2001.
[7] 卢健. 茉莉花茶窨制过程中主要挥发性物质变化及工艺改进研究[D].杭州:浙江大学, 2015.
LU J.Research on the changes of volatile compounds of jasmine tea during the scenting process and technology improvement[D].Hangzhou:Zhejiang University, 2015.
[8] 卢健, 王东, 朱建杰, 等.茉莉花茶隔离窨制中主要影响因子对挥发性组分的影响[J].中国食品学报, 2019, 19(1):65-74.
LU J, WANG D, ZHU J J, et al.Effects of main factors on the volatile compounds of jasmine scented tea during the isolated scenting process[J].Journal of Chinese Institute of Food Science and Technology, 2019, 19(1):65-74.
[9] 卢健, 王东, 汪群, 等.传统窨制与隔离窨制中茉莉花茶香气成分的比较分析[J].中国农学通报, 2022, 38(25):158-164.
LU J, WANG D, WANG Q, et al.Comparison analysis of aromatic constituents of jasmine scented tea during orthodox and isolated scenting process[J].Chinese Agricultural Science Bulletin, 2022, 38(25):158-164.
[10] 陈志伟. 探讨茉莉花茶香气的影响因素[J].福建茶叶, 2023, 45(5):130-132.
CHEN Z W.To explore the influencing factors of jasmine tea aroma[J].Tea in Fujian, 2023, 45(5):130-132.
[11] 徐永成. 世界茶业经贸变化与特点[J].中国茶叶, 2004, 26(3):4-6.
XU Y C.Dynamics and characteristic of tea trade in world tea industry[J].China Tea, 2004, 26(3):4-6.
[12] 徐颖, 乔薪蓓, 贾娟.我国袋泡茶的种类及发展对策[J].中国果菜, 2022, 42(7):80-84.
XU Y, QIAO X B, JIA J.Types and development countermeasures of bagged tea in China[J].China Fruit & Vegetable, 2022, 42(7):80-84.
[13] 詹承烨. 绿碎茶的制造[J].蚕桑茶叶通讯, 1992(1):16-18.
ZHAN C Y.Manufacture of green broken tea[J].Newsletter of Sericulture and Tea, 1992(1):16-18.
[14] 叶飞, 桂安辉, 刘盼盼, 等.茉莉绿碎茶窨花工艺的优化及理化品质改善[J].现代食品科技, 2022, 38(3):135-142.
YE F, GUI A H, LIU P P, et al.Physico-chemical characteristics improvement and scenting process optimization of jasmine broken green tea[J].Modern Food Science and Technology, 2022, 38(3):135-142.
[15] 叶秋萍, 余雯, 郑世仲, 等.茉莉花茶窨制过程水分变化与香气品质变化的相关性分析[J].食品科学, 2022, 43(24):266-272.
YE Q P, YU W, ZHENG S Z, et al.Correlation analysis of moisture content and aroma quality in the scenting process of jasmine tea[J].Food Science, 2022, 43(24):266-272.
[16] 方世辉, 徐国谦, 夏涛, 等.花茶窨制中几个主要因子对花茶香气的影响[J].安徽农业大学学报, 2004, 31(4):440-445.
FANG S H, XU G Q, XIA T, et al.Influences of main factors on the aroma of scented tea[J].Journal of Anhui Agricultural University, 2004, 31(4):440-445.
[17] AN H M, OU X C, ZHANG Y B, et al.Study on the key volatile compounds and aroma quality of jasmine tea with different scenting technology[J].Food Chemistry, 2022, 385:132718.
[18] 刘佳顺, 安会敏, 陈圆, 等.窨制对不同类型黑茶香气的影响[J].食品科学, 2023, 44(18):294-304.
LIU J S, AN H M, CHEN Y, et al.Effect of scenting on aroma of different types of dark tea[J].Food Science, 2023, 44(18):294-304.
[19] LIN J, CHEN Y, ZHANG P, et al.A novel quality evaluation index and strategies to identify scenting quality of jasmine tea based on headspace volatiles analysis[J].Food Science and Biotechnology, 2013, 22(2):331-340.
[20] 唐夏妮, 夏益民, 雷永宏, 等.利用茉莉花茶香气指数鉴定其窨制品质及构建决策树模型[J].茶叶科学, 2016, 36(6):646-654.
