食品与发酵工业 >

2026 , Vol. 52 >Issue 15: 356 - 364

DOI: https://doi.org/10.13995/j.cnki.11-1802/ts.044438

研究报告

山茱萸多糖-壳聚糖复合膜的制备及其在红提保鲜中的应用

  • 耿卿琳 ,
  • 毕保雪 ,
  • 薛淑娟 ,
  • 崔永霞 ,
  • 王利丽 ,
  • 程俊儒 ,
  • 马晓东
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  • 1(河南中医药大学 药学院,河南 郑州,450046)
    2(河南中医药大学,豫药全产业链研发河南省协同创新中心,河南 郑州,450046)
    3(河南概验现代中医药科技有限公司,河南 郑州,450046)
第一作者:硕士研究生(王利丽教授为通信作者,E-mail:wllywlly2004@163.com)

收稿日期: 2025-09-05

  修回日期: 2025-12-18

  网络出版日期: 2026-08-20

基金资助

2023年郑州市协同创新专项(2023XTCX053)

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Preparation of Cornus officinalis polysaccharide-chitosan composite film and its application in red grapes preservation

  • GENG Qinglin ,
  • BI Baoxue ,
  • XUE Shujuan ,
  • CUI Yongxia ,
  • WANG Lili ,
  • CHENG Junru ,
  • MA Xiaodong
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  • 1(College of Pharmacy, Henan University of Chinese Medicine, Zhengzhou 450046,China)
    2(Collaborative Innovation Center of Research and Development on the whole Industry Chain of Yu-Yao, Henan University of Chinese Medicine, Zhengzhou 450046,China)
    3(Henan Gaiyan Modern Chinese Medicine Technology Co.Ltd.,Zhengzhou 450046,China)

Received date: 2025-09-05

  Revised date: 2025-12-18

  Online published: 2026-08-20

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摘要

该研究以山茱萸多糖(Cornus officinalis polysaccharide,COP)与壳聚糖(chitosan,CS)为基质制备复合膜,并对其保鲜性能进行实验探究。首先采用水提醇沉法对山茱萸进行多糖提取,Sevag法(氯仿∶正丁醇)脱蛋白,大孔吸附树脂脱色,透析袋除去小分子物质;其次以COP为原料,CS为成膜基质,采用流延法制备出5种COP-CS复合膜。通过对复合膜理化性能的研究,表明CS∶COP质量比1∶1复合膜具有更好的机械性能和水蒸气透过率及阻油性,通过扫描电镜观察其复合膜结构发现COP-CS复合膜[COP∶CS(1∶1)]的膜结构较为紧密。以红提进行保鲜实验,发现COP-CS复合膜能有效延长红提的保鲜时间,为今后COP复合膜制备的工业化生产奠定基础。

关键词： 山茱萸多糖; 壳聚糖; 复合膜; 保鲜

本文引用格式

耿卿琳 , 毕保雪 , 薛淑娟 , 崔永霞 , 王利丽 , 程俊儒 , 马晓东 . 山茱萸多糖-壳聚糖复合膜的制备及其在红提保鲜中的应用[J]. 食品与发酵工业, 2026 , 52(15) : 356 -364 . DOI: 10.13995/j.cnki.11-1802/ts.044438

Abstract

Composite films were prepared using Cornus officinalis polysaccharide (COP) and chitosan as the matrix, and its preservation performance was experimentally investigated.Firstly, polysaccharide extraction of COP was carried out by the aqueous alcoholic precipitation method, polysaccharide deproteinization by the Sevag method (chloroform∶n-butanol), decolorization by macroporous adsorbent resin, and removal of small molecules by dialysis bag.Secondly, five types of COP-CS composite films were prepared using the casting method, with COP as the active component and chitosan (CS) as the film-forming matrix.The study of the physicochemical properties of the membrane agents showed that the composite membranes possessed better mechanical properties and water vapor permeability, as well as better oil-blocking properties, compared with the CS and COP membranes as single membranes.Finally, the membrane structure of the composite membrane was observed by scanning electron microscopy, and it was found that the membrane structure of the COP-CS composite, COP∶CS(1∶1), membrane was more compact.Using red grape for preservation experiments, it was found that the composite film of COP and CS could effectively extend the preservation time of red grapes, laying the foundation for the industrial production of COP composite film preparation in the future.

Key words： Cornus officinalis polysaccharide; chitosan; composite membrane; freshness preservation

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