TANG X N, XIA Y M, LEI Y H, et al.The construction of jasmine tea flavor index and decision tree model in identificating scenting quality[J].Journal of Tea Science, 2016, 36(6):646-654.
[21] 陈梅春, 林增钦, 郑梅霞, 等.茉莉花茶香气品质评价指标的构建与研究[J].茶叶通讯, 2021, 48(1):90-97.
CHEN M C, LIN Z Q, ZHENG M X, et al.Construction and study on aroma quality evaluation index of jasmine tea[J].Journal of Tea Communication, 2021, 48(1):90-97.
[22] LI C F, YAO M Z, MA C L, et al.Differential metabolic profiles during the albescent stages of ‘Anji baicha’ (Camellia sinensis)[J].PLoS One, 2015, 10(10):e0139996.
[23] STUPAK M, GOODALL I,TOMANIOVA M, et al.A novel approach to assess the quality and authenticity of Scotch Whisky based on gas chromatography coupled to high resolution mass spectrometry[J].Analytica Chimica Acta, 2018, 1042:60-70.
[24] 徐国谦, 方世辉, 夏涛.茉莉花茶加工工艺研究进展[J].福建茶叶, 2001,23(2):10-12.
XU G Q, FANG S H, XIA T.Progress in the studies on proceeding technology for the jasmine flower tea[J].Tea in Fujian, 2001,23(2):10-12.
[25] 韦雅杰, 高彦祥.茶汤滋味物质及其调控研究进展[J].食品研究与开发, 2022, 43(11):189-197.
WEI Y J, GAO Y X.Taste-related compounds in tea infusion and the regulation:A review[J].Food Research and Development, 2022, 43(11):189-197.
[26] 陆宁, 宛晓春, 潘冬.茉莉花茶香气成分与品质之间关系的初步研究[J].食品科学, 2004, 25(6):93-97.
LU N, WAN X C, PAN D.Extraction and analysis of jasmine tea aroma constituents of three different grades[J].Food Science, 2004, 25(6):93-97.
[27] 安会敏, 欧行畅, 熊一帆, 等.茉莉花茶特征香气成分研究[J].茶叶科学, 2020, 40(2):225-237.
AN H M, OU X C, XIONG Y F, et al.Study on the characteristic aroma components of jasmine tea[J].Journal of Tea Science, 2020, 40(2):225-237.
[28] ZENG L T, ZHOU Y, GUI J D, et al.Formation of volatile tea constituent indole during the oolong tea manufacturing process[J].Journal of Agricultural and Food Chemistry, 2016, 64(24):5011-5019.
[29] ZHANG C, ZHOU C Z, TIAN C Y, et al.Volatilomics analysis of jasmine tea during multiple rounds of scenting processes[J].Foods, 2023, 12(4):812.
[30] 黄新安, 宛晓春, 夏涛.小花茉莉清香品质研究[J].茶业通报, 2007, 29(2):73-74.
HUANG X A, WAN X C, XIA T.Study on the fragrant quality of jasmine parviflora[J].Journal of Tea Business, 2007, 29(2):73-74.
[31] 刘用敏. 各级茶叶表面吸附的物理量计算. 茶叶科学简报, 1990, 31(2):32-35.
LIU Y M. Calculation of physical quantities adsorbed on the surface of tea at all levels. Acta Tea Sinica, 1990, 31(2):32-35.
[32] 张丽霞. 茉莉花茶加工理论研究进展[J].茶叶通讯, 1998,25(1):21-23.
ZHANG L X.Research progress on processing theory of jasmine tea[J].Journal of Tea Communication, 1998,25(1):21-23.
[33] 周跃斌, 杨伟丽, 施兆鹏.茶叶吸香机理的探讨[J].湖南农业大学学报, 1998,24(6):445-449.
ZHOU Y B, YANG W L, SHI Z P.A study on teas mechanism of absorption of jasmine scent[J].Journal of Hunan Agricultural University (Natural Sciences), 1998,24(6):445-449.
[34] 杨伟丽, 周跃斌, 朱旗.论茉莉花茶的湿窨机制[J].湖南农业大学学报(自然科学版), 2000, 26(5):401-404.
YANG W L, ZHOU Y B, ZHU Q.Wet scenting mechanism of jasmine tea[J].Journal of Hunan Agricultural University, 2000, 26(5):401-404.
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